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Basic Information
| CAS No.: | 6084-58-8 | ||||
|---|---|---|---|---|---|
| Name: | O-ISOBUTYLHYDROXYLAMINE HYDROCHLORIDE | ||||
| Article Data: | 8 | ||||
| Molecular Structure: | |||||
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| Formula: | C4H12ClNO | ||||
| Molecular Weight: | 125.598 | ||||
| Synonyms: | O-ISOBUTYLHYDROXYLAMINE HYDROCHLORIDE;ISOBUTYLOXYAMINE HYDROCHLORIDE;Isobutylhydroxylaminehydrochloride;o-isobutylhydroxylamineHCl | ||||
| Melting Point: | 129°C | ||||
| Boiling Point: | 167.7°C at 760 mmHg | ||||
| Flash Point: | 55.2°C | ||||
| Risk Codes: | 36/37/38 | ||||
| Safety: |
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| PSA: | 35.25000 | ||||
| LogP: | 2.03500 | ||||
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Synthetic route
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- 6084-58-8
O-isobutylhydroxylamine hydrochloride
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: O-1-(2-methyl)propyl-N-hydroxyphthalimide With methylhydrazine In dichloromethane at 0 - 20℃; for 2h; Stage #2: With hydrogenchloride In 1,4-dioxane at 0℃; | 99% |
| With hydrazine In ethanol; water for 2h; hydrazinolysis; Heating; | 31.9% |
| With methylhydrazine In dichloromethane | |
| Stage #1: O-1-(2-methyl)propyl-N-hydroxyphthalimide With hydrazine hydrate In dichloromethane Inert atmosphere; Stage #2: With hydrogenchloride In 1,4-dioxane Inert atmosphere; |
- 6084-58-8
O-isobutylhydroxylamine hydrochloride
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethanol; water at 65℃; | 61.8% |
| With hydrogenchloride In ethanol; water at 65℃; | 61.8% |
- 6084-58-8
O-isobutylhydroxylamine hydrochloride
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: C13H15NO2 With hydrazine hydrate In tetrahydrofuran at 20℃; for 12h; Stage #2: With hydrogenchloride In 1,4-dioxane at 20℃; for 0.0833333h; | 53% |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethanol at 0 - 5℃; for 72h; |
Conditions
| Conditions | Yield |
|---|---|
| In ethanol at 20℃; Inert atmosphere; | 99% |
- 853579-43-8
2,7-bis(N'-ethoxycarbonylthiourea)-9H-fluorene
- 6084-58-8
O-isobutylhydroxylamine hydrochloride
- 853579-28-9
2,7-bis(N'-ethoxycarbonyl-N''-isobutoxy)guanidino-9H-fluorene
Conditions
| Conditions | Yield |
|---|---|
| With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In 1,4-dioxane; dichloromethane at 20℃; | 93% |
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- 6084-58-8
O-isobutylhydroxylamine hydrochloride
- 851181-35-6
3-(2-methyl-propyl)oxyimino-2-(4-hydroxy-benzyl)-butyric acid methyl ester
Conditions
| Conditions | Yield |
|---|---|
| With sodium acetate In methanol | 90% |
| With triethylamine In ethanol at 45℃; for 24h; | 80% |
- 924650-01-1
methyl 3-acetyl-5-(dipropylcarbamoyl)-benzoate
- 6084-58-8
O-isobutylhydroxylamine hydrochloride
- 1163142-89-9
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Conditions
| Conditions | Yield |
|---|---|
| In ethanol at 80℃; | 85% |
- 6084-58-8
O-isobutylhydroxylamine hydrochloride
- 501-53-1
benzyl chloroformate
- 1174758-23-6
benzyl N-(isobutyloxy)carbamate
Conditions
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 84% |
- 1446092-98-3
C31H44O7
- 6084-58-8
O-isobutylhydroxylamine hydrochloride
Conditions
| Conditions | Yield |
|---|---|
| With pyridine for 3h; Reflux; | 84% |
