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CAS No.: | 6979-97-1 | |||
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Name: | 3',5'-DIACETYLTHYMIDINE | |||
Article Data: | 54 | |||
Molecular Structure: | ||||
Formula: | C14H18 N2 O7 | |||
Molecular Weight: | 326.306 | |||
Synonyms: | 3',5'-Di-O-acetylthymidine;3',5'-Diacetyl-5-methyl-2'-deoxyuridine; 3',5'-Diacetylthymidine;Di-O-acetylthymidine; NSC 526766; NSC 67672 | |||
EINECS: | 230-244-5 | |||
Density: | 1.37 g/cm3 | |||
Melting Point: | 126 - 128 C | |||
Boiling Point: | 463.51°C (rough estimate) | |||
Solubility: | soluble | white crystalline powder | ||
Hazard Symbols: | Not regulated UN NO. | |||
Transport Information: | OTH | |||
PSA: | 116.69000 | |||
LogP: | -0.37270 |
Conditions | Yield |
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With pyridine |
Conditions | Yield |
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With protease N In aq. phosphate buffer; acetonitrile at 20℃; for 24h; Reagent/catalyst; Enzymatic reaction; | A 6% B 74% |
3',5'-Diacetylthymidine
1-(2-Deoxy-3,5-di-O-acetyl-β-D-ribofuranosyl)-4-chloro-5-methyl-2(1H)-pyrimidinone
Conditions | Yield |
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With thionyl chloride In chloroform; N,N-dimethyl-formamide for 1.5h; Heating; | 160 mg |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 160 mg / SOCl2 / CHCl3; dimethylformamide / 1.5 h / Heating 2: 0.5N NaOH / H2O / 1 h / 40 °C 3: NH3 / methanol / 36 h / 50 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 160 mg / SOCl2 / CHCl3; dimethylformamide / 1.5 h / Heating 2: 0.5N NaOH / H2O / 1 h / 40 °C View Scheme |
3',5'-Diacetylthymidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 160 mg / SOCl2 / CHCl3; dimethylformamide / 1.5 h / Heating 2: 0.25 h / Heating View Scheme |