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5353-15-1

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Basic Information
CAS No.: 5353-15-1
Name: BENZENE,1,2,4-TRIMETHOXY-5-(2-PROPENYL)-
Article Data: 12
Molecular Structure:
Molecular Structure of 5353-15-1 (BENZENE,1,2,4-TRIMETHOXY-5-(2-PROPENYL)-)
Formula: C12H16O3
Molecular Weight: 208.257
Synonyms: 2,4,5-Trimethoxyallylbenzene;1-Allyl-2,4,5-trimethoxy-benzol;(2,4,5-trimethoxyphenyl)prop-1-ene;Benzene,1,2,4-trimethoxy-5-(2-propenyl);1,2,4-TRIMETHOXY-5-ALLYLBENZENE;1-allyl-2,4,5-trimethoxybenzene;
Density: 1.011g/cm3
Melting Point: 25 °C
Boiling Point: 287.7°Cat760mmHg
Flash Point: 95.4°C
PSA: 27.69000
LogP: 2.44090
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Synthetic route
135-77-3

1,2,4-trimethoxy-benzene

(η3-allyl)Fe(CO)4BF4

(η3-allyl)Fe(CO)4BF4

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
With carbon monoxide In nitromethane at 25℃; under 760 Torr; for 20h;87%
627-40-7

methylallylether

C9H11F3O5SSi

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
With cesium fluoride In tetrahydrofuran at 50℃; for 28h; Claisen Rearrangement; Inert atmosphere;60%
437761-99-4

2,4,5-trimethoxycinnamyltosylhydrazone

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
With sodium tetrahydroborate In acetic acid at 90 - 120℃; for 12h;43%

(1R*,2R*,3S*)-1,3-bis(2',4',5'-trimethoxyphenyl)-2-methylpent-4-en-1-ol

A

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

(+/-)-(2R,3R,4S,5S)-2-(bromomethyl)-4-methyl-1,3-bis(2',4',5'-trimethoxyphenyl)-tetrahydrofuran

Conditions
ConditionsYield
With Bromotrichloromethane; cyclohexa-1,4-diene; {4-[3,5-bis(trifluoromethyl)phenyl]-4-oxybut-3-en-2-one}-cobalt(II) In toluene at 60℃; for 11h; optical yield given as %de; diastereoselective reaction;A 36%
B 22%
67-56-1

methanol

93-15-2

1,2-dimethoxy-4-(2-propenyl)benzene

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
With toluene-4-sulfonic acid; sodium hydroxide; sodium perchlorate 1) electrolysis, 4.5h, 15 deg C 2) MeOH, 10 min, room temperature; Yield given. Multistep reaction;
With hydrogenchloride; sodium hydroxide; sodium perchlorate 1.) electrolyzed at room temp.; Yield given. Multistep reaction;
2033-89-8

3,4-dimethoxyphenol

106-95-6

allyl bromide

77-78-1

dimethyl sulfate

A

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

B

5353-16-2

2-allyl-1,3,4-trimethoxybenzene

Conditions
ConditionsYield
Multistep reaction;
...Expand
6906-64-5

1-(allyloxy)-3,5-dimethoxybenzene

74-88-4

methyl iodide

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
(i) (heating), (ii) KOH, EtOH, (iii) /BRN= 969135/; Multistep reaction;
5273-86-9

C12H16O3

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 62 percent / DDQ; silica gel / dioxane / 20 °C
2: 79 percent / methanol / 20 °C
3: 43 percent / NaBH4 / acetic acid; acetic acid / 12 h / 90 - 120 °C
View Scheme
99217-07-9, 106128-88-5, 99217-06-8

trans 2,4,5-trimethoxy cinnamaldehyde

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 79 percent / methanol / 20 °C
2: 43 percent / NaBH4 / acetic acid; acetic acid / 12 h / 90 - 120 °C
View Scheme
490-64-2

asaronic acid

106-95-6

allyl bromide

5353-15-1

1-allyl-2,4,5-trimethoxybenzene

Conditions
ConditionsYield
With copper(I) oxide; palladium diacetate; dimethyl sulfoxide; silver carbonate In toluene at 110℃; for 2h; chemoselective reaction;89 %Chromat.
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