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365458-36-2

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Basic Information
CAS No.: 365458-36-2
Name: 1,3,2-Benzodioxaborole, 4,5,6,7-tetrafluoro-2-(pentafluorophenyl)-
Article Data: 3
Molecular Structure:
Molecular Structure of 365458-36-2 (1,3,2-Benzodioxaborole, 4,5,6,7-tetrafluoro-2-(pentafluorophenyl)-)
Formula: C12BF9O2
Molecular Weight: 357.927
Synonyms: 4,5,6,7-TETRAFLUORO-2-(2,3,4,5,6-PENTAFLUOROPHENYL)-1,3,2-BENZODIOXABOROLE;
Density: 1.72
Melting Point: 131-132℃
Boiling Point: 274℃
Flash Point: 119℃
PSA: 18.46000
LogP: 3.10510
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2-(pentafluorophenyl)-tetrafluoro-1,3,2-benzodioxaborole

Conditions
ConditionsYield
In toluene byproducts: water; mixt. heated to reflux; water removed by azeotropic distillation; after 4 h solvent evapd. under reduced pressure; residue sublimed at 110°C/0.1 mm Hg;87%
In toluene under N2; C6F4(OH)2 and C6F5B(OH)2 in toluene heated to reflux for 12 h using Dean-Stark apparatus; volatiles removed under reduced pressure; sublimed at 80°C; takenup in pentane; filtered; cryst. at -35°C; elem. anal.;42%
In toluene byproducts: H2O; (Ar or under vac.); mixed in toluene; heated to reflux; water removed byazeotropic distillation; after 4 h, solvent evapd. under reduced pressu re; sublimed at 110°C;
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