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Basic Information
| CAS No.: | 612548-45-5 |
|---|---|
| Name: | Perindopril L-Arginine |
| Molecular Structure: | |
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| Formula: | C25H46N6O7 |
| Molecular Weight: | 542.676 |
| Synonyms: | Perindopril L-Arginine;L-Arginine mono[(2S,3aS,7aS)-1-[(2S)-2-[[(1S)-1-(ethoxycarbonyl)butyl]amino]-1-oxopropyl]octahydro-1H-indole-2-carboxylate] |
| PSA: | 221.16000 |
| LogP: | 2.82220 |
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Synthetic route
- 74-79-3
L-arginine
- 80875-98-5
(2S,3aS,7aS)-perhydroindole-2-carboxylic acid
- 612548-45-5
perindopril L-arginine
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: N-(1-(S)-Ethoxycarbonylbutyl)-L-alanine; (2S,3aS,7aS)-perhydroindole-2-carboxylic acid With triethylamine In acetonitrile at 10℃; for 5h; Stage #2: L-arginine In dimethyl sulfoxide at 50℃; for 5h; Reagent/catalyst; Temperature; Time; Concentration; Solvent; | 89% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With methanesulfonic acid In dimethyl sulfoxide at 70℃; for 1h; | 88% |
Conditions
| Conditions | Yield |
|---|---|
| In dimethyl sulfoxide; acetonitrile at 50℃; | 79% |
| In water at 20℃; | |
| In ethanol; dichloromethane at 70 - 75℃; | |
| In ethanol; dichloromethane at 45 - 75℃; | |
| In methanol at 20℃; Product distribution / selectivity; Reflux; |
Conditions
| Conditions | Yield |
|---|---|
| With water; 6-chloro-3,4-dihydro-2H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide at 59.84℃; for 250h; Kinetics; |
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Perindopril L-Arginine
