69745-30-8Relevant articles and documents
Thermal- and photo-induced transformations of N-aryl-N-nitroso-hydroxylamine ammonium salts to azoxy compounds
Hwu, Jih Ru,Yau, Chii Shyang,Tsay, Shwu-Chen,Ho, Tong-Ing
, p. 9001 - 9004 (1997)
Heating of an ethanolic solution containing N-aryl-N-nitrosohydroxylamine ammonium salts at 78°C produced the desired azoxy compounds in 80-93% yields. Furthermore, irradiation with UV light (κ ≤300 nm) of ethanolic solutions of those ammonium salts at room temperature also provided the desired azoxy compounds in 51-72% yields.