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77060-26-5

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Basic Information
CAS No.: 77060-26-5
Name: methyl 4-(10,13-dimethyl-3,7-dioxo-2,4,5,6,8,9,11,12,14,15,16,17-dodecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoate
Article Data: 6
Molecular Structure:
Molecular Structure of 77060-26-5 (methyl 4-(10,13-dimethyl-3,7-dioxo-2,4,5,6,8,9,11,12,14,15,16,17-dodecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoate)
Formula: C24H38 O4
Molecular Weight: 390.563
Synonyms: 7b-Hydroxy-3-oxo-5b-cholan-24-oic acid
Density: 1.081g/cm3
Boiling Point: 503.8°C at 760 mmHg
Flash Point: 214.9°C
PSA: 60.44000
LogP: 4.98270
Synthetic route
459840-75-6

3-keto-7β-succinyloxy-5β-cholan-24-oic acid

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
With 20percent NaOH for 1h; Heating;95%
128-13-2

ursodeoxycholic acid

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
With dipotassium hydrogenphosphate; D-glucose; Pseudomonas paucimobilis; yeast extracxt; peptone In water at 28℃; for 24h;90%
Multi-step reaction with 4 steps
1: triethylamine; DMAP / ethyl acetate / 10 h / Heating
2: 5percent NaOH / methanol / 1 h
3: Jones' reagent / acetone / 0.08 h
4: 95 percent / 20percent NaOH / 1 h / Heating
View Scheme
434-13-9

Lithocholic acid

A

128-13-2

ursodeoxycholic acid

B

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
With Gibberella zeae VKM F-2600 extract In methanol; aq. phosphate buffer at 29℃; for 122h; pH=7; Microbiological reaction;A 83%
B n/a
106351-12-6

7β-formyloxy-3-oxo-5β-cholanoic acid-(24)

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
With potassium hydroxide
2646-38-0, 2898-95-5, 31687-63-5, 31687-65-7, 108609-27-4

3,7-dihydroxycholan-24-oic acid, monosodium salt

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
With DL-dithiothreitol; NAD In water; ethyl acetate for 40h; Ambient temperature; 3α-hydroxysteroid dehydrogenase, puryvate/lactic dehydrogenase, serum albumin, potassium phosphate buffer pH=8.5; Yield given;
459840-78-9

Succinic acid mono-[(3R,5S,7S,8R,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-7-yl] ester

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Jones' reagent / acetone / 0.08 h
2: 95 percent / 20percent NaOH / 1 h / Heating
View Scheme
103767-93-7

Succinic acid mono-[(3R,5S,7S,8R,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-3-(3-carboxy-propionyloxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-7-yl] ester

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 5percent NaOH / methanol / 1 h
2: Jones' reagent / acetone / 0.08 h
3: 95 percent / 20percent NaOH / 1 h / Heating
View Scheme
64986-84-1

3α-hydroxy-7β-formyloxy-5β-cholanoic acid-(24)

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chromium (VI)-oxide; acetic acid
2: aqueous KOH-solution
View Scheme
6058-15-7, 6159-50-8

(R)-4-((3R,5S,7S,8R,9S,10S,13R,14S,17R)-3,7-bis(formyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: aq. NaOH solution
2: chromium (VI)-oxide; acetic acid
3: aqueous KOH-solution
View Scheme
434-13-9

Lithocholic acid

77060-26-5

3-keto-7β-hydroxy-5β-cholan-24-oic acid

Conditions
ConditionsYield
With Cunninghamella echinulata VKM F-470 extract In methanol; aq. phosphate buffer at 29℃; pH=7; Microbiological reaction;
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