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589-87-7

Basic Information
CAS No.: 589-87-7
Name: Benzene,1-bromo-4-iodo-
Article Data: 159
Cas Database
Molecular Structure:
Molecular Structure of 589-87-7 (Benzene,1-bromo-4-iodo-)
Formula: C6H4BrI
Molecular Weight: 282.906
Synonyms: 4-Bromo-1-iodobenzene;4-Bromoiodobenzene;4-Bromophenyl iodide;4-Iodo-1-bromobenzene;4-Iodobromobenzene;NSC 8033;p-Bromoiodobenzene;p-Bromophenyl iodide;p-Iodobromobenzene;
EINECS: 209-662-7
Density: 2.215 g/cm3
Melting Point: 89-91 °C(lit.)
Boiling Point: 244.8 °C at 760 mmHg
Flash Point: 101.9 °C
Solubility: Insoluble in water.
Appearance: white to brown cryst. powder, crystals or needles
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36-37/39
Transport Information: N/A
PSA: 0.00000
LogP: 3.05370
Synthetic route
106-40-1

4-bromo-aniline

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
Stage #1: 4-bromo-aniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 0.5h; Inert atmosphere;
Stage #2: With potassium iodide In ethyl acetate for 0.5h;
100%
With sulfuric acid; potassium iodide; sodium nitrite In water at -5 - 60℃; Inert atmosphere;92%
Stage #1: 4-bromo-aniline With sulfuric acid; silica gel; sodium nitrite at 20℃; grinding; Neat (no solvent);
Stage #2: With water at 20℃; grinding; Neat (no solvent);
Stage #3: With potassium iodide at 20℃; for 0.166667h; Sandmeyer reaction; grinding; Neat (no solvent);
87%

4-bromophenyldiazonium nitrate

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
With potassium iodide for 24h;100%
673-40-5

4-bromobenzenediazonium tetrafluoroborate

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
With potassium iodide In water at 25℃; for 0.0833333h; Solvent; Sandmeyer Reaction;99%
With diiodomethane; tetrabutylammonium perchlorate In methanol; N,N-dimethyl-formamide at 20℃; for 3h; Sandmeyer Reaction; Electrochemical reaction;61%
With iodine; potassium iodide In dimethyl sulfoxide at 15℃;

triethyl(4-iodophenyl)germane

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 4h;96%
23268-74-8

(4-bromophenyl)triethylgermane

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
With N-iodo-succinimide In N,N-dimethyl-formamide at 50℃; for 4h;96%
1514-50-7

4-iodobenzenediazonium tetrafluoroborate

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
With potassium bromide In acetonitrile at 20℃; for 1h; Sandmeyer Reaction; Inert atmosphere;95%
With N-Bromosuccinimide; tetrabutylammonium perchlorate In methanol; N,N-dimethyl-formamide at 20℃; for 3h; Sandmeyer Reaction; Electrochemical reaction;68%
With (triphenylphosphine)gold(I) chloride; sodium bromide In acetonitrile at 50℃; for 5h; Sandmeyer Reaction;73 %Chromat.
52010-62-5

1-(4-Bromophenyl)-3,3-diethyltriazene

74-88-4

methyl iodide

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
at 110 - 120℃; for 6h;94%
5467-74-3

4-Bromophenylboronic acid

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
With sodium nitrite In acetonitrile at 80℃; for 1.5h; Sealed tube;94%
With N-iodo-succinimide In acetonitrile at 81℃; for 6h;88%
With potassium fluoride; iodine In 1,4-dioxane at 80℃; for 1h;86%
374564-35-9

potassium 4-bromophenyltrifluoroborate

589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
With caesium tribromide In water; N,N-dimethyl-formamide at 80℃; for 5h; chemoselective reaction;94%
With chloroamine-T; sodium iodide In tetrahydrofuran; water at 20℃; for 0.25h;87%
100-64-1

Cyclohexanone oxime

41018-52-4

(4-bromophenyl)-λ3-iodanediyl diacetate

A

589-87-7

1,4-bromoiodobenzene

B

10259-08-2

acetoxy-1 nitroso-1 cyclohexane

Conditions
ConditionsYield
In acetic acid at -15℃; for 0.25h;A n/a
B 94%
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Chemistry

Empirical Formula: C6H4BrI 
Molecular Weight: 282.9044 g/mol
EINECS: 209-662-7 
Index of Refraction: 1.654
Density: 2.215 g/cm3
Flash Point: 101.9 °C
Melting point: 89-91 °C(lit.)
Sensitive: Light Sensitive
Enthalpy of Vaporization: 46.24 kJ/mol
Boiling Point: 244.8 °C at 760 mmHg
Vapour Pressure: 0.0464 mmHg at 25 °C
Appearance: white to brown cryst. powder, crystals or needles
Structure of 1-Bromo-4-iodobenzene (CAS NO.589-87-7):
                       
Product Category of 1-Bromo-4-iodobenzene (CAS NO.589-87-7): Miscellaneous;Benzene derivates;Bromine and Iodine Compounds;Aryl;Halogenated Hydrocarbons;Halogenated benzene series

Uses

 1-Bromo-4-iodobenzene (CAS NO.589-87-7) can be used in organic synthesis.

Toxicity Data With Reference

 1-Bromo-4-iodobenzene (CAS NO.589-87-7) hasn't been listed as a carcinogen by NTP, IARC, ACGIH, or CA Prop 65. And the toxicological properties have not been fully investigated.

Safety Profile

Hazard Codes:  Xi
Risk Statements:
R36/37/38:  Irritating to eyes, respiratory system and skin 
Safety Statements:
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36:  Wear suitable protective clothing 
S37/39:  Wear suitable gloves and eye/face protection 

Specification

 1-Bromo-4-iodobenzene , its cas register number is 589-87-7. It also can be called p-Bromoiodobenzene ; Benzene, 1-bromo-4-iodo- ; and p-Bromophenyl iodide . It is hazardous, so the first aid measures and others should be known. Such as: When on the skin: first, should flush skin with plenty of water immediately for at least 15 minutes while removing contaminated clothing. Secondly, get medical aid. Or in the eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Then get medical aid soon. While, it's inhaled: Remove from exposure and move to fresh air immediately. Give artificial respiration while not breathing. When breathing is difficult, give oxygen. And as soon as to get medical aid. Then you have the ingesting of the product: Wash mouth out with water, and get medical aid immediately. Notes to physician: Treat supportively and symptomatically.
In addition, 1-Bromo-4-iodobenzene (CAS NO.589-87-7) could be stable under normal temperatures and pressures. It is not compatible with strong oxidizing agents, and you must not take it with incompatible materials, light. And also prevent it to broken down into hazardous decomposition products: carbon monoxide, carbon dioxide, hydrogen bromide, hydrogen iodide.