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| CAS No.: | 3622-84-2 |
|---|---|
| Name: | N-n-Butylbenzenesulfonamide |
| Molecular Structure: | |
|
|
|
| Formula: | C10H15NO2S |
| Molecular Weight: | 213.301 |
| Synonyms: | AK 551;BBSA;BM 4 (sulfonamide);Cetamoll BMB;Dellatol BBS;N-(n-Butyl)benzenesulfonamide;NSC 3536;PlasthallBSA;Plastomoll BMB;Topcizer 7;Uniplex 214;BM 4;N-Butyl-benzenesulfonamide; |
| EINECS: | 222-823-6 |
| Density: | 1.125 g/cm3 |
| Melting Point: | -30oC |
| Boiling Point: | 326.7 °C at 760 mmHg |
| Flash Point: | 151.4 °C |
| Solubility: | 450mg/L at 20℃ |
| Appearance: | COA |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 26-36 |
| PSA: | 54.55000 |
| LogP: | 3.23670 |
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| Conditions | Yield |
|---|---|
| With sodium hydroxide In water at 25℃; pH=10.2; | 99% |
| With sodium hydroxide In water at 20℃; for 1.5h; Reagent/catalyst; | 99% |
| In dichloromethane at 0 - 20℃; for 0.25h; | 98% |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 25℃; for 13.5h; Inert atmosphere; | 97.6% |
| Conditions | Yield |
|---|---|
| With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 0.5h; | 93% |
- 3622-84-2
N-butylbenzenesulfonamide
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid for 10h; | 91% |
| Conditions | Yield |
|---|---|
| With iodine In 1,2-dichloro-ethane at 25℃; for 12h; | 90% |
| Conditions | Yield |
|---|---|
| With hydrogenchloride; tetramethylammonium tetrafluoroborate In water; acetonitrile at 20℃; for 0.0833333h; Electrochemical reaction; | 81% |
| Conditions | Yield |
|---|---|
| With titanium tetrachloride In 1,1,2,2-tetrachloroethane at 120℃; for 48h; sealed tube; | 80% |
| Conditions | Yield |
|---|---|
| Stage #1: N-butylamine With N-Bromosuccinimide; tetraethylammoniumcyanide In dichloromethane Stage #2: PVS In dichloromethane at 20℃; for 1h; | 72% |
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; caesium carbonate In ethanol at 80℃; for 16h; Sealed tube; | 66% |
| Conditions | Yield |
|---|---|
| Stage #1: benzenediazonium tetrafluoroborate With 1,4-diazabicyclo[2.2.2]octane-triethylenediamine-bis(sulfur dioxide); benzotriazol-1-ol In 1,2-dichloro-ethane at 60℃; for 1h; Inert atmosphere; Stage #2: N-butylamine With N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane at 20℃; for 2h; Inert atmosphere; | 64% |
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Chemistry
IUPAC Name:N-butylbenzenesulfonamide
Molecular Formula:C10H15NO2S
Molecular Weight:213.296600 g/mol
Appearance:clear oily liquid
Melting Point:-30 °C
Boiling Point:314 °C(lit.)
Flash Point:>230 °F
density:1.15 g/mL at 25 °C(lit.)
vapor pressure:0.35 mm Hg ( 150 °C)
refractive index:n20/D 1.525(lit.)
EINECS:222-823-6
Synonyms of N-BUTYLBENZENESULFONAMIDE(3622-84-2):
TIMTEC-BB SBB008484;RIT-CIZER NO 7;N-N-BUTYLBENZENESULFONAMIDE;N-N-BUTYLBENZENESULPHONAMIDE;N-BENZENESULFONYL-N-BUTYLAMINE;N-BUTYLBENZENESULFONAMIDE;(butyl)benzenesulfonamide;Benzenesulfonamide,N-butyl-;N-n-Butylbenzenesulfonamide
Categories of N-BUTYLBENZENESULFONAMIDE(3622-84-2):
Camphor, etc. (Plasticizer);Functional Materials;Plasticizer;Organic Building Blocks;Sulfonamides/Sulfinamides;Sulfur Compounds
Uses
N-BUTYLBENZENESULFONAMIDE(3622-84-2) is used as a plasticizer in polyamide and cellulose resin.
Toxicity Data With Reference
| 1. | orl-rat LD50:2050 mg/kg | TPKVAL Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Sciences. 15 (1979),110. | ||
| 2. | orl-mus LD50:2500 mg/kg | TPKVAL Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Sciences. 15 (1979),110. | ||
| 3. | orl-uns LD50:2900 mg/kg | GISAAA Gigiena i Sanitariya. 39 (4)(1974),86. |
Consensus Reports
Safety Profile
Safety Information of N-BUTYLBENZENESULFONAMIDE(3622-84-2):
Hazard Codes:Xi 
Risk Statements:36/37/38
36/37/38:Irritating to eyes, respiratory system and skin
Safety Statements:26-36
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36:Wear suitable protective clothing
WGK Germany:2
RTECS:DB1283000
Moderately toxic by ingestion. When heated to decomposition it emits toxic vapors of NOx and SOx.