1-Propene, 3,3,3-trichloro-

Base Information

• Chemical Name: 1-Propene, 3,3,3-trichloro-
• CAS No.: 2233-00-3
• Molecular Formula: C3H3Cl3
• Molecular Weight: 145.416
• Hs Code.: 2903299090
• European Community (EC) Number: 811-549-8
• DSSTox Substance ID: DTXSID3062281
• Nikkaji Number: J101.375K
• Wikidata: Q81989956
• Mol file: 2233-00-3.mol

Synonyms:3,3,3-trichloroprop-1-ene;2233-00-3;3,3,3-TRICHLOROPROPENE;1-Propene, 3,3,3-trichloro-;3,3,3-Trichloro-1-propene;3,3,3-Trichloropropylene;Propene, 3,3,3-trichloro-;BRN 1740219;4-01-00-00749 (Beilstein Handbook Reference);CH2=CHCCl3;3,3,3-trichloro-propene;3,3,3-Dichloro-1-propene;SCHEMBL185771;DTXSID3062281;SCHEMBL12898061;MFCD01749212;AKOS006277121;LS-123554;Propene, 3,3,3-trichloro- (6CI,7CI,8CI)

Chemical Property of 1-Propene, 3,3,3-trichloro-

Chemical Property:

• Vapor Pressure: 23.5mmHg at 25°C
• Melting Point: -30°C
• Refractive Index: 1.474
• Boiling Point: 114.5 °C at 760 mmHg
• Flash Point: 37.7 °C
• PSA: 0.00000
• Density: 1.354 g/cm³
• LogP: 2.54260
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 143.930033
• Heavy Atom Count: 6
• Complexity: 51.5

Purity/Quality:

99% ^*data from raw suppliers

3,3,3-Trichloroprop-1-ene 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC(Cl)(Cl)Cl

Technology Process of 1-Propene, 3,3,3-trichloro-

There total 6 articles about 1-Propene, 3,3,3-trichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1,2,3-pentachloro-propane (21700-31-2) → 3,3,3-trichloro-1-propene (2233-00-3) + 1,1,2,3-Tetrachloropropene (10436-39-2)

Guidance literature:

at 400 ℃; for 0.0130556h; under 750.075 Torr; Inert atmosphere;

Reference yield:

tetrachloromethane (56-23-5) + ethene (74-85-1) → 1,1,2,2-tetrachloroethylene (127-18-4) + 1,1,1,3-tetrachloropropane (1070-78-6) + 3,3,3-trichloro-1-propene (2233-00-3) + hexachloroethane (67-72-1)

Guidance literature:

In tetrachloromethane; other Radiation; γ-radiation of C2H4 in CCl4;; yields given;;

DOI:10.1021/j100671a004

Reference yield:

1,1,1,3-tetrachloropropane (1070-78-6) → 3,3-dichloroallyl chloride (2567-14-8) + 3,3,3-trichloro-1-propene (2233-00-3)

Guidance literature:

With 2-ethoxy-ethanol; potassium hydroxide; at 80 ℃;

upstream raw materials:

1,1,1,3-tetrachloropropane

3-bromo-1,1,1-trichloropropane

2-ethoxy-ethanol

tetrachloromethane

Downstream raw materials:

benzyl-(3,3,3-trichloro-ξ-propenyl)-sulfide

3-(4-bromo-phenyl)-1,1-dichloro-propene

(3,3-dichloro-allyl)-phenyl ether

1,1,1-trichloropropane