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Basic Information
| CAS No.: | 80-78-4 | ||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Name: | SOLANIDINE | ||||||||||||||
| Article Data: | 20 | ||||||||||||||
| Molecular Structure: | |||||||||||||||
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| Formula: | C27H43 N O | ||||||||||||||
| Molecular Weight: | 397.645 | ||||||||||||||
| Synonyms: | Solanid-5-en-3b-ol (8CI); Solanidine (6CI,7CI);1H-Naphth[2',1':4,5]indeno[1,2-b]indolizine, solanid-5-en-3-ol deriv.; NSC76025; Solanidin; Solatubin; Solatubine | ||||||||||||||
| Density: | 1.1g/cm3 | ||||||||||||||
| Melting Point: | 212-214°C | ||||||||||||||
| Boiling Point: | 503.1°C at 760 mmHg | ||||||||||||||
| Flash Point: | 223.5°C | ||||||||||||||
| Hazard Symbols: |
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| Risk Codes: | 23/24/25 | ||||||||||||||
| Safety: |
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| PSA: | 23.47000 | ||||||||||||||
| LogP: | 5.59290 | ||||||||||||||
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Synthetic route
- 80-78-4
solanidine
Conditions
| Conditions | Yield |
|---|---|
| With tetrabutyl ammonium fluoride In tetrahydrofuran at 50℃; for 2h; | 99% |
| With tetrabutyl ammonium fluoride In tetrahydrofuran at 50℃; for 2h; | 99% |
- 19330-95-1
3β-Hydroxy-7'-oxo-3'α,6'α-dimethyl-1'αH,3aαH-indolizidino<1',2';16,17>androst-5-en
- 80-78-4
solanidine
Conditions
| Conditions | Yield |
|---|---|
| With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene at 0 - 20℃; for 3.5h; Inert atmosphere; | 73% |
| With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene at 0 - 20℃; for 3.5h; Inert atmosphere; | 73% |
- 78720-01-1
C30H47NO5S
A
- 80-78-4
solanidine
B
- 78719-99-0
camtschatcanidine
C
- 78720-00-0
camtschatcanidine monomesylate
Conditions
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride In diethyl ether for 1h; Heating; | A 63.8% B 20% C 15.7% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With ethanol; sodium |
- 80-78-4
solanidine
Conditions
| Conditions | Yield |
|---|---|
| With ethanol; sodium ethanolate at 200 - 210℃; |
- 81942-09-8
solanidine 3-O-α-L-rhamnopyranosyl-(1<*>2)-O-<β-D-glucopyranosyl-(1<*>4)>-β-D-glucopyranoside
- 80-78-4
solanidine
Conditions
| Conditions | Yield |
|---|---|
| With hesperidinase In acetic acid at 37℃; for 24h; | |
| Multi-step reaction with 2 steps 1: 38 mg / 1 N H2SO4 / 2 h / Heating 2: hesperidinase / aq. acetic acid / 24 h / 37 °C View Scheme |
Conditions
| Conditions | Yield |
|---|---|
| With hesperidinase In acetic acid at 37℃; for 24h; |
- 80-78-4
solanidine
Conditions
| Conditions | Yield |
|---|---|
| With hesperidinase In acetic acid at 37℃; for 24h; |
- 20562-03-2
α-chaconine
A
- 511-36-4
solanidine 3-O-β-D-glucopyranoside
B
- 73-34-7
L-rhamnose
C
- 80-78-4
solanidine
Conditions
| Conditions | Yield |
|---|---|
| With water In 1,4-dioxane at 120℃; for 70h; | A 25 mg B 20 mg C 9 mg |
...Expand
- 20562-03-2
α-chaconine
A
- 511-36-4
solanidine 3-O-β-D-glucopyranoside
B
- 80-78-4
solanidine
C
- 469-14-7
solanidine 3-O-α-L-rhamnopyranosyl-(1->4)-β-D-glucopyranoside
D
- 472-51-5
solanidine 3-O-α-L-rhamnopyranosyl-(1->2)-β-D-glucopyranoside
Conditions
| Conditions | Yield |
|---|---|
| at 300℃; | A 27 mg B 15 mg C 19 mg D 31 mg |
...Expand
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SOLANIDINE
