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Cas Database |
| Name |
1-Chloroethyl cyclohexyl carbonate |
EINECS | 444-950-8 |
| CAS No. | 99464-83-2 | Density | 1.13 g/cm3 |
| PSA | 35.53000 | LogP | 3.05710 |
| Solubility | N/A | Melting Point |
N/A |
| Formula | C9H15ClO3 | Boiling Point | 283.9 °C at 760 mmHg |
| Molecular Weight | 206.669 | Flash Point | 115.6 °C |
| Transport Information | N/A | Appearance | Colorless and transparent liquid |
| Safety | 26-36/37/39 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
1-Chloroethyl Cyclohexyl Carbonate (JCC-2);Intermediate of Candesartan Cilexetil;1-Chloroethyl Cyclohexyl Carbonate (Intermediate of Candesartan Cilexetil);1-Chloro Ethyl Cyclohexyl Carbonate;Cyclohexyl-(1-chloroethyl)-carbonate; |
Article Data | 21 |
1-Chloroethyl cyclohexyl carbonate Synthetic route
- 50893-53-3
carbonochloridic acid 1-chloro-ethyl ester
- 108-93-0
cyclohexanol
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
| Conditions | Yield |
|---|---|
| With pyridine In dichloromethane at 0 - 20℃; | 94% |
| With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | 94% |
| With pyridine In dichloromethane at -78℃; | 80% |
- 123-63-7
paracetaldehyde
- 108-93-0
cyclohexanol
- 503-38-8
trichloromethyl chloroformate
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
| Conditions | Yield |
|---|---|
| Stage #1: paracetaldehyde; trichloromethyl chloroformate With pyridine at -10 - 0℃; for 8h; Stage #2: cyclohexanol With pyridine at 20℃; for 3h; Reagent/catalyst; Temperature; | 93% |
| Conditions | Yield |
|---|---|
| With zinc(II) chloride |
- 139481-72-4
2-Ethoxy-1-[[2'-(N-triphenylmethyltetrazol-5-yl)-biphenyl-4-yl]methyl]benzimidazole-7-carboxylic acid
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
- 170791-09-0
cilexetil trityl candesartan
| Conditions | Yield |
|---|---|
| With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In tetrahydrofuran at 20 - 65℃; for 6h; Product distribution / selectivity; | 100% |
| With potassium carbonate In ISOPROPYLAMIDE at 60℃; for 4h; | 98% |
| With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 4h; Temperature; Flow reactor; Alkaline conditions; Large scale; | 96% |
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
- 1307853-85-5
1-{[(cyclohexyloxy)carbonyl]oxy}ethyl 1-({4-[2-(1-benzyl-1H-1,2,3,4-tetrazol-5-yl)phenyl]phenyl}methyl)-2-ethoxy-1H-1,3-benzodiazole-7-carboxylate
| Conditions | Yield |
|---|---|
| With potassium carbonate In N,N-dimethyl-formamide at 65℃; for 4h; | 100% |
| With potassium carbonate In N,N-dimethyl-formamide at 65℃; for 4h; Time; Temperature; | 100% |
| With potassium carbonate In N,N-dimethyl-formamide at 60 - 65℃; for 2 - 3h; |
- 632322-61-3
1-((2'-cyano-[1,1'-biphenyl]-4-yl)methyl)-2-ethoxy-1H-benzo[d]imidazole-7-carboxylic acid
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
- 632322-62-4
2-ethoxy-1-[(2'-cyanobiphenyl-4-yl)methyl]-1H-benzimidazole-7-carboxylicacid-1-[[(cyclohexyloxy)carbonyl]oxy]ethyl ester
| Conditions | Yield |
|---|---|
| Reflux; | 97.43% |
| With potassium carbonate In N,N-dimethyl acetamide at 60℃; for 3h; Product distribution / selectivity; | 64% |
- 1621527-49-8
(R)-3-((tert-butoxycarbonyl)amino)-4-(5'-chloro-2'-fluoro-[1,1-biphenyl]-4-yl)butanoic acid
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
| Conditions | Yield |
|---|---|
| With caesium carbonate In N,N-dimethyl-formamide at 0 - 23℃; for 22.5h; Cooling with ice; | 97% |
- 761404-85-7
4-(1-hydroxy-1-methylethyl)-2-propyl-1-(4-(2-(1-(triphenylmethyl)tetrazol-5-yl)phenyl)phenyl)methylimidazole-5-carboxylic acid
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
- 1337980-10-5
1-{[(cyclohexyloxy)carbonyl]oxy}ethyl 4-(2-hydroxypropan-2-yl)-2-propyl-1-({2'-[1-(triphenylmethyl)-1H-1,2,3,4-tetrazol-5-yl]-[1,1'-biphenyl]-4-yl}methyl)-1H-imidazole-5-carboxylate
| Conditions | Yield |
|---|---|
| With potassium carbonate; potassium iodide In N,N-dimethyl acetamide at 70℃; for 2h; | 95% |
- 99464-83-2
1-chloroethyl cyclohexyl carbonate
- 1307853-85-5
1-{[(cyclohexyloxy)carbonyl]oxy}ethyl 1-({4-[2-(1-benzyl-1H-1,2,3,4-tetrazol-5-yl)phenyl]phenyl}methyl)-2-ethoxy-1H-1,3-benzodiazole-7-carboxylate
| Conditions | Yield |
|---|---|
| With potassium carbonate | 94% |
| Conditions | Yield |
|---|---|
| With potassium carbonate In N,N-dimethyl-formamide at 65℃; for 4h; | 93% |
1-Chloroethyl cyclohexyl carbonate Chemical Properties
Empirical Formula: C9H15ClO3
Molecular Weight: 206.6666g/mol
Structure of 1-Chloroethyl cyclohexyl carbonate (CAS NO.99464-83-2):
Index of Refraction: 1.464
Molar Refractivity: 50.05 cm3
Molar Volume: 181.3 cm3
Polarizability: 19.84×10-24cm3
Surface Tension: 35.1 dyne/cm
Density: 1.13 g/cm3
Flash Point: 115.6 °C
Enthalpy of Vaporization: 52.29 kJ/mol
Boiling Point: 283.9 °C at 760 mmHg
Vapour Pressure: 0.00307 mmHg at 25°C
Product Categories: CARBONATES;INTERMEDIATESOF;(intermediate of candesartan cilexetil);Intermediates of Candesartan;Candesartan Cilexatil
1-Chloroethyl cyclohexyl carbonate Safety Profile
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
1-Chloroethyl cyclohexyl carbonate Specification
1-Chloroethyl cyclohexyl carbonate , its cas register number is 99464-83-2. It also can be called Carbonic acid, 1-chloroethyl cyclohexyl ester .
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