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1-Chloroethyl Isopropyl Carbonate
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Name

1-Chloroethyl Isopropyl Carbonate

 EINECS N/A
CAS No. 98298-66-9 Density 1.114 g/cm>3
PSA 35.53000 LogP 2.13280
Solubility N/A Melting Point N/A
Formula C6H10ClO3 Boiling Point 164.31 °C at 760 mmHg
Molecular Weight 166.605 Flash Point 55.181 °C
Transport Information N/A Appearance Colorless and transparent liquid
Safety 16-36/37/39 Risk Codes 10-34
Molecular Structure Molecular Structure of 98298-66-9 (1-Chloroethyl isopropyl carbonate) Hazard Symbols N/A
Synonyms

1-(Isopropyloxycarbonyloxy)ethylchloride;Isopropyl 1-chloroethyl carbonate;a-Chloroethyl isopropyl carbonate;

Article Data 30

1-Chloroethyl Isopropyl Carbonate Synthetic route

50893-53-3

carbonochloridic acid 1-chloro-ethyl ester

67-63-0

isopropyl alcohol

98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

Conditions
ConditionsYield
With pyridine at -78 - 25℃;99%
With pyridine at -78℃;99%
With pyridine In dichloromethane at -78 - 20℃;97%
50893-53-3

carbonochloridic acid 1-chloro-ethyl ester

98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

75-44-5

phosgene

75-07-0

acetaldehyde

67-63-0

isopropyl alcohol

98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

Conditions
ConditionsYield
Stage #1: phosgene; acetaldehyde
Stage #2: isopropyl alcohol With pyridine
98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

84089-73-6, 91508-00-8

1-iodoethyl isopropyl carbonate

Conditions
ConditionsYield
With tetrabutylammomium bromide; sodium iodide; calcium chloride In ethyl acetate for 3h; Reflux;95%
With sodium iodide In acetonitrile at 50℃; for 6h;90%
With 18-crown-6 ether; sodium iodide In benzene for 12h; Heating;85%

7-[5,6-difluoro-8-(methylamino)-4-[(3aS,6aS)-5-methyl-2,3,3a,4,6,6a-hexahydropyrrolo[2,3-c]pyrrol-1-yl]-9H-pyrido[2,3-b]indol-3-yl]-4-oxoquinolizine-3-carboxylic acid

98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

1-isopropoxycarbonyloxyethyl 7-[5,6-difluoro-8-(methylamino)-4-[(3aS,6aS)-5-methyl-2,3,3a,4,6,6a-hexahydropyrrolo[2,3-c]pyrrol-1-yl]-9H-pyrido[2,3-b]indol-3-yl]-4-oxoquinolizine-3-carboxylate

Conditions
ConditionsYield
Stage #1: 7-[5,6-difluoro-8-(methylamino)-4-[(3aS,6aS)-5-methyl-2,3,3a,4,6,6a-hexahydropyrrolo[2,3-c]pyrrol-1-yl]-9H-pyrido[2,3-b]indol-3-yl]-4-oxoquinolizine-3-carboxylic acid With potassium carbonate In dimethyl sulfoxide at 20℃; for 0.5h;
Stage #2: 1-(isopropoxycarbonyloxy)ethyl chloride In dimethyl sulfoxide at 20℃; for 15.5h;		90.4%
1174039-19-0

(R)-7-[3-tertbutoxycarbonylamino-4-(2,4,5-tri-fluorophenyl)butyryl]-3-trifluoromethyl-5,6,7,8-tetrahydro-imidazo[1,5-a]pyrazine-1-carboxylic acid

98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

(R)-7-[3-amino-4-(2,4,5-trifluorophenyl)butyryl]-3-trifluoromethyl-5,6,7,8-tetrahydroimidazo[1,5-a]pyrazine-1-carboxylic acid isopropoxycarbonyloxy ethyl ester

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 65℃; for 2h; In a sealed tube;85.3%
98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

104483-30-9

1-bromoethyl isopropyl carbonate

Conditions
ConditionsYield
With tetrabutylammomium bromide; hydrogen bromide82%
With tetrabutylammomium bromide; hydrogen bromide at 85℃; for 6h; Yield given;
98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

60846-23-3

cefotaxime sodium salt

1-(isopropoxycarbonyloxy)ethyl 7β-<2-(2-aminothiazol-4-yl)-(Z)-methoxyiminoacetamido>-3-acetoxymethyl-3-cephem-4-carboxylate

Conditions
ConditionsYield
With tetra(n-butyl)ammonium hydrogensulfate In N,N-dimethyl-formamide at 40 - 45℃; for 18h;82%
98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

Sodium; (6R,7R)-7-{2-(2-amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-8-oxo-3-vinyl-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

1-(ispropyloxycarbonyloxy)ethyl 7β-<2-(2-aminothiazol-4-yl)-(Z)-methoxyiminoacetamido>-3-vinyl-3-cephem-4-carboxylate

Conditions
ConditionsYield
With tetra(n-butyl)ammonium hydrogensulfate In N,N-dimethyl-formamide for 18h;81%

raltegravir potassium

98298-66-9

1-(isopropoxycarbonyloxy)ethyl chloride

1538603-91-6

1-((4-((4-fluorobenzyl)carbamoyl)-1-methyl-2-(2-(5-methyl-1,3,4-oxadiazole-2-carboxamido)propan-2-yl)-6-oxo-1,6-dihydropyrimidin-5-yl)oxy)ethyl isopropyl carbonate

Conditions
ConditionsYield
With 18-crown-6 ether; potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 60℃; for 4h;74%

1-Chloroethyl Isopropyl Carbonate Chemical Properties

The MF of 1-Chloroethyl Isopropyl Carbonate(98298-66-9): C6H11ClO3
The MW of 1-Chloroethyl Isopropyl Carbonate(98298-66-9): 166.6
bp: 70 °C at 15mmHg
Density: 1.113 g/cm3 
Flash Point: 55.2 °C 
Boiling Point: 164.3 °C at 760 mmHg 
Index of Refraction: 1.423 
Categories: CARBONATES;(intermediate of cefpodoxime proxetil)
Synonyms: 1-CHLOROETHYL ISOPROPYL CARBONATE;CARBONIC ACID 1-CHLOROETHYL ISOPROPYL ESTER;JCC-1;1-CHLOROETHYL ISOPROPYL CARBONATE (JCC-1)(INTERMEDIATE OF CEFPODOXIME PROXETIL (BANAN));1-chloroethyl isopropyl carbonate (intermediate of cefpodoxime proxetil);1-Chloroethyl Isopropyl Carbonate (JCC-1);1 CHLORO ETHYL ISPPROPYL CARBONATE (CEIC);Carbonic acid, 1-chloroethyl-, 1-methyl-, ethyl ester
The Structure of 1-Chloroethyl Isopropyl Carbonate(98298-66-9):

1-Chloroethyl Isopropyl Carbonate Safety Profile

Risk Statements: 10-34
10:  Flammable 
34:  Causes burns 
Safety Statements: 16-36/37/39
16:  Keep away from sources of ignition - No smoking 
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection
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