Tetrahedron Letters p. 9001 - 9004 (1997)
Update date:2022-08-04
Topics:
Hwu, Jih Ru
Yau, Chii Shyang
Tsay, Shwu-Chen
Ho, Tong-Ing
Heating of an ethanolic solution containing N-aryl-N-nitrosohydroxylamine ammonium salts at 78°C produced the desired azoxy compounds in 80-93% yields. Furthermore, irradiation with UV light (κ ≤300 nm) of ethanolic solutions of those ammonium salts at room temperature also provided the desired azoxy compounds in 51-72% yields.
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