2233-00-3

Basic information

• Product Name: 3,3,3-Trichloropropene
• Synonyms: 3,3,3-Trichloropropene;3,3,3-TRICHLOROPROPYLENE;3,3,3-Trichloro-1-propene;3,3,3-Trichloroprop-1-ene95%
• CAS NO: 2233-00-3
• Molecular Formula: C₃H₃Cl₃
• Molecular Weight: 145.41
• Mol File: 2233-00-3.mol
• Article Data: 9

Chemical Properties

• Melting Point: -30°C
• Boiling Point: 122.72°C (estimate)
• Flash Point: 37.7 °C
• Appearance: /
• Density: 1.3670
• Vapor Pressure: 23.5mmHg at 25°C
• Refractive Index: 1.4827
• CAS DataBase Reference: 3,3,3-Trichloropropene(CAS DataBase Reference)
• NIST Chemistry Reference: 3,3,3-Trichloropropene(2233-00-3)
• EPA Substance Registry System: 3,3,3-Trichloropropene(2233-00-3)

Safety Data

• Hazardous Substances Data: 2233-00-3(Hazardous Substances Data)

Usage

Safety Profile

Mutation data reported. Whenheated to decomposition it emits toxic vapors of Clí.

InChI:InChI=1/C3H3Cl3/c1-2-3(4,5)6/h2H,1H2

Upstream product

• 56-23-5 tetrachloromethane 
• 74-85-1 ethene 
• 21700-31-2 1,1,1,2,3-pentachloro-propane 
• 1070-78-6 1,1,1,3-tetrachloropropane 
• 110-80-5 2-ethoxy-ethanol 
• 13749-37-6 3-bromo-1,1,1-trichloropropane 

Downstream Products

• 17219-58-8 1,1-dichloro-but-1-ene 
• 677-21-4 1,1,1-trifluoropropylene 
• 2567-14-8 3,3-dichloroallyl chloride 
• 7789-89-1 1,1,1-trichloropropane 
• 23153-17-5 1,1,1-trichloro-3-iodo-propane 
• 99846-91-0 (3,3-dichloro-allyl)-phenyl ether 
• 99184-45-9 benzyl-(3,3,3-trichloro-ξ-propenyl)-sulfide 
• 80687-85-0 (3,3-Dichloro-allyl)-cyclohexane 
• 99586-08-0 phenyl-(3,3,3-trichloro-propyl)-sulfide 
• 26593-47-5 1,1,-dichloro-1-pentene 
• 88920-84-7 (4,4-dichlorobut-3-en-1-yl)benzene 
• 84816-05-7 tetrachlorofluoropropane 
• 563-58-6 1,1-dichloropropene 
• 114700-65-1 ((E)-1-Chloro-propenyl)-triethyl-silane 

Relevant articles and documents

-

-

PREPARATION OF 2,3,3,3-TETRAFLUOROPROPENE AND INTERMEDIATES THEREOF

The present invention provides a process for preparation of 2,3,3,3-tetrafluoropropene and intermediates thereof. Owing to its low global warming potential and zero ozone depleting potential, it is been proposed as a replacement for existing chlorofluorocarbons and hydrofluorocarbons as refrigerant.

A method of synthesizing 2,3,3,3-tetrafluoropropene

A method of synthesizing 2,3,3,3-tetrafluoropropene is disclosed. The method includes (1) reacting 1,1,1,3-tetrachloropropane with metal powder, and subjecting a reaction solution to alkali washing, drying and rectification to obtain trichloropropylene, (2) mixing the trichloropropylene prepared in the step (1) with a solvent, feeding a fluorine-nitrogen mixed gas, reacting, and rectifying the reaction solution to obtain difluorotrichloropropane, and (3) reacting the difluorotrichloropropane prepared by the step (2) with anhydrous hydrogen fluoride under an action of a catalyst, and subjecting a reaction product to alkali washing, drying and compression to obtain a 2,3,3,3-tetrafluoropropene product. The method has advantages of a simple process, a low cost and environment protection.

PROCESS FOR PREPARING CHLORINE-CONTAINING FLUOROCARBON COMPOUND

The present invention provides a process for preparing at least one chlorine-containing fluorocarbon compound selected from the group consisting of chlorine-containing fluoropropane compounds represented by Formula (1): CFnCl3-nCHClCH2—Cl, wherein n is 1 or 2, and chlorine-containing fluoropropene compounds represented by Formula (2): CFnCl3-nCCl═CH2, wherein n is 1 or 2, wherein the process includes the step of contacting at least one chlorine-containing compound selected from the group consisting of 1,1,1,2,3-pentachloropropane, 1,1,2,3-tetrachloropropene, and 2,3,3,3-tetrachloropropene with hydrogen fluoride in the absence of a catalyst while heating. According to the present invention, the chlorine-containing propane and propene compounds having 1 or 2 fluorine atoms can be prepared by an industrially applicable, simple and effective process.