- Phenazine
- Phenazine, 5,10-dihydro-
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Cas Database |
| Name |
Phenazine, 5,10-dihydro- |
EINECS | N/A |
| CAS No. | 613-32-1 | Density | 1.152 g/cm3 |
| PSA | 31.58000 | LogP | 3.21140 |
| Solubility | N/A | Melting Point |
315-316 °C |
| Formula | C12H10N2 | Boiling Point | 358.5 °C at 760 mmHg |
| Molecular Weight | 182.225 | Flash Point | 236.2 °C |
| Transport Information | N/A | Appearance | N/A |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
5,10-Dihydrophenazine;Dihydrophenazine;N,N'-Dihydrophenazine;NSC 402913; |
Article Data | 58 |
Phenazine, 5,10-dihydro- Synthetic route
| Conditions | Yield |
|---|---|
| With sodium dithionite; water In ethanol for 2.5h; Ambient temperature; | 98% |
| With sodium dithionite In ethanol; water at 20℃; for 4h; Inert atmosphere; | 98% |
| With sodium dithionite In ethanol; water at 85℃; for 0.5h; Inert atmosphere; | 97.5% |
| Conditions | Yield |
|---|---|
| With 18-crown-6 ether; copper; caesium carbonate In 1,2-dichloro-benzene for 24h; Reflux; | 72.1% |
| With copper(l) iodide; 2,2'-biimidazole; caesium carbonate In N,N-dimethyl-formamide at 120℃; for 24h; Ullmann reaction; Inert atmosphere; | 63% |
| Conditions | Yield |
|---|---|
| With tris-(dibenzylideneacetone)dipalladium(0); acetophenone p-toluenesulfonylhydrazone; lithium tert-butoxide In 1,4-dioxane at 100℃; for 6h; Inert atmosphere; | 70% |
| Conditions | Yield |
|---|---|
| With Cp*Rh(2-(2-pyridyl)phenyl)H; hydrogen In tetrahydrofuran at 80℃; under 3040.2 Torr; for 48h; Catalytic behavior; Glovebox; | A 19% B 54% |
| Conditions | Yield |
|---|---|
| With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 30% B 35% |
| Conditions | Yield |
|---|---|
| With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 35% B 15% |
- 56975-77-0
N'‑(1‑phenylethylidene)benzenesulfonohydrazide
- 615-36-1
2-bromoaniline
A
- 613-32-1
5,10-dihydrophenazine
B
- 64097-92-3
2-(1-phenylvinyl)aniline
| Conditions | Yield |
|---|---|
| With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 11% B 30% |
- 4545-21-5
acetophenone p-toluenesulfonylhydrazone
- 615-36-1
2-bromoaniline
A
- 613-32-1
5,10-dihydrophenazine
B
- 64097-92-3
2-(1-phenylvinyl)aniline
| Conditions | Yield |
|---|---|
| With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; XPhos In 1,4-dioxane at 110℃; Inert atmosphere; | A 22% B 28% |
- 18264-71-6
bis(2-nitrophenyl)amine
- 613-32-1
5,10-dihydrophenazine
| Conditions | Yield |
|---|---|
| With methanol; sodium |
| Conditions | Yield |
|---|---|
| at 200 - 210℃; im Rohr; |
Phenazine, 5,10-dihydro- Specification
This chemical is called Phenazine, 5,10-dihydro-, and its systematic name is 5,10-dihydrophenazine. With the molecular formula of C12H10N2, its molecular weight is 182.22. The CAS registry number of this chemical is 613-32-1.
Other characteristics of the Phenazine, 5,10-dihydro- can be summarised as followings: (1)ACD/LogP: 2.51; (2)# of Rule of 5 Violations: 0; (3)#H bond acceptors: 2; (4)#H bond donors: 2; (5)#Freely Rotating Bonds: 0; (6)Polar Surface Area: 6.48 Å2; (7)Index of Refraction: 1.624; (8)Molar Refractivity: 55.88 cm3; (9)Molar Volume: 158.1 cm3; (10)Polarizability: 22.15×10-24cm3; (11)Surface Tension: 46.2 dyne/cm; (12)Density: 1.152 g/cm3; (13)Flash Point: 236.2 °C; (14)Enthalpy of Vaporization: 60.4 kJ/mol; (15)Boiling Point: 358.5 °C at 760 mmHg; (16)Vapour Pressure: 2.54E-05 mmHg at 25°C.
You can still convert the following datas into molecular structure:
1.SMILES: c3ccc2c(Nc1c(cccc1)N2)c3
2.InChI: InChI=1/C12H10N2/c1-2-6-10-9(5-1)13-11-7-3-4-8-12(11)14-10/h1-8,13-14H
3.InChIKey: IVURTNNWJAPOML-UHFFFAOYAT
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