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550-89-0

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Basic Information
CAS No.: 550-89-0
Name: phenazine-1-carboxamide
Article Data: 10
Molecular Structure:
Molecular Structure of 550-89-0 (phenazine-1-carboxamide)
Formula: C13H9N3O
Molecular Weight: 223.234
Synonyms: Phenazine-1-carboxamide;1-Carbamoyl-phenazin;α-Amidophenazin;phenazine-1-carboxylic acid amide;Phenazin-1-carbamid;
Density: 1.371g/cm3
Melting Point: 242oC
Boiling Point: 526.1°C at 760 mmHg
Flash Point: 272°C
Solubility: 0.01 g/100 g water(15oC)
Appearance: green-yellow solid
PSA: 68.87000
LogP: 2.58220
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Conditions
ConditionsYield
With thionyl chloride und anschliessend Behandeln mit konz.wss.NH3;
Multi-step reaction with 2 steps
1: concentrated H2SO4
2: concentrated aqueous NH3
View Scheme
Multi-step reaction with 2 steps
1: methanol / 20 °C / Darkness
2: ammonia / methanol / 20 °C
View Scheme
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Conditions
ConditionsYield
With ammonium hydroxide
With ammonia In methanol at 20℃;11.4 mg
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Conditions
ConditionsYield
at 200℃;
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Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: KOH / 145 - 160 °C
2: concentrated H2SO4
3: concentrated aqueous NH3
View Scheme
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Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: KOH / 145 - 160 °C
2: concentrated H2SO4
3: concentrated aqueous NH3
View Scheme
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Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: N-ethylmorpholine;; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere
2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere
4: ammonia / water; dichloromethane / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 4 steps
1: N-ethylmorpholine;; 2.3-butanediol; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere
2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere
4: ammonium hydroxide / water; dichloromethane / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1.1: copper(l) chloride; copper; N-ethylmorpholine; / 15 h / 70 °C
2.1: sodium hydroxide; sodium tetrahydroborate / 5 h / Reflux
3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16 h / 20 °C / Cooling with ice; Inert atmosphere
3.2: 0.5 h / 0 °C
View Scheme

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550-89-0

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Conditions
ConditionsYield
With ammonia In dichloromethane; water at 20℃; Inert atmosphere;100 mg
With ammonium hydroxide In dichloromethane; water at 20℃; Inert atmosphere;100 mg
With ammonia; triethylamine In dichloromethane at 0℃; Reflux;
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Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
2: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere
3: ammonia / water; dichloromethane / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
2: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere
3: ammonium hydroxide / water; dichloromethane / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: sodium hydroxide; sodium tetrahydroborate / 5 h / Reflux
2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16 h / 20 °C / Cooling with ice; Inert atmosphere
2.2: 0.5 h / 0 °C
View Scheme
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Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: N-ethylmorpholine;; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere
2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere
4: ammonia / water; dichloromethane / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 4 steps
1: N-ethylmorpholine;; 2.3-butanediol; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere
2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere
3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere
4: ammonium hydroxide / water; dichloromethane / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1.1: copper(l) chloride; copper; N-ethylmorpholine; / 15 h / 70 °C
2.1: sodium hydroxide; sodium tetrahydroborate / 5 h / Reflux
3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16 h / 20 °C / Cooling with ice; Inert atmosphere
3.2: 0.5 h / 0 °C
View Scheme
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Conditions
ConditionsYield
Stage #1: phenazine-1-carboxamide With bromine; sodium methylate In tetrahydrofuran; methanol at -78 - 55℃; for 75h;
Stage #2: With sodium hydroxide In methanol; water at 90℃; for 4h;		82%
With sodium hypobromide; water
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    Chemical Technology Co.,LTD is a professional enterprise which engaged in pharmaceutical intermediates, material intermediates production research and development.Company foc

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     China (Mainland)  |  Contact Details

    Business Type:Other

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  • Oxychloroaphine

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    Oxychloroaphine

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    Nanjing Raymon Biotech Co., Ltd. is specialized in developing and marketing middle & high level pharmaceutical intermediates. We are supplying different categories of high-quality

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     China (Mainland)  |  Contact Details

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    Shanghai PotentPharm Technology Co., Ltd is located in Pudong New District of Shanghai. As a high-tech medicine and chemical company, we commit ourselves to developing forefront ch

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    high quality;competitive price Storage:keep sealed and keep from direct light Package:Sample: 50g/ bottle 100g/ bottle 1000g/ bottle bulk: 25kg/drum 50kg/drum 202kg/drum Application:Scientific research Transportation:For small batches, they will

    Weihai MooChun Bio- Tech co., LTD., specializing in the production and supply of plant extracts, Chinese medicine extract oil, fluorine meticulous chemicals, committed to promoting

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • phenazine-1-carboxamide

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    phenazine-1-carboxamide

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    1, We supply best price with high quality 2,We could suppli different kinds of package as customer's request 3,Products could be sent by courier/air/sea 7918,We could do customized service Package:As requested Application:Pha

    Jiaxing Isen Chemical Co Ltd is a high-tech pharmaceutical and chemical company, dedicated to pharmaceutical raw materials, intermediates research and product development . Dependi

  • Jiaxing Isen Chemical Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0086-0573-85287218

    Address:Room 301, Unit 2, Building 3, Alley 94, East Renmin Road, Pinghu City, Zhejiang Province, China

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    Phenazine-1-carboxamide

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    Jiangxi Shengwei Chemical Technology Co., Ltd.supplies scientific research products as below:1.High-purity organic chemical reagents;2.Analytical reagents; 3.Biochemical reagents;4.Chemical raw materials;5.Experimental instruments;6.Experimental cons

    Jiangxi Shengwei Chemical Technology Co., Ltd.supplies scientific research products as below: 1.High-purity organic chemical reagents; 2.Analytical reagents; 3.Biochemical reagent

  • Jiangxi shengwei chemical technology co. LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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  • FT-0697117

  • Casno:

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    FT-0697117

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    Finetech Industry Limited is a company in England,which specializing in developing, manufacturing and marketing fine organic compounds and intermediates for the fine chemical and p

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-27-87465837

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  • 550-89-0

  • Casno:

    550-89-0

    550-89-0

    Min.Order: 0

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    Hebei Ruishun Trade Co.,Ltd registered capital one million, we have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center, we do

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    China (Mainland)  |  Contact Details

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  • Phenazine-1-carboxamide

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    Phenazine-1-carboxamide

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    SHANGHAI ZZBIO CO. LTD. is a high-tech enterprise involved in oligosaccharides & polysaccharides, PEG & PEGylation and phytochemicals for customers in pharmaceutical industry, food

  • SHANGHAI ZZBIO CO., LTD.

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-21-68404353-215

    Address:Rm 710, 30 BLDG, 2419 Hu Nan RD., Pudong New Area, Shanghai, China

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    Phenazine-1-carboxyamide

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    Phenazine-1-carboxyamideAppearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect th

  • Chemical Co.Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • Oxychloroaphine

  • Casno:

    550-89-0

    Oxychloroaphine

    Min.Order: 0

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  • NovaChemistry

    United Kingdom  |  Contact Details

    Business Type:Trading Company

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