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3789-75-1

Basic Information
CAS No.: 3789-75-1
Name: 3-HYDROXY-4-PHENYLAZO-NAPHTHALENE-2-CARBOXYLIC ACID PHENYLAMIDE
Article Data: 7
Molecular Structure:
Molecular Structure of 3789-75-1 (3-HYDROXY-4-PHENYLAZO-NAPHTHALENE-2-CARBOXYLIC ACID PHENYLAMIDE)
Formula: C23H17 N3 O2
Molecular Weight: 367.407
Synonyms: 2-Naphthalenecarboxamide,3-hydroxy-N-phenyl-4-(phenylazo)- (9CI); 2-Naphthanilide, 3-hydroxy-4-(phenylazo)-(6CI,7CI,8CI); Bronze Red; Shanghai Bronze Red
Density: 1.23±0.1 g/cm3(Predicted)
Melting Point: 204-205 °C
Boiling Point: 535.2±45.0 °C(Predicted)
PSA: 74.05000
LogP: 4.83010
Synthetic route
92-77-3

2,3-oxynaphthoic acid phenylamide

100-34-5

benzene diazonium chloride

3789-75-1

1-phenylazo-2-hydroxy-3-phenylcarbamoylnaphthalene

Conditions
ConditionsYield
With sodium hydroxide at 10℃; for 30h;94.9%
2684-02-8

benzenediazonium

92-77-3

2,3-oxynaphthoic acid phenylamide

3789-75-1

1-phenylazo-2-hydroxy-3-phenylcarbamoylnaphthalene

2684-02-8

benzenediazonium

871874-72-5

2-hydroxy-3-phenylcarbamoyl-naphthalene-1-sulfonic acid

3789-75-1

1-phenylazo-2-hydroxy-3-phenylcarbamoylnaphthalene

Conditions
ConditionsYield
in alkal. Loesung;
92-77-3

2,3-oxynaphthoic acid phenylamide

3789-75-1

1-phenylazo-2-hydroxy-3-phenylcarbamoylnaphthalene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: nitrobenzene; chlorosulfonic acid / 50 - 60 °C
2: in alkal. Loesung
View Scheme
3789-75-1

1-phenylazo-2-hydroxy-3-phenylcarbamoylnaphthalene

74-88-4

methyl iodide

87407-75-8

N-methyl-1-phenylazo-2-methoxy-3-naphthanilide

Conditions
ConditionsYield
With sodium hydride In dimethyl sulfoxide at 40℃; for 38h;28.8%
3789-75-1

1-phenylazo-2-hydroxy-3-phenylcarbamoylnaphthalene

74-88-4

methyl iodide

83038-40-8

1-phenylazo-2-hydroxy-3-naphtho-N-methylanilide

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 40 - 42℃;
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