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Cas Database |
| Name |
Lithium bis(oxalate)borate |
EINECS | N/A |
| CAS No. | 244761-29-3 | Density | N/A |
| PSA | 105.20000 | LogP | -2.37800 |
| Solubility | 1015g/L at 20℃ | Melting Point |
>300°C (lit.) |
| Formula | C4BLiO8 | Boiling Point | N/A |
| Molecular Weight | 193.791 | Flash Point | N/A |
| Transport Information | N/A | Appearance | N/A |
| Safety | 26 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols | Xi |
| Synonyms |
Borate(1-),bis[ethanedioato(2-)-kO1,kO2]-, lithium, (T-4)- (9CI);Lithium bis(oxalato)borate;Lithium bis(oxalato)borate(1-); |
Article Data | 13 |
Lithium bis(oxalate)borate Synthetic route
- 131543-46-9
Glyoxal
- 14720-30-0
boron fluoridedichloride
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| In 1,4-dioxane at 30℃; under 0 Torr; for 3h; Flow reactor; | 99.2% |
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| In acetonitrile at 43 - 57℃; for 11h; Inert atmosphere; | 98.8% |
- 409071-16-5
lithium difluoromono[1,2-oxalato(2-)-O,O'] borate
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| With 1,1,2,2-tetrafluoro-3-(1,1,2,2-tetrafluoroethoxy)propane; 2,3-(4-formylbenzo)-1,4,7,10-tetraoxa-2-cyclododecene; 10-benzyl-1,4,7-trioxa-10-azacyclododecane at 90℃; under 900.09 Torr; for 5h; Inert atmosphere; | 93% |
- 18294-04-7
bis(trimethylsilyl)ethanedioic acid ester
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| With lithium tetramethanolatoborate In acetonitrile at 45 - 50℃; | 92% |
- 1310-66-3
lithium hydroxide monohydrate
- 18546-66-2
tris-(triethylsilyl)-borate
- 144-62-7
oxalic acid
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| Stage #1: lithium hydroxide monohydrate; oxalic acid In tetrahydrofuran for 2h; Reflux; Stage #2: tris-(triethylsilyl)-borate at 150℃; for 1h; | 83.3% |
- 1310-66-3
lithium hydroxide monohydrate
- 4325-85-3
tris(trimethylsilyl)borate
- 144-62-7
oxalic acid
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| Stage #1: lithium hydroxide monohydrate; oxalic acid In N,N-dimethyl-formamide at 100℃; for 1h; Stage #2: tris(trimethylsilyl)borate at 120℃; for 6h; Solvent; Temperature; | 83.1% |
- 383189-04-6
tris(dimethylvinylsilyl) borate
- 144-62-7
oxalic acid
- 554-13-2
lithium carbonate
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| Stage #1: oxalic acid; lithium carbonate With 1,2-propylene cyclic carbonate at 200℃; for 1h; Stage #2: tris(dimethylvinylsilyl) borate at 250℃; for 2h; | 81.9% |
- 1310-66-3
lithium hydroxide monohydrate
- 11113-50-1
boric acid
- 144-62-7
oxalic acid
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| Stage #1: lithium hydroxide monohydrate; boric acid; oxalic acid for 1h; Milling; Stage #2: at 240℃; for 6h; Temperature; | 79.5% |
| In water at 80 - 85℃; for 24h; Solvent; | 72% |
- 144-62-7
oxalic acid
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| Stage #1: boron trifluoride dimethyl carbonate complex; lithium fluoride In dimethyl sulfoxide at 90℃; for 7h; Inert atmosphere; Stage #2: oxalic acid With tetrachlorosilane In dimethyl sulfoxide at 20 - 150℃; for 25h; Solvent; Temperature; Reagent/catalyst; Inert atmosphere; | 60% |
- 144-62-7
oxalic acid
- 244761-29-3
lithium bis[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
| With lithium hydroxide; boric acid | |
| With lithium hydroxide; boric acid at 179.84℃; for 2h; |
Lithium bis(oxalate)borate Specification
The Lithium bis(oxalate)borate, with the CAS registry number 244761-29-3, is also known as Acetic acid, 2,2'-[(hydroxyborylene)didioxy]bis[2-oxo-, lithium salt (1:3). This chemical's molecular formula is C4BLiO8 and molecular weight is 193.79. What's more, its systematic name is called Trilithium 2,2'-[(oxidoboranediyl)didioxy]bis(oxoacetate). This chemical's classification code is TSCA Flag P [A commenced PMN (Premanufacture Notice) substance].
Physical properties about Lithium bis(oxalate)borate are: (1) #H bond acceptors: 11; (2) #H bond donors: 3; (3) #Freely Rotating Bonds: 9; (4) Polar Surface Area: 174.38 Å2.
You can still convert the following datas into molecular structure:
(1) SMILES: [Li+].[Li+].[Li+].O=C(OOB([O-])OOC(=O)C([O-])=O)C([O-])=O
(2) InChI: InChI=1/C4H2BO11.3Li/c6-1(7)3(10)13-15-5(12)16-14-4(11)2(8)9;;;/h(H,6,7)(H,8,9);;;/q-1;3*+1/p-2
(3) InChIKey: JTIFZKXQGWPTGY-NUQVWONBAS
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