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Cas Database |
| Name |
Cyclohexanecarboxaldehyde |
EINECS | 218-057-7 |
| CAS No. | 2043-61-0 | Density | 0.992 g/cm3 |
| PSA | 17.07000 | LogP | 1.76560 |
| Solubility | Soluble in chloroform, ether, alcohol. Slightly soluble in water. | Melting Point |
34-35 °C |
| Formula | C7H12O | Boiling Point | 159.5 °C at 760 mmHg |
| Molecular Weight | 112.172 | Flash Point | 40.6 °C |
| Transport Information | UN 1989 3/PG 3 | Appearance | Clear colorless to faintly pink liquid |
| Safety | 16-26-36-37/39 | Risk Codes | 10-36/37/38-36 |
| Molecular Structure |
|
Hazard Symbols |
 Xi,  F
|
| Synonyms |
Hexahydrobenzaldehyde;Cyclohexane carboxaldehyde;1-Cyclohexylcarboaldehyde;Cyclohexane formaldehyde;Cyclohexanecarboxaldehyde (8CI)(9CI);Cyclohexanaecarboxaldehyde;Formylcyclohexane;Cyclohexylformaldehyde;Cyclohexanal;1-Formylcyclohexane; |
Article Data | 386 |
Cyclohexanecarboxaldehyde Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With 2,2,6,6-tetramethyl-piperidine-N-oxyl; 1-(diacetoxyiodo)-4-methylbenzene In chloroform at 20℃; for 24h; | 100% |
| With 2,2,6,6-tetramethyl-piperidine-N-oxyl; oxygen; copper(I) bromide dimethylsulfide complex In chlorobenzene at 80℃; for 8h; | 99% |
| With sodium hydrogencarbonate; sodium bromide In dichloromethane at 20℃; Electrochemical reaction; | 99% |
- 25957-47-5
Sodium; 1-oxa-spiro[2.5]octane-2-carboxylate
- 2043-61-0
cyclohexanecarbaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid stream of steam under a carbon dioxide atmosphere; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; (-)-(2-menthyl-4,7-dimethylindenyl)Rh(CO)2 at 120℃; under 30002.4 Torr; for 3h; | 100% |
| With hydrogen In cyclohexane at 120℃; under 45004.5 Torr; for 5h; Autoclave; | 99% |
| With hydrogen In water at 100℃; under 15001.5 Torr; for 12h; Autoclave; Green chemistry; | 99.5% |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; β-cyclodextrin/Pd In water at 25℃; under 15001.2 Torr; for 2h; | 100% |
| With glucose-6-phosphate dehydrogenase; D-glucose 6-phosphate; pentaerythritol tetranitrate reductase T26S mutant; NADPH In N,N-dimethyl-formamide at 30℃; for 24h; pH=7; aq. phosphate buffer; Enzymatic reaction; | 84 %Chromat. |
| With progesterone 5β-reductase from Arabidopsis thaliana, thale cress; NADPH In aq. buffer at 30℃; for 24h; pH=7.5; Reagent/catalyst; Enzymatic reaction; | |
| With D-glucose; glucose dehydrogenase (GDH; 10U); holo-(flavin free double bond reductase from Nicotiana tabacum); nicotinamide adenine dinucleotide phosphate In aq. phosphate buffer at 30℃; for 24h; pH=6.4; Enzymatic reaction; | 55 %Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| With MCM-41 silicate; hydrogen; di(rhodium)tetracarbonyl dichloride at 100℃; under 21001.7 Torr; for 20h; | 99.4% |
| With Rh; benzaldehyde In benzene Mechanism; Irradiation; other d8 metal carbonyls, other aromatic ketones and aldehydes; relative quantum yields; |
Conditions
| Conditions | Yield |
|---|---|
| With tri-n-butyl-tin hydride; triphenylphosphine; palladium dichloride In benzene for 10h; Ambient temperature; | 98% |
| With sodium tris(tert-butoxo)aluminium hydride In tetrahydrofuran; diethylene glycol dimethyl ether at -78℃; for 3h; | 89% |
| With polymer(resin Amberlyst A-26)-supported tetracarbonylhydridoferrate anion In tetrahydrofuran for 0.75h; Heating; | 85% |
- 2043-61-0
cyclohexanecarbaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In tetrahydrofuran at 20℃; for 2h; | 98% |
- 70777-60-5
Cyclohexancarboxaldehyde dithioethyleneacetal
- 2043-61-0
cyclohexanecarbaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With silica gel; copper(II) nitrate In tetrachloromethane for 0.25h; Ambient temperature; | 97% |
| With hydrogen bromide; dihydrogen peroxide In acetonitrile at 25℃; for 0.133333h; | 92% |
| With t-butyl bromide; dimethyl sulfoxide at 70 - 75℃; for 4h; | 86% |
| With trimethylsilyl iodide; dimethyl sulfoxide In tetrachloromethane at 75 - 80℃; for 6h; | 82% |
- 56698-00-1
2-cyclohexyl-1,3-dithiane
- 2043-61-0
cyclohexanecarbaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With silica gel; copper(II) nitrate In tetrachloromethane for 0.416667h; Ambient temperature; | 97% |
| With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In neat (no solvent) at 20℃; for 0.75h; Milling; | 83% |
| With dihydrogen peroxide; tantalum pentachloride; sodium iodide In water; ethyl acetate at 20℃; for 144h; | 81% |
- 80783-98-8
N-methoxy-N-methylcyclohexanecarboxamide
- 2043-61-0
cyclohexanecarbaldehyde
Conditions
| Conditions | Yield |
|---|---|
| With lithium diisobutyl-tert-butoxyaluminum hydride In tetrahydrofuran; hexane at 0℃; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 96% |
| With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.166667h; | 86% |
| With diisobutylaluminium hydride In tetrahydrofuran at 0℃; for 0.5h; | 74% |
| Stage #1: N-methoxy-N-methylcyclohexanecarboxamide With chloromagnesium dimethylaminoborohydride In tetrahydrofuran at 25℃; for 0.5h; Inert atmosphere; Stage #2: With acetaldehyde; acetic acid In tetrahydrofuran; pentane for 0.5h; Inert atmosphere; | 65% |
Cyclohexanecarboxaldehyde Chemical Properties
Formula : C7H12O
MW : 112.17
Boiling Point : 161 ° C
Chinese name : cyclohexane formaldehyde; Cyclohexyl - formaldehyde
English title :cyclohexanecarboxaldehyde;cxyclohexanal;
cyclohexanecarbaldehyde
Nature Description : colorless, transparent liquid
Refractive index : n20/D 1.452(lit.)
Fp : 105 °F
storage temp. : 2-8°C
Sensitive : Air Sensitive
MOL File: 2043-61-0.mol
Appearance：Colorless or slight yellow liquid
Cyclohexanecarboxaldehyde Safety Profile
Hazard Codes : Xi,F
Risk Statements : 10-36/37/38
Safety Statements : 16-26-36-37/39
RIDADR : UN 1989 3/PG 3
WGK Germany : 3
PackingGroup : III
Risk Statements : 10-36/37/38
Safety Statements : 16-26-36-37/39
RIDADR : UN 1989 3/PG 3
WGK Germany : 3
PackingGroup : III
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