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94-20-2

Basic Information
CAS No.: 94-20-2
Name: 1-(4-Chlorophenyl)sulfonyl-3-propylurea
Molecular Structure:
Molecular Structure of 94-20-2 (1-(4-Chlorophenyl)sulfonyl-3-propylurea)
Formula: C10H13ClN2O3S
Molecular Weight: 276.76
Synonyms: Urea,1-[(p-chlorophenyl)sulfonyl]-3-propyl- (8CI);1-(p-Chlorobenzenesulfonyl)-3-propylurea;1-Propyl-3-(p-chlorobenzenesulfonyl)urea;Adiaben;Asucrol;Catanil;Chloronase;Diabaril;Diabechlor;Diabenal;Diabenese;Diabeneza;Diabet-Pages;Diabetoral;Diabinese;Glisema;Meldian;Melitase;Millinese;N-(p-Chlorobenzenesulfonyl)-N'-propylurea;NSC 44634;NSC 626720;P 607;Stabinol;U 9818;
EINECS: 202-314-5
Density: 1.334 g/cm3
Melting Point: 128 °C
Boiling Point: 302°C (rough estimate)
Flash Point:
Solubility: Insoluble in water
Appearance: white crystalline powder
Hazard Symbols: HarmfulXn
Risk Codes: 20/21/22-40
Safety: 22-36
Transport Information:
PSA: 83.65000
LogP: 3.60050
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    2016 hot sale Storage:Keep in cool and dry place. Keep away from heat source and direct sunlight. Package:25kg carton drum Application:Hormone; Hyper, Hypoglycaemic;antidiabetic Transportation:by sea Port:shanghai

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    chlorpropamide

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    please contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant informationAppearance:White powder Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated place

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Chemistry

IUPAC Name: Chloropropamide
The MF of Chlorpropamide (CAS NO.94-20-2) is C10H13ClN2O3S.

                            
The MW of Chlorpropamide (CAS NO.94-20-2) is 276.74.
Synonyms of Chlorpropamide (CAS NO.94-20-2): 1-(4-chlorophenyl)sulfonyl-3-propyl-urea ; 4-Chlor-N-(propylcarbamoyl)benzolsulfonamid ; Benzenesulfonamide, 4-chloro-N-((propylamino)carbonyl)- ; Oradian
Appearance: white crystalline powder
Stability: Stable. Combustible
Index of Refraction: 1.552 
EINECS: 202-314-5
Density: 1.334 g/ml 
Melting Point: 128 °C
Merck: 2186

Uses

  Chlorpropamide (CAS NO.94-20-2) is sulfonylurea oral hypoglycemic agents which mainly selectively act on the pancreatic islet-β-cells, promoting insulin secretion.Chlorpropamide has a relatively large side-effects, so the using of the drug are decreasing trend.

Production

 Chlorobenzene sulfonamide reacts with chlorobenzene sulfonyl amide,generating C urea sodium salt. Then hydrochloric acid, refined to derive. Another method is based on chlorobenzene sulfonamide, isopropyl isocyanate, triethylamine as raw materials.

Toxicity Data With Reference

1.    

sce-mus-orl 177 mg/kg

    MUREAV    Mutation Research. 77 (1980),349.
2.    

sce-ham-ipr 7100 µg/kg

    MUREAV    Mutation Research. 77 (1980),349.
3.    

orl-wmn TDLo:25 mg/kg/5D-I:BLD

    DICPBB    Drug Intelligence and Clinical Pharmacy. 18 (1984),981.
4.    

orl-wmn TDLo:300 mg/kg:CNS

    CTOXAO    Clinical Toxicology. 11 (1977),13.
5.    

orl-man TDLo:83 mg/kg/25D-I:GIT

    AJGAAR    American Journal of Gastroenterology. 80 (1985),381.
6.    

orl-rat LD50:2150 mg/kg

    FATOAO    Farmakologiya i Toksikologiya (Moscow). 25 (1962),93.
7.    

ipr-rat LD50:580 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 18 (1971),185.
8.    

ivn-rat LD50:590 mg/kg

    PMDCAY    Progress in Medical Chemistry. 1 (1961),187.
9.    

orl-mus LD50:1546 mg/kg

    AIPTAK    Archives Internationales de Pharmacodynamie et de Therapie. 153 (1965),379.
10.    

ivn-mus LD50:500 mg/kg

    PMDCAY    Progress in Medical Chemistry. 1 (1961),187.

Consensus Reports

NCI Carcinogenesis Bioassay (feed); No Evidence: mouse, rat NCITR*    National Cancer Institute Carcinogenesis Technical Report Series. (Bethesda, MD 20014) No. NCI-CG-TR-45 ,1978. . EPA Genetic Toxicology Program.

Safety Profile

Moderately toxic by ingestion, intraperitoneal, and intravenous routes. Human systemic effects by ingestion: hemolysis with or without anemia, ulceration or bleeding from large intestine, cholestatic jaundice. Human teratogenic effects by ingestion: fetal death. Human reproductive effects by ingestion and possibly other routes: stillbirth, reduced viability and abnormal characteristics of newborn at birth. An experimental teratogen. Experimental reproductive effects. Mutation data reported. An antidiabetic agent. When heated to decomposition it emits very toxic fumes of Cl, NOx, and SOx.Safety information of Chlorpropamide (CAS NO.94-20-2):
Hazard Codes  HarmfulXn
Risk Statements 
20/21/22 Harmful by inhalation, in contact with skin and if swallowed
40 Limited evidence of a carcinogenic effect
Safety Statements 
22 Do not breathe dust
36 Wear suitable protective clothing
WGK Germany  3
RTECS  YS6650000

Specification

A halogenated amide. Organic amides/imides react with azo and diazo compounds to generate toxic gases. Flammable gases are formed by the reaction of organic amides/imides with strong reducing agents. Amides are very weak bases (weaker than water). Imides are less basic yet and in fact react with strong bases to form salts. That is, they can react as acids. Mixing amides with dehydrating agents such as P2O5 or SOCl2 generates the corresponding nitrile. The combustion of these compounds generates mixed oxides of nitrogen (NOx).