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| CAS No.: | 58479-61-1 |
|---|---|
| Name: | tert-Butylchlorodiphenylsilane |
| Article Data: | 18 |
| Molecular Structure: | |
|
|
|
| Formula: | C16H19ClSi |
| Molecular Weight: | 274.865 |
| Synonyms: | Benzene,1,1'-[chloro(1,1-dimethylethyl)silylene]bis-;Silane,chloro(1,1-dimethylethyl)diphenyl- (9CI);(1,1-Dimethylethyl)diphenylsilylchloride;(Chloro)(tert-butyl)diphenylsilane;Chloro(1,1-dimethylethyl)diphenylsilane;Chlorodiphenyl-tert-butylsilane;Diphenyl-tert-butylsilyl chloride;Silane, chloro(1,1-dimethylethyl)diphenyl-; |
| EINECS: | 261-282-0 |
| Density: | 1.04 g/cm3 |
| Boiling Point: | 334.4 °C at 760 mmHg |
| Flash Point: | 143.3 °C |
| Solubility: | reacts in water |
| Appearance: | Colorless-light yellow to brown liquid |
| Hazard Symbols: |
 Xi,  C
|
| Risk Codes: | 14-34-37-29-20/21/22 |
| Safety: | 26-36/37/39-45-8 |
| Transport Information: | UN 2987 8/PG 2 |
| PSA: | 0.00000 |
| LogP: | 3.78520 |
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| Conditions | Yield |
|---|---|
| In hexane for 4h; Reflux; | 92% |
| In pentane for 12h; | 65% |
- 507-20-0
tertiary butyl chloride
- 80-10-4
diphenylsilyl dichloride
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| Stage #1: tertiary butyl chloride With magnesium In tetrahydrofuran at 60℃; for 2h; Stage #2: With lithium chloride; copper(I) bromide In tetrahydrofuran at 20℃; for 1h; Stage #3: diphenylsilyl dichloride In tetrahydrofuran at 50℃; for 6h; Reagent/catalyst; Temperature; | 87% |
| With copper(l) cyanide; magnesium In tetrahydrofuran for 5h; Heating; | 80% |
| With magnesium In tetrahydrofuran; hexane | 75% |
- 76358-47-9
tert-butyl(methoxy)diphenylsilane
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| With iron(III) chloride; acetyl chloride In 1,2-dichloro-ethane for 72h; | 86% |
| With hydrogenchloride In water |
- 80-10-4
diphenylsilyl dichloride
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| copper (II) acetylacetonate | 85% |
- 93547-88-7
t-butyl diphenylsilanol
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| With thionyl chloride In chloroform for 0.5h; | 81% |
- 6328-61-6
trimethylsilyldiphenylmethane
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| With SO2Cl2 In not given | 74% |
| With SO2Cl2 In not given | 74% |
- 33729-92-9
tert-butyldiphenylsilane
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| With iron(III) chloride; acetyl chloride In dichloromethane for 24h; | 69% |
| With sulfuryl dichloride | |
| With dichloromethane; eosin y at 20℃; for 24h; Reagent/catalyst; Sealed tube; Inert atmosphere; Irradiation; Green chemistry; | 99 %Spectr. |
- 98-59-9
p-toluenesulfonyl chloride
- 158262-82-9
(1S,3S,5R,6S)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-bicyclo[3.1.0]hexan-3-ol
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| With pyridine; dmap In dichloromethane for 24h; Ambient temperature; | 67% |
- 17887-41-1
phenyl-tert-butyldichlorosilane
- 591-51-5
phenyllithium
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| Inert atmosphere; |
- 58479-61-1
tert-butylchlorodiphenylsilane
| Conditions | Yield |
|---|---|
| With hydrogenchloride In water |
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Chemistry
The molecular structure of Tert-Butyldiphenylchlorosilane (CAS NO.58479-61-1):
Formula: C16H19ClSi
Molecular Weight: 274.84
EINECS: 261-282-0
Density: 1.057 g/mL at 25 °C(lit.)
Boiling Point: 90°C [at 0.01mmHg]
Refractive Index: 1.568
Flash Point: 115°C
Storage temp: Store at 5°C
Water Solubility: reacts
Sensitive: Moisture Sensitive
Appearance is Colorless-light yellow to brown liquid.
IUPAC Name: tert-butyl-chloro-diphenylsilane
Synonyms: EINECS 261-282-0 ; Benzene, 1,1'-(chloro(1,1-dimethylethyl)silylene)bis- ; Silane, chloro(1,1-dimethylethyl)diphenyl- ; tert-Butylchlorodiphenylsilane
Product Categories: FINE Chemical & INTERMEDIATES;Biochemistry;Monochlorosilanes;Nucleosides, Nucleotides & Related Reagents;Protecting Agents for Hydroxyl and Amino Groups;Protecting Agents, Phosphorylating Agents & Condensing Agents;Protection & Derivatization Reagents (for Synthesis);Reagents for Oligosaccharide Synthesis;Si (Classes of Silicon Compounds);Si-Cl Compounds;Silicon Compounds (for Synthesis);Synthetic Organic Chemistry;Blocking Agents;Phenyl Silanes;Protective Agents;Silylating Agents
Uses
Tert-Butyldiphenylchlorosilane (CAS NO.58479-61-1) can be used as pharmaceutical intermediates and used in organic synthesis .
Safety Profile
Hazard Codes: 
C
Xi
Risk Statements: 14-34-37-29-20/21/22
R14: Reacts violently with water
R34: Causes burns
R37: Irritating to the respiratory system
R29: Contact with water liberates toxic gas
R20/21/22 :Harmful by inhalation, in contact with skin and if swallowed
Safety Statements: 26-36/37/39-45-8
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
S8: Keep container dry
RIDADR: UN 2987 8/PG 2
WGK Germany: 3