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Basic Information
| CAS No.: | 52846-75-0 |
|---|---|
| Name: | rac 4-(3-Aminobutyl)phenol |
| Article Data: | 5 |
| Molecular Structure: | |
|
|
|
| Formula: | C10H15NO |
| Molecular Weight: | 165.235 |
| Synonyms: | p-hydroxyhomoamphetamine;4-morpholin-4-ylbut-2-ylamine;4-morpholinobutan-2-amine;1-methyl-3-morpholino-propylamine; |
| PSA: | 46.25000 |
| LogP: | 2.37230 |
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Synthetic route
- 5471-51-2
4-(4-hydroxyphenyl)-2-oxobutane
- 52846-75-0
p-hydroxyhomoamphetamine
Conditions
| Conditions | Yield |
|---|---|
| With nickel(II) tetrafluoroborate hexahydrate; ammonia; hydrogen; bis(2-diphenylphosphinoethyl)phenylphosphine In 2,2,2-trifluoroethanol at 120℃; for 24h; chemoselective reaction; | 93% |
| With ammonia; hydrogen In tetrahydrofuran at 120℃; for 15h; | 89% |
| With palladium 10% on activated carbon; ammonium formate In methanol for 5h; |
- 51062-15-8
(+)-(R)-1-Methyl-3-(4-methoxyphenyl)-1-propylamine
- 52846-75-0
p-hydroxyhomoamphetamine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen bromide |
- 52846-75-0
p-hydroxyhomoamphetamine
Conditions
| Conditions | Yield |
|---|---|
| With sodium amalgam; acetic acid at 50 - 60℃; |
- 1222558-29-3
[((E)-4-(4-methoxyphenyl)but-3-en-2-ylidene)amino]hydroxide
- 52846-75-0
p-hydroxyhomoamphetamine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: H2 / PtO2 / methanol / 6 h / 60 °C / 15200 Torr 2: HBr View Scheme |
- 22214-30-8, 59417-71-9, 3160-35-8
4-(4'-hydroxyphenyl)but-3-en-2-one
- 52846-75-0
p-hydroxyhomoamphetamine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: palladium 10% on activated carbon; hydrogen / ethanol / 1 h / 20 °C / 1520.1 Torr 2: palladium 10% on activated carbon; ammonium formate / methanol / 5 h View Scheme |
- 123-08-0
4-hydroxy-benzaldehyde
- 52846-75-0
p-hydroxyhomoamphetamine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: sodium hydroxide / water / 2 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / ethanol / 1 h / 20 °C / 1520.1 Torr 3: palladium 10% on activated carbon; ammonium formate / methanol / 5 h View Scheme |
- 52846-75-0
p-hydroxyhomoamphetamine
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: C18H13NO4; p-hydroxyhomoamphetamine With sodium tetrahydroborate In methanol; dimethyl sulfoxide for 1h; Stage #2: With 5%-palladium/activated carbon; hydrogen In methanol for 1h; Stage #3: With hydrogenchloride In ethyl acetate for 2h; | 94% |
- 52846-75-0
p-hydroxyhomoamphetamine
- 108-24-7
acetic anhydride
A
- 1204483-45-3
N-[3-(4-hydroxyphenyl)-1-methylpropyl]acetamide
B
- 1204484-14-9
4-(3-acetylaminobutyl)phenyl acetate
Conditions
| Conditions | Yield |
|---|---|
| With triethylamine In ethyl acetate at 0℃; for 1h; | A 74% B 7% |
...Expand
- 79798-34-8
3-methyl-5-(2-oxiranylmethoxy-styryl)-isoxazole
- 52846-75-0
p-hydroxyhomoamphetamine
- 78351-27-6
4-[3-(2-Hydroxy-3-{2-[(E)-2-(3-methyl-isoxazol-5-yl)-vinyl]-phenoxy}-propylamino)-butyl]-phenol
Conditions
| Conditions | Yield |
|---|---|
| In ethanol 1.) reflux, 1 h, 2.) 25 deg C, overnight; | 30% |
- 52846-75-0
p-hydroxyhomoamphetamine
- 448-61-3
2,4,6-triphenylpyrylium tetrafluoroborate
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: p-hydroxyhomoamphetamine With acetic acid In dichloromethane at 20℃; Stage #2: 2,4,6-triphenylpyrylium tetrafluoroborate In dichloromethane at 20℃; for 6h; | 22% |
| In ethanol at 80 - 85℃; for 4h; |
Raw Materials
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