18419-84-6Relevant articles and documents
Diethyla propoxycyclohexyl four methyl two silane purifying method and application
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Paragraph 0033-0041, (2016/10/07)
The invention relates to the technical field of chemical industry, in particular to a purification method and an application of dioxethyl-tetramethyl-disilane. A reduced pressure distillation method is utilized for purifying 1, 2-dioxethyl-1, 1, 2, 2-tetramethyl-disilane, and in the reduced pressure distillation process, fillers of a rectifying column for the reduced pressure distillation include magnesium chips, calcium chloride or mixture of the magnesium chips and the calcium chloride. In purification steps of the 1, 2-dioxethyl-1, 1, 2, 2-tetramethyl-disilane, the magnesium chips and/or calcium chloride are/is used as the fillers in the reduced pressure distillation, so that removal of residual hydrogen chloride and ethanol in a reaction system is facilitated, and the 1, 2-dioxethyl-1, 1, 2, 2-tetramethyl-disilane with high purity can be obtained.