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Cas Database |
| Name |
trans-Mentha-2,8-dien-1-ol |
EINECS | N/A |
| CAS No. | 22972-51-6 | Density | 0.947 g/cm3 |
| PSA | 20.23000 | LogP | 2.27970 |
| Solubility | 4.2g/L | Melting Point |
N/A |
| Formula | C10H16O | Boiling Point | 216.873 °C at 760 mmHg |
| Molecular Weight | 152.236 | Flash Point | 86.957 °C |
| Transport Information | N/A | Appearance | white solid |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
2-Cyclohexen-1-ol,1-methyl-4-(1-methylethenyl)-, (1S-cis)-;(+)-(1S,4R)-p-Mentha-2,8-dien-1-ol;(+)-cis-p-Mentha-2,8-dien-1-ol;(+)-p-Mentha-2,8-dien-1-ol;(1S,4R)-p-Menth-2,8-dien-1-ol;cis-Isolimonenol;p-Mentha-2,8-dien-1-b-ol; |
Article Data | 35 |
trans-Mentha-2,8-dien-1-ol Synthetic route
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| With piperidine In dimethyl sulfoxide at 170℃; for 4h; | 75% |
- 1415961-21-5
(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| at 180℃; under 1 Torr; Cope Elimination; Pyrolysis; | 74% |
| With dihydrogen peroxide In ethanol; water at 150 - 162℃; Reflux; Schlenk technique; Glovebox; Inert atmosphere; | 38.2 g |
- 74756-11-9
(1S,2S,4R)-2-phenylseleninyl-p-menth-8-en-1-ol
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| In chloroform for 0.5h; Heating; | 53% |
| In chloroform at 62℃; for 6h; Inert atmosphere; | 512 g |
- 6909-30-4
(1S,2R,4R)-limonene-1,2-epoxide
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| Stage #1: (1S,2R,4R)-limonene-1,2-epoxide With sodium tetrahydroborate; diphenyl diselenide for 2h; Heating; Stage #2: With dihydrogen peroxide for 7h; Heating; Further stages.; | 31.6% |
| Multi-step reaction with 2 steps 1.1: H2O / 18 h / 150 °C 2.1: H2O2 / H2O / 18 h / 20 °C 2.2: 150 - 180 °C View Scheme | |
| Multi-step reaction with 3 steps 1: H2O / 150 °C / sealed vessel 2: 30percent H2O2 / H2O 3: pyrolysis View Scheme |
- 5989-27-5
D-limonene
A
- 52154-82-2
(1R,4R)-p-mentha-2,8-dien-1-ol
B
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| With oxygen; rose bengal In methanol at 0℃; for 8.5h; UV-irradiation; | A 5.3% B 13.4% |
| With air Erwaermen des Reaktionsprodukts mit wss. Natriumsulfit-Loesung; | |
| (i) O2, MeOH, (irradiation), (ii) LiAlH4, Et2O; Multistep reaction; | |
| (i) O2, rose bengal, MeOH, (irradiation), (ii) LiAlH4, Et2O; Multistep reaction; | |
| With air Erwaermen des Reaktionsprodukts mit wss. Natriumsulfit-Loesung; |
- 5989-27-5
D-limonene
B
- 18383-51-2
(-)-trans-carveol
C
- 52154-82-2
(1R,4R)-p-mentha-2,8-dien-1-ol
D
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
E
- 2102-62-7
p-Menthadiene-<1(7),8>-trans-ol-(2)
F
- 10374-04-6
p-Menthadiene<1(7),8>-cis-ol-(2)
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane; air; zinc 5,10,15,20-tetraphenylporphyrin; triphenylphosphine In benzene for 3h; Irradiation; multistep reaction: photosensitized oxygenation of olefines; | |
| With sodium tetrahydroborate; tetraphenylporphyrine; oxygen Product distribution; 1.) acetonitrile, irradiation, 2.) methanol; other sensitizers; | A 5 % Chromat. B 7 % Chromat. C 9 % Chromat. D 40 % Chromat. E 16 % Chromat. F 23 % Chromat. |
| With oxygen; fullerene-C60 In toluene at 0 - 10℃; for 4h; Product distribution; Irradiation; other sensitizer in other solvent; |
- 138-86-3
limonene.
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| With oxygen Irradiation; |
- 5989-27-5
D-limonene
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| With oxygen Irradiation; | |
| Multi-step reaction with 4 steps 1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1.5 h / -5 - 20 °C 2: water / 18 h / 20 °C / Reflux 3: dihydrogen peroxide / water; acetonitrile / 2 h / 20 °C / Cooling with ice 4: 180 °C / 1 Torr / Pyrolysis View Scheme | |
| Multi-step reaction with 4 steps 1.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 5 °C 2.1: sodium tetrahydroborate / ethanol / 1 h / 8 °C / Inert atmosphere 2.2: 4 h / 8 - 80 °C / Inert atmosphere 3.1: dihydrogen peroxide / ethanol; tetrahydrofuran / 6 h / 6 - 20 °C / Inert atmosphere 4.1: chloroform / 6 h / 62 °C / Inert atmosphere View Scheme |
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| at 140℃; |
- 22972-51-6
(1S,4R)-p-mentha-2,8-dien-1-ol
| Conditions | Yield |
|---|---|
| pyrolysis; Yield given; |
trans-Mentha-2,8-dien-1-ol Specification
The trans-Mentha-2,8-dien-1-ol is a chemical which the formula C10H16O. With the CAS registry number 22972-51-6, it is also named as (+)-(1S,4R)-p-Mentha-2,8-dien-1-ol ; (1S,4R)-1-methyl-4-(prop-1-en-2-yl)cyclohex-2-enol ; (1S,4R) 1-methyl-4-(1-methylethenyl)-2-cyclohexen-1-ol . It is white solid. This product should be stored on the place where the temperature is at 0-5°C. At this temperature, the product can be kept perfect.
The trans-Mentha-2,8-dien-1-ol has many suppliers, such as PharmaSci Shanghai Co., Ltd. and Ring Specialty Chemicals Inc. The price of this product changes with the market.
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