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Basic Information
CAS No.: 36916-19-5
Name: 5-CHLOOR-2-(3-METHYL-4H-1,2,4-TRIAZOOL-4-YL)BENZOFENON
Article Data: 22
Molecular Structure:
Molecular Structure of 36916-19-5 (5-CHLOOR-2-(3-METHYL-4H-1,2,4-TRIAZOOL-4-YL)BENZOFENON)
Formula: C16H12 Cl N3 O
Molecular Weight: 297.744
Synonyms: Benzophenone,5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)-
Density: 1.291g/cm3
Boiling Point: 529.798°C at 760 mmHg
Flash Point: 274.212°C
PSA: 47.78000
LogP: 3.46010
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Synthetic route
36916-18-4

7-Chloro-1-methyl-5-phenyl-s-triazolo<4,3-a>quinoline

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

Conditions
ConditionsYield
With potassium permanganate; sodium periodate; potassium carbonate In water; acetone for 100.7h;72.1%
Multi-step reaction with 2 steps
1: 20.8 percent / ozone in oxygen / methanol; CH2Cl2 / 12 h / cooling in an ice bath
2: 59.7 percent / AgNO3, 1N NaOH / methanol; H2O / 18 h / Ambient temperature
View Scheme
36916-20-8

4-(2-benzoyl-4-chlorophenyl)-5-methyl-4H-1,2,4-triazole-3-carboxaldehyde

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

Conditions
ConditionsYield
With sodium hydroxide; silver nitrate In methanol; water for 18h; Ambient temperature;59.7%
28981-97-7

alprazolam

A

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

B

triazolaminoquinoleine

Conditions
ConditionsYield
In methanol at 50℃; for 360h; aq. buffer; Irradiation;A n/a
B 50.65%
36916-18-4

7-Chloro-1-methyl-5-phenyl-s-triazolo<4,3-a>quinoline

A

75158-63-3

C17H12ClN3O

B

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

C

36916-20-8

4-(2-benzoyl-4-chlorophenyl)-5-methyl-4H-1,2,4-triazole-3-carboxaldehyde

Conditions
ConditionsYield
With ozone In methanol; dichloromethane at 0℃; for 12h;A 4%
B 43.5%
C 20.8%
...Expand
36916-18-4

7-Chloro-1-methyl-5-phenyl-s-triazolo<4,3-a>quinoline

A

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

B

36916-20-8

4-(2-benzoyl-4-chlorophenyl)-5-methyl-4H-1,2,4-triazole-3-carboxaldehyde

Conditions
ConditionsYield
With ruthenium(IV) oxide; sodium periodate In water; acetone at 0 - 4℃; for 23.5h;A 20.8%
B 18%
28981-97-7

alprazolam

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

Conditions
ConditionsYield
With hydrogenchloride In methanol
28981-97-7

alprazolam

A

28910-92-1

U 31957

B

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

C

triazolaminoquinoleine

Conditions
ConditionsYield
With hydrogenchloride In water for 8h; pH=3.6; Kinetics; Further Variations:; pH-values; UV-irradiation;
...Expand
10352-30-4

2,6-dichloro-4-phenylquinoline

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 74.5 percent / hydrazin hydrate / 1 h / Heating
2: 83.9 percent / xylene / 2.67 h / Heating
3: 20.8 percent / ozone in oxygen / methanol; CH2Cl2 / 12 h / cooling in an ice bath
4: 59.7 percent / AgNO3, 1N NaOH / methanol; H2O / 18 h / Ambient temperature
View Scheme
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6-chloro-2-hydrazino-4-phenylquinoline

36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 83.9 percent / xylene / 2.67 h / Heating
2: 20.8 percent / ozone in oxygen / methanol; CH2Cl2 / 12 h / cooling in an ice bath
3: 59.7 percent / AgNO3, 1N NaOH / methanol; H2O / 18 h / Ambient temperature
View Scheme
36916-19-5

5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

38150-27-5

5-chloro-2-[3-(hydroxymethyl)-5-methyl-4H-1,2,4-triazol-4-yl] benzophenone

Conditions
ConditionsYield
With paraformaldehyde In 5,5-dimethyl-1,3-cyclohexadiene72.8%
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    Methanone,[5-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)phenyl]phenyl- Purity 99% CAS NO.36916-19-5 Application:Pharmaceutical Intermediates / Active Pharmaceutical Ingredients / For Chemical Research

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