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| CAS No.: | 3652-92-4 |
|---|---|
| Name: | 1,3-Dimethyl-1,3-dihydro-2-phenyl-2H-benzimidazole |
| Article Data: | 29 |
| Molecular Structure: | |
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| Formula: | C15H16N2 |
| Molecular Weight: | 224.305 |
| Synonyms: | 1,3-Dimethyl-2-phenyl-2,3-dihydro-1H-benzimidazol;Benzimidazoline,1,3-dimethyl-2-phenyl;1,3-Dimethyl-2-phenylbenzimidazolin;HMS1473O11;1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzimidazole;1,3-Dimethyl-2-phenylbenzimidazoline;1,3-dimethyl-2-phenyl-2,3-dihydrobenzimidazoline;1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzoimidazole; |
| Density: | 1.095g/cm3 |
| Melting Point: | 93-94 °C |
| Boiling Point: | 359.9°C at 760 mmHg |
| Flash Point: | 160.2°C |
| PSA: | 6.48000 |
| LogP: | 3.40140 |
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benzaldehyde
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N,N'-dimethyl-1,2-phenylenediamine
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0333333h; | 100% |
| With acetic acid In methanol at 20℃; for 0.5h; | 86% |
| With acetic acid In methanol for 0.5h; Ambient temperature; | 65% |
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In methanol for 1h; Reduction; | 90% |
| With 1-Benzyl-1,4-dihydronicotinamide In water; isopropyl alcohol at 25℃; pH=6; Equilibrium constant; Reduction; |
- 3653-05-2
N,N’-dimethyl-2-phenyl-benzo[d]imidazolium iodide
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| With methanol; sodium tetrahydroborate at 20℃; for 1h; Inert atmosphere; | 89% |
| With methanol; sodium tetrahydroborate at 0 - 20℃; Inert atmosphere; | 77% |
| With sodium tetrahydroborate In methanol at 20℃; for 0.5h; | 70% |
- 7181-87-5
1,3-dimethylbenzimidazolium Iodide
- 100-58-3
phenylmagnesium bromide
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| In tetrahydrofuran for 11h; Heating; | 77% |
- 858784-83-5
N-methyl-2-(N-methyl-hydrazino)-aniline
- 100-52-7
benzaldehyde
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| With acetic acid |
- 858784-83-5
N-methyl-2-(N-methyl-hydrazino)-aniline
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benzaldehyde
- 64-19-7
acetic acid
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
- 53088-00-9
2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
- 74-88-4
methyl iodide
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| Stage #1: 2-phenyl-2,3-dihydro-1H-benzoimidazole; methyl iodide With sodium hydroxide In methanol at 110℃; Stage #2: With sodium tetrahydroborate In methanol for 1h; Further stages.; |
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1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: H2O; H2SO4 / 4 h / 85 °C View Scheme | |
| Multi-step reaction with 2 steps 1: conc. sulphuric acid / 4 h / Heating 2: 65 percent / glacial acetic acid / methanol / 0.5 h / Ambient temperature; other aromatic aldehydes View Scheme | |
| Multi-step reaction with 2 steps 1: sulfuric acid / 4 h / 85 °C 2: dichloromethane / 12 h / 0 - 20 °C / Molecular sieve; Inert atmosphere View Scheme |
- 49633-28-5
1,2-bis-(p-methylphenylsulfonamido)-benzene
- 3652-92-4
1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 4 N aq. sodium hydroxide / 0.33 h / Heating 2: conc. sulphuric acid / 4 h / Heating 3: 65 percent / glacial acetic acid / methanol / 0.5 h / Ambient temperature; other aromatic aldehydes View Scheme |
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- Total:31 Page 1 of 1 1
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