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Basic Information
CAS No.: 72299-67-3
Name: 6-AMINO-1,2,3,4-TETRAHYDRO-ISOQUINOLINE
Molecular Structure:
Molecular Structure of 72299-67-3 (6-AMINO-1,2,3,4-TETRAHYDRO-ISOQUINOLINE)
Formula: C9H12 N2
Molecular Weight: 148.208
Synonyms: 6-AMINO-1,2,3,4-TETRAHYDRO-ISOQUINOLINE;1,2,3,4-TETRAHYDROISOQUINOLIN-6-AMINE;1,2,3,4-TETRAHYDRO-ISOQUINOLIN-6-YLAMINE
Density: 1.101g/cm3
Boiling Point: 315.903°C at 760 mmHg
Flash Point: 169.23°C
PSA: 38.05000
LogP: 1.82450
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Synthetic route

1,2,3,4-tetrahydroisoquinolin-6-amine dihydrobromide

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Conditions
ConditionsYield
With sodium hydroxide In water100%
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6-isoquinolinamine

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1,2,3,4-tetrahydroisoquinolin-6-amine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen; acetic acid In ethanol; water Flow reactor; Heating;99%
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6-amino-3,4-dihydro-isoquinoline-1(2H)-one

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1,2,3,4-tetrahydroisoquinolin-6-amine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 72h; Reduction; Heating;0.6 g
23687-26-5

6-isoquinolinamine

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tert-butyl 6-amino-3,4-dihydroisoquinoline-2(1H)-carboxylate

3-{1-ethoxy-1-phenylmethylidene}-5-nitro-2-indolinone

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1,2,3,4-tetrahydroisoquinolin-6-amine

...Expand
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7-nitro-1,2,3,4-tetrahydroisoquinoline

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6-nitro-1,2,3,4-tetrahydro-isoquinoline

A

72299-68-4

1,2,3,4-Tetrahydro-isoquinolin-7-ylamine

B

72299-67-3

1,2,3,4-tetrahydroisoquinolin-6-amine

Conditions
ConditionsYield
With iron; ammonium chloride In ethanol; water at 60℃; for 24h;
...Expand
164148-92-9

tert-butyl 6-amino-3,4-dihydroisoquinoline-2(1H)-carboxylate

72299-67-3

1,2,3,4-tetrahydroisoquinolin-6-amine

Conditions
ConditionsYield
With hydrogenchloride In 1,4-dioxane; dichloromethane at 20℃; for 1.5h;4.85 g
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di-tert-butyl dicarbonate

72299-67-3

1,2,3,4-tetrahydroisoquinolin-6-amine

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tert-butyl 6-amino-3,4-dihydroisoquinoline-2(1H)-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; N,N-dimethyl-formamide at 40℃; under 7500.75 Torr; Flow reactor;91%
In tetrahydrofuran; water at 20℃; for 3h;73%
In tetrahydrofuran at 20℃; for 3h;73%
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bromoacetic acid tert-butyl ester

72299-67-3

1,2,3,4-tetrahydroisoquinolin-6-amine

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6-amino-1,2,3,4-tetrahydroisoquinolineacetic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 20℃; for 24h; Condensation;70%
72299-67-3

1,2,3,4-tetrahydroisoquinolin-6-amine

164148-93-0

6-[(4-cyanobenzoyl)amino]-1,2,3,4-tetrahydroisoquinolineacetic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 70 percent / K2CO3 / acetonitrile / 24 h / 20 °C
2: 60 percent / (1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide)*HCl; DMAP / CH2Cl2 / 12 h / 20 °C
View Scheme
72299-67-3

1,2,3,4-tetrahydroisoquinolin-6-amine

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6-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]iminomethyl]benzoyl]amino]-1,2,3,4-tetrahydroisoquinolineacetic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 70 percent / K2CO3 / acetonitrile / 24 h / 20 °C
2: 60 percent / (1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide)*HCl; DMAP / CH2Cl2 / 12 h / 20 °C
3: 0.34 g
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Chemistry

IUPAC Name: 1,2,3,4-Tetrahydroisoquinolin-2-ium-6-amine
Systematic of 6-Amino-1,2,3,4-tetrahydro-isoquinoline (CAS NO.72299-67-3): 7-Amino-1,2,3,4-tetrahydroisoquinoline ; 1,2,3,4-Tetrahydroisoquinolin-7-ylamine
CAS NO: 72299-67-3
Molecular Formula of 6-Amino-1,2,3,4-tetrahydro-isoquinoline (CAS NO.72299-67-3): C9H12N2
Molecular Weight of 6-Amino-1,2,3,4-tetrahydro-isoquinoline (CAS NO.72299-67-3): 148.205
Molecular Structure:

Product Categories: pharmacetical;Quinoline series 
H bond acceptors: 2
H bond donors: 3
Freely Rotating Bonds: 1
Polar Surface Area: 38.05 Å2
Index of Refraction: 1.6
Molar Refractivity: 46.011 cm3
Molar Volume: 134.576 cm3
Surface Tension: 46.882 dyne/cm
Density: 1.101 g/cm3
Flash Point: 169.23 °C
Enthalpy of Vaporization: 55.719 kJ/mol
Boiling Point: 315.903 °C at 760 mmHg