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67952-60-7

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Basic Information
CAS No.: 67952-60-7
Name: 2-(METHYLDITHIO)-ISOBUTYRALDEHYDE
Molecular Structure:
Molecular Structure of 67952-60-7 (2-(METHYLDITHIO)-ISOBUTYRALDEHYDE)
Formula: C5H10 O S2
Molecular Weight: 150.266
Synonyms: EINECS 267-914-1;2-Methyl-2-methyldithio-propanal;
Density: 1.101g/cm3
Boiling Point: 184.2°Cat760mmHg
Flash Point: 61.7°C
PSA: 67.67000
LogP: 1.97510
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ConditionsYield
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Conditions
ConditionsYield
Stage #1: 2-methyl-2-(methyldithio)propionaldehyde; methylamine In ethanol at 20℃; for 4h;
Stage #2: With sodium tetrahydroborate; ethanol at 0℃;		65%
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Conditions
ConditionsYield
Stage #1: 2-methyl-2-(methyldithio)propionaldehyde; (3-amino-5-hydroxymethylphenyl)methanol In ethanol at 20℃; for 3h;
Stage #2: With sodium tetrahydroborate In ethanol at 0℃; for 1h;		65%
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Conditions
ConditionsYield
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2,2'-carbonylbis(4,5,6,7-tetrahydro-7,8,8-trimethyl-4,7-methano-indazole)

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2-[bis(4,5,6,7-tetrahydro-7,8,8-trimethyl-4,7-methano-2-indazolyl)methyl](1-methyl-1-sulfanylethyl)methane

Conditions
ConditionsYield
With pyridine at 80℃; for 15h; Peterson reaction;48%
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2-methyl-2-(methyldithio)propionaldehyde

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Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 48h;43%
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Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; magnesium sulfate; zinc(II) chloride In 1,2-dichloro-ethane at 20℃; for 25h;40%
67952-60-7

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(5-(2-(2-(2-methoxyethoxy)ethoxy)ethylamino)-1,3-phenylene)dimethanol

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Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; magnesium sulfate; zinc(II) chloride In 1,2-dichloro-ethane at 20℃; for 23h;22%
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Conditions
ConditionsYield
With pyridine In tetrahydrofuran for 16h; Reflux;4.49 g
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    Supply top quality products with a reasonable price Application:api

    Hebei Ruishun Trade Co.,Ltd registered capital one million, we have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center, we do

  • Hebei Ruishun Trade Co.,Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-311-68037669

    Address:WanDa commerce building ,yuhua district

       Inquiry Now

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