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844856-42-4

Basic Information
CAS No.: 844856-42-4
Name: 3-broMo-3-chloro-biphenyl
Article Data: 1
Cas Database
Molecular Structure:
Molecular Structure of 844856-42-4 (3-broMo-3-chloro-biphenyl)
Formula: C12H8BrCl
Molecular Weight: 267.553
Synonyms: 3-bromo-3'-chloro-1,1'-biphenyl
Density: 1.463±0.06 g/cm3(Predicted)
Melting Point: 41 °C
Boiling Point: 331.7±17.0 °C(Predicted)
PSA: 0.00000
LogP: 4.76950
Synthetic route
108-86-1

bromobenzene

456-39-3

3-chlorobenzenediazonium tetrafluoroborate

A

844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

B

91354-09-5

4-bromo-3'-chloro-1,1'-biphenyl

C

2-bromo-3’-chloro-1,1’-biphenyl

Conditions
ConditionsYield
With pyridine at 23℃; for 18h; Gomberg-Bachman Arylation; Inert atmosphere; Irradiation; Overall yield = 90 percent; Overall yield = 144 mg;
108847-20-7

4-dibenzothiophene boronic acid

844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

1369369-50-5

4-(3'-chloro-[1,1'-biphenyl]-3-yl)dibenzo[b,d]thiophene

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water; toluene for 5h; Inert atmosphere; Reflux;90%
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water; toluene at 90℃; for 5h;90%
With tetrakis(triphenylphosphine) palladium(0) In ethanol; water; toluene at 80℃; for 7h; Alkaline conditions; Inert atmosphere;82%
844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

86-74-8

9H-carbazole

9-(3'-Chlorobiphenyl-3-yl)-9H-carbazole

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene for 12h; Reflux;90%
844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

C33H28BN3O3

C39H24ClN3O

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 6h; Reflux;73%
844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

10-(4-pyridyl)-9-anthryl boric acid

C31H20ClN

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); tetrabutyl-ammonium chloride; potassium carbonate In ethanol; water; toluene at 78℃; for 8h; Inert atmosphere;72%
1115023-84-1

2-([1,1‘:3’,1“-terphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

C30H21Cl

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere;70%
1036378-83-2

2-([1,1':3′,1''-terphenyl]-5'-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

C30H21Cl

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere;65%
654664-63-8

benzo[l]phenanthrene-2-boronic acid

844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

C30H19Cl

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere;65%
844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

1226810-15-6

2-(carbazol-9-yl)-9H-carbazole

C36H23ClN2

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 6h; Inert atmosphere;59%
844856-42-4

3-bromo-3′-chloro-1,1′-biphenyl

5122-94-1

4-biphenylboronic acid

C24H17Cl

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere;55%
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    Introduction Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical manufacturing for overseas customers, in the field

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