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CAS No.: | 60037-58-3 |
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Name: | Z-13-OCTADECEN-1-YL ACETATE |
Article Data: | 3 |
Molecular Structure: | |
Formula: | C20H38 O2 |
Molecular Weight: | 310.521 |
Synonyms: | 13-Octadecen-1-ol,acetate, (13Z)- (9CI); 13-Octadecen-1-ol, acetate, (Z)-; (Z)-13-Octadecen-1-olacetate; (Z)-13-Octadecenyl acetate |
Density: | 0.872g/cm3 |
Boiling Point: | 379.5oC at 760 mmHg |
Flash Point: | 87.8oC |
PSA: | 26.30000 |
LogP: | 6.58700 |
Conditions | Yield |
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With pyridine for 24h; Ambient temperature; | 100% |
With pyridine at 0℃; for 3h; | 96% |
With pyridine In dichloromethane for 5h; Ambient temperature; | 86% |
cis-13-docosenoic acid
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
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Multi-step reaction with 6 steps 1: 91 percent / 30percent H2O2, HCOOH 2: 89 percent / aq. Na2CO3, H3PO4, NaIO4 3: 1.) NaH, DMSO 4: PTS 5: 90 percent / LiAlH4 (LAH) / diethyl ether 6: 100 percent / pyridine / 24 h / Ambient temperature View Scheme |
13,14-dihydroxy-behenic acid
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 89 percent / aq. Na2CO3, H3PO4, NaIO4 2: 1.) NaH, DMSO 3: PTS 4: 90 percent / LiAlH4 (LAH) / diethyl ether 5: 100 percent / pyridine / 24 h / Ambient temperature View Scheme |
13-oxotridecanoic acid
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1.) NaH, DMSO 2: PTS 3: 90 percent / LiAlH4 (LAH) / diethyl ether 4: 100 percent / pyridine / 24 h / Ambient temperature View Scheme |
(13Z)-octadec-13-enoic acid
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: PTS 2: 90 percent / LiAlH4 (LAH) / diethyl ether 3: 100 percent / pyridine / 24 h / Ambient temperature View Scheme |
cis-13-octadecenoic acid, methyl ester
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / LiAlH4 (LAH) / diethyl ether 2: 100 percent / pyridine / 24 h / Ambient temperature View Scheme |
4-(Z)-nonenemagnesium bromide
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 54 percent / Li2CuCl4 / tetrahydrofuran / 3 h / -10 °C 2: 53 percent / pyridinium p-toluenesulfonate / methanol / 6 h / 55 °C 3: 86 percent / pyridine / CH2Cl2 / 5 h / Ambient temperature View Scheme |
1-tetrahydropyranyloxy-13-(Z)-octadecene
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
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Multi-step reaction with 2 steps 1: 53 percent / pyridinium p-toluenesulfonate / methanol / 6 h / 55 °C 2: 86 percent / pyridine / CH2Cl2 / 5 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: pyridinium p-toluenesulfonate / ethanol / 80 °C 2: pyridine / 3 h / 0 °C View Scheme |
(Z)-1-(tetrahydropyran-2-yloxy)-4-nonene
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: pyridinium p-toluenesulfonate / methanol / 80 °C 2: pyridine 3: dilithium tetrachlorocuprate; magnesium / tetrahydrofuran 4: pyridinium p-toluenesulfonate / ethanol / 80 °C 5: pyridine / 3 h / 0 °C View Scheme |
(Z)-4-nonen-1-ol
(Z)-13-octadecen-1-yl acetate
Conditions | Yield |
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Multi-step reaction with 4 steps 1: pyridine 2: dilithium tetrachlorocuprate; magnesium / tetrahydrofuran 3: pyridinium p-toluenesulfonate / ethanol / 80 °C 4: pyridine / 3 h / 0 °C View Scheme |