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Basic Information
| CAS No.: | 710-24-7 |
|---|---|
| Name: | P-ACETAMIDOBENZENESULFINIC ACID |
| Molecular Structure: | |
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| Formula: | C8H9NO3S |
| Molecular Weight: | 199.23 |
| Synonyms: | 4-ACETAMIDOBENZENESULPHINIC ACID;P-ACETYLAMINOBENZENESULFINIC ACID;P-ACETYLAMINOPHENYLSULFINIC ACID;P-ACETAMIDOBENZENESULFINIC ACID;P-ACETAMIDOPHENYLSULFINIC ACID;P-ACETAMINO BENZENE SULFINIC ACID;4-acetamidobenzenesulfinic acid |
| Density: | 1.46±0.1 g/cm3(Predicted) |
| Melting Point: | 152-154 °C (decomp) |
| PSA: | 89.10000 |
| LogP: | 2.74080 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; aluminium(III) triflate; sulfur dioxide In ethanol at 0℃; under 7600.51 Torr; for 50h; Pressure; Temperature; | 94% |
| With sulfur dioxide at 90℃; for 1h; Reagent/catalyst; Temperature; Inert atmosphere; | 94.07% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydrogencarbonate; sodium sulfite In water at 70 - 80℃; for 1h; Reduction; | 72% |
| With triethylamine; para-thiocresol In dichloromethane at -76℃; for 0.25h; | 64% |
| With sodium sulfite |
- 18522-22-0
o-nitrophenyl N-acetylthiosulfanilate
- 77505-27-2
N,N'-diethyl-N,N'-diphenylmethionamide
A
- 710-24-7
4-acetamidobenzenesulfinic acid
Conditions
| Conditions | Yield |
|---|---|
| With potassium 1) toluene, 2) 70 deg C, 10 h, boiling water bath, 1 h; Yield given. Multistep reaction; | A n/a B 49% |
| With potassium 1) toluene, 2) 70 deg C, 10 h, boiling water bath, 1 h; Yield given. Multistep reaction; | A 48% B n/a |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide |
- 87015-43-8
acetic acid-[4-(3-oxo-3-phenyl-propane-1-sulfonyl)-anilide]
A
- 710-24-7
4-acetamidobenzenesulfinic acid
B
- 768-03-6
Phenyl vinyl ketone
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In acetone at 20℃; Rate constant; Equilibrium constant; | |
| With potassium dihydrogenphosphate; acetaldehyde; citric acid; NADH; aldehyde dehydrogenase In water at 20℃; Rate constant; |
- 87015-50-7
acetic acid-[4-(2-nitro-1-phenyl-ethanesulfonyl)-anilide]
A
- 102-96-5
(2-nitroethenyl)benzene
B
- 710-24-7
4-acetamidobenzenesulfinic acid
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In acetone at 20℃; Rate constant; Equilibrium constant; |
Conditions
| Conditions | Yield |
|---|---|
| In methanol at 20℃; for 12h; Green chemistry; | 97% |
Conditions
| Conditions | Yield |
|---|---|
| With photoredox catalyst Ni/TiO2 In acetonitrile at 20℃; for 12h; Molecular sieve; Irradiation; | 90% |
- 67082-95-5
3-(3-phenylpropyl-2-yn-1-ylidene)-2,4-pentanedione
- 710-24-7
4-acetamidobenzenesulfinic acid
Conditions
| Conditions | Yield |
|---|---|
| With air In water at 80℃; for 3h; | 82% |
Conditions
| Conditions | Yield |
|---|---|
| In ethanol for 24h; | 80% |
