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CAS No.: | 3738-00-9 |
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Name: | AMBROX DL |
Article Data: | 21 |
Molecular Structure: | |
Formula: | C16H28 O |
Molecular Weight: | 236.398 |
Synonyms: | 3a,6,6,9a-Tetramethyldodecahydronaphtho[2,1-b]furan;Amberlyn; Ambrox DL; Cetalox; Dodecahydro-3a,6,6,9a-tetramethylnaphtho[2,1-b]furan;Synambran |
EINECS: | 223-118-6 |
Density: | 0.939 g/cm3 |
Melting Point: | 75-85ºC |
Boiling Point: | 273.9 ºC at 760 mmHg |
Flash Point: | 104.8 ºC |
Solubility: | Insoluble in water |
Appearance: | White crystalline solid |
PSA: | 9.23000 |
LogP: | 4.40800 |
(3aRS,5aSR,9aSR,9bRS)-3a,6,6,9a-tetramethyldodecahydronaphtho[2,1-b]furan
Conditions | Yield |
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iron(III) chloride; silica gel In dichloromethane; 1,2-dichloro-ethane at 24℃; for 0.333333h; Product distribution / selectivity; | 79% |
iron(III) chloride; silica gel In dichloromethane; 1,2-dichloro-ethane at 24℃; for 0.333333h; Product distribution / selectivity; | 79% |
iron(III) chloride In dichloromethane; 1,2-dichloro-ethane at 10℃; for 3h; Product distribution / selectivity; | |
scandium tris(trifluoromethanesulfonate) In dichloromethane at 20℃; for 6h; Product distribution / selectivity; | |
iron(III) chloride In dichloromethane; 1,2-dichloro-ethane at 10℃; for 3h; Product distribution / selectivity; |
A
(3aRS,5aSR,9aSR,9bRS)-3a,6,6,9a-tetramethyldodecahydronaphtho[2,1-b]furan
B
(3aSR,5aSR,9aSR,9bRS)-3a,6,6,9a-tetramethyldodecahydronaphtho[2,1-b]furan
Conditions | Yield |
---|---|
scandium tris(trifluoromethanesulfonate) In dichloromethane at 20℃; for 6h; Product distribution / selectivity; | |
methanesulfonic acid In dichloromethane at 0℃; for 0.333333h; Product distribution / selectivity; | |
iron(III) chloride; silica gel In dichloromethane; 1,2-dichloro-ethane at 20℃; for 0.333333h; Product distribution / selectivity; |