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877-37-2

Basic Information
CAS No.: 877-37-2
Name: 2-bromo-4-chloropropiophenone
Article Data: 71
Molecular Structure:
Molecular Structure of 877-37-2 (2-bromo-4-chloropropiophenone)
Formula: C9H8 Br Cl O
Molecular Weight: 247.519
Synonyms: Propiophenone,2-bromo-4'-chloro- (7CI,8CI); 2-Bromo-1-(4-chlorophenyl)-1-propanone;2-Bromo-4'-chloropropiophenone; a-Bromo-4'-chloropropiophenone; a-Bromo-p-chloropropiophenone
Density: 1.518g/cm3
Melting Point: 77-79 °C(Solv: ligroine (8032-32-4))
Boiling Point: 296.7°C at 760 mmHg
Flash Point: 133.2°C
PSA: 17.07000
LogP: 3.30610
Synthetic route
6285-05-8

4'-chloropropiophenone

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
With bromine at 20℃; for 0.333333h;100%
Stage #1: 4'-chloropropiophenone With bromine In methanol at 20℃; for 0.166667h;
Stage #2: With hydrogen bromide In methanol; water for 110h; Inert atmosphere;
98%
With bromine; hydrogen bromide In methanol at 20℃; for 110h; Inert atmosphere;98%
563-76-8

α-bromopropionyl bromide

108-90-7

chlorobenzene

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
Stage #1: chlorobenzene With aluminum (III) chloride In dichloromethane at 10 - 15℃; for 1h;
Stage #2: α-bromopropionyl bromide In dichloromethane at 20℃; for 16h;
Stage #3: With water In dichloromethane at 0℃;
95.5%
Stage #1: chlorobenzene With aluminum (III) chloride In dichloromethane at 10 - 15℃; for 1h;
Stage #2: α-bromopropionyl bromide In dichloromethane at 20℃; for 16h;
95.5%
With aluminium trichloride at 0℃; for 1.5h;91%
With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 1h; Concentration; Inert atmosphere;74%
108-90-7

chlorobenzene

α-bromo-propionyl chloride

α-bromo-propionyl chloride

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
With aluminium trichloride
etheric solution of 2-diazo-1-<4-chloro-phenyl>-propanone-(1)

etheric solution of 2-diazo-1-<4-chloro-phenyl>-propanone-(1)

Conditions
ConditionsYield
With hydrogen bromide

2-bromo-1-(4-chlorophenyl)-1-propanone

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: carbon disulfide; AlCl3 / Erwaermen des Reaktionsgemisches
2: acetic acid; bromine
View Scheme
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane
2: bromine / dichloromethane
View Scheme
603-35-0

triphenylphosphine

A

103458-84-0

triphenyl[1-(4-chlorophenyl)-1-oxo-2-propyl]-phosphonium bromide

B

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
In acetonitrile
6285-05-8

4'-chloropropiophenone

aluminum chlorid

aluminum chlorid

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
With bromine In chloroform
6285-05-8

4'-chloropropiophenone

4-chloro-α-(3-isobutyl-1,2,4-triazol-1-yl)-propiophenone

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
In diethyl ether; bromine
6285-05-8

4'-chloropropiophenone

1137670-77-9

2-(2,6-dichloro-phenyl)-6-(4,5-diphenyl-oxazol-2-yl)-1H-benzoimidazole

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
With hydrogen bromide; bromine In dichloromethane for 0.25h;
623-03-0

4-Cyanochlorobenzene

877-37-2

2-bromo-1-(4-chlorophenyl)-1-propanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: iodine; magnesium / diethyl ether / Inert atmosphere
1.2: 6 h / Reflux
1.3: Heating
2.1: bromine / diethyl ether / 20 °C / Cooling with ice
View Scheme
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