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80532-66-7

Basic Information
CAS No.: 80532-66-7
Name: methyl α,β-epoxy-α-methylcinnamate
Article Data: 10
Cas Database
Molecular Structure:
Molecular Structure of 80532-66-7 (methyl α,β-epoxy-α-methylcinnamate)
Formula: N/A
Molecular Weight: 192.214
Synonyms: methyl α,β-epoxy-α-methylcinnamate
EINECS: N/A
Density: N/A
Melting Point: N/A
Boiling Point: N/A
Flash Point: N/A
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety:
Transport Information: N/A
PSA: N/A
LogP: N/A
Synthetic route
17639-93-9

2-chloro-propionic acid methyl ester

100-52-7

benzaldehyde

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In N,N-dimethyl-formamide 1.) 20 deg C, 72 h, 2.) 40 deg C, 24 h;80%
With sodium methylate In methanol; toluene at 0 - 20℃; Darzens condensation;
With ethanol; sodium ethanolate
21370-57-0, 22946-43-6, 25692-59-5

methyl 2-methyl-3-phenylacrylate

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In tetrachloromethane for 3h; Reflux;67%
25547-51-7

trans-2-methyl-3-phenyloxiranecarboxylic acid

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

92817-97-5

(2S,3R)-2-Hydroxy-3-methanesulfonyloxy-2-methyl-3-phenyl-propionic acid methyl ester

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
With sodium hydride In diethyl ether Yield given;
92817-31-7

(2S,3S)-2-Hydroxy-3-methanesulfonyloxy-2-methyl-3-phenyl-propionic acid methyl ester

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
With sodium hydride In diethyl ether Yield given;
100-52-7

benzaldehyde

polymer-PPh2(1+)-CH2-Ph*Br(1-)

polymer-PPh2(1+)-CH2-Ph*Br(1-)

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) EtMgBr / 1.) THF, -78 deg C, 10 min
View Scheme
92817-30-6

methyl (syn-2,3-dihydroxy-2-methyl-3-phenyl)propionate

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / 1.) overnight; 2.) 0 deg C, 1 h
2: NaH in mineral oil / diethyl ether
View Scheme
92817-29-3

(2RS,3RS)-2-methyl-2,3-dihydroxybenzenepropanoate

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / 1.) overnight; 2.) 0 deg C, 1 h
2: NaH in mineral oil / diethyl ether
View Scheme

5-(Hydroxy-phenyl-methyl)-2,2,5-trimethyl-[1,3]dioxolan-4-one

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: K2CO3 / methanol / 3 h / Ambient temperature
2: pyridine / 1.) overnight; 2.) 0 deg C, 1 h
3: NaH in mineral oil / diethyl ether
View Scheme
Multi-step reaction with 3 steps
1: K2CO3 / methanol / 3 h / Ambient temperature
2: pyridine / 1.) overnight; 2.) 0 deg C, 1 h
3: NaH in mineral oil / diethyl ether
View Scheme
1199-77-5

α-methylcinnamic acid

80532-66-7

methyl α,β-epoxy-α-methylcinnamate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: thionyl chloride / 3 h / 20 °C
2: 3-chloro-benzenecarboperoxoic acid / tetrachloromethane / 3 h / Reflux
View Scheme
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