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80-07-9

Basic Information
CAS No.: 80-07-9
Name: Bis(p-chlorophenyl) sulfone
Article Data: 108
Cas Database
Molecular Structure:
Molecular Structure of 80-07-9 (Bis(p-chlorophenyl) sulfone)
Formula: C12H8Cl2O2S
Molecular Weight: 287.166
Synonyms: Sulfone,bis(p-chlorophenyl) (6CI,8CI);1,1'-Sulfonylbis(4-chlorobenzene);4-Chloro-1-(4-chlorophenylsulfonyl)benzene;4-Chlorophenyl sulfone;B 0810;Bis(4-chlorophenyl) sulfone;Di-p-chlorophenyl sulfone;NSC 23899;NSC 38759;NSC 50730;NSC 7207;p,p'-Dichlorodiphenyl sulfone;p-Chlorophenyl sulfone;
EINECS: 201-247-9
Density: 1.54 g/cm3
Melting Point: 143-146 °C(lit.)
Boiling Point: 419.9 °C at 760 mmHg
Flash Point: 211.2 °C
Solubility: water: <0.1 g/100 mL at 20 °C
Appearance: off-white crystals or powder
Hazard Symbols: IrritantXi,CorrosiveC
Risk Codes: 36/37/38
Safety: 22-24/25-37/39-26
Transport Information: N/A
PSA: 42.52000
LogP: 4.90700
Synthetic route
108-90-7

chlorobenzene

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With sulfuric acid; trifluoroacetic acid; trifluoroacetic anhydride; Η-β Zeochem at 10 - 53℃; for 4h; Product distribution / selectivity;100%
With sulfuric acid at 20℃; for 4h;95.02%
Stage #1: chlorobenzene With aluminum (III) chloride; thionyl chloride In water at 50 - 90℃; for 3h;
Stage #2: With sulfuric acid; dihydrogen peroxide; acetic acid In water at 80℃; for 3h;
93.8%
3085-42-5

bis(4-chlorophenyl)sulfoxide

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With dihydrogen peroxide; acetic acid at 80℃; for 2h;99.3%
With tetrabutyl-ammonium chloride; dihydrogen peroxide In water at 95℃; for 5h; Temperature; Reagent/catalyst;97.8%
With N-(n-butyl)tridemorph phosphotungstate; dihydrogen peroxide In benzene at 90℃; for 2h; Catalytic behavior; Temperature;96.2%
98-60-2

4-chlorobenzenesulfonyl chloride

108-90-7

chlorobenzene

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
iron(III) chloride at 144℃; for 0.333333h; microwave irradiation;95%
With iron(III) chloride at 100 - 120℃;
With aluminium trichloride
With iron(III) chloride at 100 - 120℃;
14752-66-0

sodium p-chlorobenzenesulphinate

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With copper diacetate In acetonitrile at 60℃; for 3h;94%
106-46-7

para-dichlorobenzene

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With aluminum (III) chloride; thionyl chloride at 20℃; for 3h; Temperature;94%
5181-10-2

bis(4-chlorophenyl)sulfide

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With sodium bromate In water at 80℃; for 0.5h; Ionic liquid;92%
With palladium; dihydrogen peroxide In methanol at 100℃; for 6h; Green chemistry; chemoselective reaction;90%
With dihydrogen peroxide In methanol at 40℃; for 1.58333h; chemoselective reaction;89%
4547-68-6

p-chlorobenzenesulfonyl azide

108-90-7

chlorobenzene

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In dichloromethane at 25℃; for 3h; regiospecific reaction;81%
3085-42-5

bis(4-chlorophenyl)sulfoxide

A

5181-10-2

bis(4-chlorophenyl)sulfide

B

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With [ReOCl3(PPh3)2] In ethanol for 18h; Reflux;A 33%
B 65%
With phenyltrifluorodiazoethane; oxygen; 5,15,10,20-tetraphenylporphyrin In dichloromethane; acetonitrile at 20℃; for 0.5h; Irradiation;
14752-66-0

sodium p-chlorobenzenesulphinate

26018-88-2

bis(4-chlorophenyl)iodonium bromide

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With 1-butyl-3-methylimidazolium Tetrafluoroborate at 40℃;62%
14752-66-0

sodium p-chlorobenzenesulphinate

bis(4-chlorophenyl)iodonium tetrafluoroborate

80-07-9

4,4'-dichlorodiphenyl sulphone

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide at 50℃; for 4h;55%
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    Molecular Formula:C12H8Cl2O2S Molecular Weight:287.16 Density:1.54g/cm3 Melting point 146-151 oC Boiling point 397 oC Flash point 233 oC Water solubility <0.1 g/100 mL at 20 oC Irritatin… Appearance:off-white to tan Crystalline powder App

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    Molecular formula: C12H8CL2O2S Molecular weight: 287.16 CAS Registry Number: 80-07-9

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    CAS No.: 80-07-9 Molecular Fomula:C12F8Cl2O2S Molecular weight: 287.16 Appearance: white powder Assay: 99% min Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25KG/drum Application: Pharmaceutica

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Chemistry

Molecular Structure:

Molecular Formula: C12H8Cl2O2S
Molecular Weight: 287.1617
IUPAC Name: 1-Chloro-4-(4-chlorophenyl)sulfonylbenzene
Synonyms of Bis(p-chlorophenyl) sulfone (CAS NO.80-07-9): 1,1'-Sulfonylbis(4-chlorobenzene) ; 4,4'-Dichlorodiphenyl sulfone ; 4,4'-Dichlorodiphenyl sulphone ; 4-06-00-01587 (Beilstein Handbook Reference) ; 4-Chloro-1-(4-chlorophenylsulfonyl)benzene ; 4-Chlorophenyl sulfone ; AI3-01386 ; AI3-02901 ; BRN 2052955 ; Benzene, 1,1'-sulfonylbis(4-chloro- ; Bis(4-chlorophenyl) sulfone ; CCRIS 8813 ; Di-p-chlorophenyl sulfone ; EINECS 201-247-9 ; HSDB 5233 ; NSC 23899 ; Sulfone, bis(p-chlorophenyl) ; p,p'-Dichlorodiphenyl sulfone ; p-Chlorophenyl sulfone
CAS NO: 80-07-9
Classification Code: Tumor data
Melting point: 143-146 °C 
Index of Refraction: 1.61
Molar Refractivity: 69.93 cm3
Molar Volume: 201.6 cm3
Surface Tension: 48.1 dyne/cm
Density: 1.423 g/cm3
Flash Point: 211.2 °C
Enthalpy of Vaporization: 64.75 kJ/mol
Boiling Point: 419.9 °C at 760 mmHg
Vapour Pressure: 7.18E-07 mmHg at 25°C

Uses

 Bis(p-chlorophenyl) sulfone (CAS NO.80-07-9) is used to product 4,4'-diamino-diphenyl sulfone. It is also used as a raw material for engineering plastics polysulfone.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 oral 24gm/kg (24000mg/kg) BEHAVIORAL: TREMOR Helvetica Chimica Acta. Vol. 29, Pg. 1317, 1946.
rat LDLo oral 7500mg/kg (7500mg/kg) GASTROINTESTINAL: "HYPERMOTILITY, DIARRHEA" National Technical Information Service. Vol. OTS0533718,

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

The safety information of Bis(p-chlorophenyl) sulfone (CAS NO.80-07-9) is as follows:
Hazard Codes:Xi ,C
Hazard Note:Harmful/Corrosive/Moisture Sensitive
Risk Statements:36/37/38
36/37/38:Irritating to eyes, respiratory system and skin
Safety Statements:22-24/25-37/39-26
22:Do not breathe dust
24/25:Avoid contact with skin and eyes
37/39:Wear suitable gloves and eye/face protection
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
WGK Germany:2
RTECS:WR3450000
HS Code:29309070
Mildly toxic by ingestion. See also SULFONATES. When heated to decomposition it emits very toxic fumes of Cl and SOx.

Specification

Storage information of Bis(p-chlorophenyl) sulfone (CAS NO.80-07-9):
Store in a cool, dry place. Store in a tightly closed container.