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Detail of "16419-60-6"

  • CAS Number:
  • 16419-60-6
  • Name:

  • Boronicacid, B-(2-methylphenyl)-

  • Superlist Name:
  • 2-Tolylboronic acid
  • Molecular Structure:
  • Formula:
  • C7H9BO2
  • Molecular Weight:
  • 135.96
  • Synonyms:
  • Boronicacid, (2-methylphenyl)- (9CI);o-Tolueneboronic acid (7CI,8CI);(2-Tolyl)boronic acid;2-Methyl-1-phenylboronic acid;2-Methylbenzeneboronicacid;2-Methylphenylboronic acid;2-Tolueneboronic acid;o-Boronotoluene;o-Methylphenylboronic acid;o-Tolylboronic acid;
  • Density:
  • 1.1 g/cm3
  • Melting Point:
  • 162-164 °C(lit.)
  • Boiling Point:
  • 283.4 °C at 760 mmHg
  • Flash Point:
  • 125.2 °C
  • Appearance:
  • beige crystalline powder
  • Hazard Symbols:
  • IrritantXi
  • Risk Codes:
  • 36/37/38
  • Safety:
  • 26-36/37/39 Details
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CAS No.16419-60-6 2-Tolylboronic acid

16419-60-6 2-Tolylboronic acid Synonyms 2-Methylphenylboronic acid Molecular Formula C7H9BO2 Molecular Weight 135.96 CAS Registry Number 16419-60-6

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MF:C7H9BO2 MW:135.95

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Reference

Colloidal Gold Nanoparticles as Catalyst for Carbon-Carbon Bond Formation: Application to Aerobic Homocoupling of Phenylboronic Acid in Water
Colloidal Gold Nanoparticles as Catalyst for Carbon-Carbon Bond Formation: Application to Aerobic Homocoupling of Phenylboronic Acid in Water.In this study， 605-39-0 and 16419-60-6 are also used. Tsunoyama, Hironori; Sakurai, Hidehiro; Ichikuni, Nobuyuki; Negishi, Yuichi; Tsukuda, Tatsuya (Research Center for Molecular-Scale Nanoscience, Institute for Molecular Science, Okazaki 444-8585, Japan). Langmuir, 20(26), 11293-11296 (English) 2004 American Chemical Society. CODEN: LANGD5. ISSN: 0743-7463. DOCUMENT TYPE: Journal CA Section: 29 (Organometallic and Organometalloidal Compounds) Section cross-reference(s): 25 Gold nanoparticles (<2 nm) stabilized by poly(N-vinyl-2-pyrrolidone) (Au:PVP NPs) were prepd. by redn. of AuCl4- with NaBH4 in the presence of PVP and characterized via an array of methods including optical absorption spectroscopy, transmission electron microscopy, x-ray diffraction, x-ray absorption near-edge structure, extended x-ray absorption fine structure, and XPS. Au:PVP NPs acted as catalyst toward homocoupling of phenylboronic acid in water under aerobic conditions is demonstrated for the first time. Suppression of biphenyl formation under anaerobic conditions indicates that mol. oxygen dissolved in water is intimately involved in the coupling reactions. A mechanism of the aerobic homocoupling catalyzed by the Au:PVP NPs is proposed on the basis of a crucial role of dissolved oxygen, steric effects on the product yields, and the well-established mechanism for the Pd(II)-based catalysts. .
Palladium-Catalyzed Suzuki-Type Cross-Couplings of Iodocyclopropanes with Boronic Acids: Synthesis of trans-1,2-Dicyclopropyl Alkenes
Palladium-Catalyzed Suzuki-Type Cross-Couplings of Iodocyclopropanes with Boronic Acids: Synthesis of trans-1,2-Dicyclopropyl Alkenes. Charette, Andre B.; Giroux, Andre (Departement de Chimie, Universite de Montreal, Quebec, QC H3C 3J7, Can.). Journal of Organic Chemistry, 61(25), 8718-8719 (English) 1996 American Chemical Society. CODEN: JOCEAH. ISSN: 0022-3263. DOCUMENT TYPE: Journal CA Section: 24 (Alicyclic Compounds) The cross-coupling reaction between iodocyclopropanes and boronic acids under Suzuki type conditions is described. High yields of vinyl- and aryl-substituted cyclopropanes were obtained under the optimized conditions for the cross-coupling process. E.g.In this experiment, several chemicals are used like 16419-60-6 , coupling of PhB(OH)2 with trans-1-iodo-2-(benzyloxymethyl)cyclopropane to give 80% trans-1-phenyl-2-(benzyloxymethyl)cyclopropane was catalyzed by Pd(OAc)2/PPh3 in DMF-H2O in presence of K2CO3 and Bu4NCl. .
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