Products Categories
Basic Information
| CAS No.: | 62595-74-8 |
|---|---|
| Name: | 3-broMopiperidine-2,6-dione |
| Article Data: | 14 |
| Molecular Structure: | |
|
|
|
| Formula: | C5H6BrNO2 |
| Molecular Weight: | 192.012 |
| Synonyms: | 3-bromopiperidine-2,5-dione;2,6-Piperidinedione,3-bromo;3-bromo-glutarimide;3-Bromglutarimid;3-bromo-piperidine-2,6-dione; |
| Density: | 1.748g/cm3 |
| Melting Point: | 107 °C(Solv: chloroform (67-66-3)) |
| Boiling Point: | 336.42oC at 760 mmHg |
| Flash Point: | 157.261oC |
| PSA: | 49.66000 |
| LogP: | 0.46240 |
Related products
- 81281-59-67-Benzylideneaminotheophylline
- 82993-81-5D-threo-Ritalinic acid hydrochloride
- 73441-42-6METHYL-5-CHLORO-2,2-DIMETHYLVALERATE
- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 958254-66-51H-Imidazo[4,5-b]pyridine-2-carboxaldehyde, 1-methyl-, hydrochloride
- 99170-93-1N-Methyl-2-oxazolamine
- 717878-06-31-(4-fluorophenyl)-4-nitro-1H-imidazole
- 914458-26-7[5-(2-fluorophenyl)-1-pentyl-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone
- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
Synthetic route
- 1121-89-7
piperidine-2,6-dione
- 62595-74-8
3-bromopiperidine-2,6-dione
Conditions
| Conditions | Yield |
|---|---|
| With bromine In chloroform at 110℃; for 1.5h; | 99% |
| With bromine In chloroform at 20 - 110℃; for 1.5h; Inert atmosphere; Sealed tube; | 55% |
| With bromine In chloroform at 113℃; for 1.5h; Sealed tube; | 54.5% |
- 62595-74-8
3-bromopiperidine-2,6-dione
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) iodide; potassium carbonate In tetrahydrofuran at 60℃; for 6h; Reagent/catalyst; Solvent; Temperature; | 90.4% |
| In N,N-dimethyl-formamide at 100℃; for 20h; Solvent; Temperature; | 73.1% |
- 62595-74-8
3-bromopiperidine-2,6-dione
- 68621-88-5
(3-aminophenyl)carbamic acid tert-butyl ester
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydrogencarbonate In N,N-dimethyl-formamide at 80℃; for 16h; | 84.2% |
| In N,N-dimethyl-formamide at 80℃; for 12h; |
- 62595-74-8
3-bromopiperidine-2,6-dione
- 103-67-3
benzyl-methyl-amine
Conditions
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 20℃; for 16h; | 83% |
| In tetrahydrofuran at 72℃; for 16h; |
- 109-01-3
1-methyl-piperazine
- 62595-74-8
3-bromopiperidine-2,6-dione
Conditions
| Conditions | Yield |
|---|---|
| at 20℃; for 2h; | 82% |
- 62595-74-8
3-bromopiperidine-2,6-dione
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide In water; acetone at 20℃; for 24h; Inert atmosphere; | 80% |
| With sodium azide In acetone at 20℃; for 48h; | 1.44g |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: C25H26F2N4O3 With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.25h; Stage #2: 3-bromopiperidine-2,6-dione In tetrahydrofuran; mineral oil for 1h; | 78.41% |
- 7747-10-6
2-Phenyl-4,5,6,7-tetrahydro-4,7-dithia-1,3-indandion
- 62595-74-8
3-bromopiperidine-2,6-dione
- 76059-14-8
3-<2-(1,3-Dioxo-2-phenyl-4,5,6,7-tetrahydro-4,7-dithiaindanyl)>glutarimid
Conditions
| Conditions | Yield |
|---|---|
| With sodium 1.) EtOH, 2.) THF, reflux, 1 h; | 78% |
- 62595-74-8
3-bromopiperidine-2,6-dione
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: C27H30N4O3 With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.25h; Stage #2: 3-bromopiperidine-2,6-dione In tetrahydrofuran; mineral oil | 75.67% |
- 62595-74-8
3-bromopiperidine-2,6-dione
- 1745-07-9
6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
Conditions
| Conditions | Yield |
|---|---|
| at 20℃; for 18h; | 75% |
