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Basic Information
CAS No.: 3622-84-2
Name: N-n-Butylbenzenesulfonamide
Molecular Structure:
Molecular Structure of 3622-84-2 (N-n-Butylbenzenesulfonamide)
Formula: C10H15NO2S
Molecular Weight: 213.301
Synonyms: AK 551;BBSA;BM 4 (sulfonamide);Cetamoll BMB;Dellatol BBS;N-(n-Butyl)benzenesulfonamide;NSC 3536;PlasthallBSA;Plastomoll BMB;Topcizer 7;Uniplex 214;BM 4;N-Butyl-benzenesulfonamide;
EINECS: 222-823-6
Density: 1.125 g/cm3
Melting Point: -30oC
Boiling Point: 326.7 °C at 760 mmHg
Flash Point: 151.4 °C
Solubility: 450mg/L at 20℃
Appearance: COA
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
PSA: 54.55000
LogP: 3.23670
Synthetic route
109-73-9

N-butylamine

98-09-9

benzenesulfonyl chloride

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
With sodium hydroxide In water at 25℃; pH=10.2;99%
With sodium hydroxide In water at 20℃; for 1.5h; Reagent/catalyst;99%
In dichloromethane at 0 - 20℃; for 0.25h;98%
109-73-9

N-butylamine

microgel-supported-PhSO2

microgel-supported-PhSO2

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
In tetrahydrofuran at 25℃; for 13.5h; Inert atmosphere;97.6%
6829-66-9

N-butylbenzenesulfinamide

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 0.5h;93%

C24H32N3O3S(1+)*F6P(1-)

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
With trifluoroacetic acid for 10h;91%
873-55-2

sodium benzenesulfonate

109-73-9

N-butylamine

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
With iodine In 1,2-dichloro-ethane at 25℃; for 12h;90%
108-98-5

thiophenol

109-73-9

N-butylamine

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
With hydrogenchloride; tetramethylammonium tetrafluoroborate In water; acetonitrile at 20℃; for 0.0833333h; Electrochemical reaction;81%
98-10-2

benzenesulfonamide

142-96-1

dibutyl ether

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
With titanium tetrachloride In 1,1,2,2-tetrachloroethane at 120℃; for 48h; sealed tube;80%
109-73-9

N-butylamine

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
Stage #1: N-butylamine With N-Bromosuccinimide; tetraethylammoniumcyanide In dichloromethane
Stage #2: PVS In dichloromethane at 20℃; for 1h;
72%
1212-08-4

S-Phenyl benzenethiosulfonate

109-73-9

N-butylamine

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
With N-Bromosuccinimide; caesium carbonate In ethanol at 80℃; for 16h; Sealed tube;66%
369-57-3

benzenediazonium tetrafluoroborate

109-73-9

N-butylamine

3622-84-2

N-butylbenzenesulfonamide

Conditions
ConditionsYield
Stage #1: benzenediazonium tetrafluoroborate With 1,4-diazabicyclo[2.2.2]octane-triethylenediamine-bis(sulfur dioxide); benzotriazol-1-ol In 1,2-dichloro-ethane at 60℃; for 1h; Inert atmosphere;
Stage #2: N-butylamine With N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane at 20℃; for 2h; Inert atmosphere;
64%
Downstream Products
5339-59-3
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Chemistry

IUPAC Name:N-butylbenzenesulfonamide
Molecular Formula:C10H15NO2S
Molecular Weight:213.296600 g/mol
Appearance:clear oily liquid
Melting Point:-30 °C
Boiling Point:314 °C(lit.)
Flash Point:>230 °F
density:1.15 g/mL at 25 °C(lit.)
vapor pressure:0.35 mm Hg ( 150 °C)
refractive index:n20/D 1.525(lit.)
EINECS:222-823-6
Synonyms of N-BUTYLBENZENESULFONAMIDE(3622-84-2):
TIMTEC-BB SBB008484;RIT-CIZER NO 7;N-N-BUTYLBENZENESULFONAMIDE;N-N-BUTYLBENZENESULPHONAMIDE;N-BENZENESULFONYL-N-BUTYLAMINE;N-BUTYLBENZENESULFONAMIDE;(butyl)benzenesulfonamide;Benzenesulfonamide,N-butyl-;N-n-Butylbenzenesulfonamide
Categories of N-BUTYLBENZENESULFONAMIDE(3622-84-2):
Camphor, etc. (Plasticizer);Functional Materials;Plasticizer;Organic Building Blocks;Sulfonamides/Sulfinamides;Sulfur Compounds

Uses

N-BUTYLBENZENESULFONAMIDE(3622-84-2) is used as a plasticizer in polyamide and cellulose resin.

Toxicity Data With Reference

1.    

orl-rat LD50:2050 mg/kg

    TPKVAL    Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Sciences. 15 (1979),110.
2.    

orl-mus LD50:2500 mg/kg

    TPKVAL    Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Sciences. 15 (1979),110.
3.    

orl-uns LD50:2900 mg/kg

    GISAAA    Gigiena i Sanitariya. 39 (4)(1974),86.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Safety Information of N-BUTYLBENZENESULFONAMIDE(3622-84-2):
Hazard Codes:Xi
Risk Statements:36/37/38
36/37/38:Irritating to eyes, respiratory system and skin
Safety Statements:26-36
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36:Wear suitable protective clothing
WGK Germany:2
RTECS:DB1283000
Moderately toxic by ingestion. When heated to decomposition it emits toxic vapors of NOx and SOx.