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Name	1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine	EINECS	227-383-9
CAS No.	5815-08-7	Density	0.844
PSA	15.71000	LogP	1.20830
Solubility	N/A	Melting Point	N/A
Formula	C9H22 N2 O	Boiling Point	50-55 °C15 mm Hg(lit.)
Molecular Weight	174.286	Flash Point	41 ºC
Transport Information	UN 1993	Appearance	Clear pale yellow liquid
Safety	1901973	Risk Codes	R10;R36/37/38
Molecular Structure		Hazard Symbols
Synonyms	Methanediamine,1-tert-butoxy-N,N,N',N'-tetramethyl- (7CI,8CI);1-(1,1-Dimethylethoxy)-N,N,N',N'-tetramethylmethanediamine;1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine;Bis(dimethylamino)-tert-butoxymethane; Bis(dimethylamino)methyl tert-butylether; Bredereck's reagent; C-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine;t-Butoxybis(dimethylamino)methane; tert-Butoxybis(dimethylamino)methane;tert-Butoxymethylenebis(dimethylamine)	Article Data	1

1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine Synthetic route

: 865-47-4
potassium tert-butylate

: 2013-91-4
N,N,N',N'-tetramethylformamidinium methyl sulfate

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

Conditions

Conditions	Yield
In diethyl ether for 1h;	67%

: 2214-82-6
Bis(dimethylamino)acetonitrile

: 865-47-4
potassium tert-butylate

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

Conditions

Conditions	Yield
In diethyl ether

: 865-47-4
potassium tert-butylate

: N,N,N',N'-tetramethylformamidinium hexafluorophosphate

A: 5762-56-1
tris(dimethylamino)methane

B: 5815-08-7
tert-Butoxybis(dimethylamino)methane

C: 36805-97-7
N,N-dimethylformamide di-tert-butyl acetal

Conditions

Conditions	Yield
In tetrahydrofuran at 50℃; for 1h;

: 865-47-4
potassium tert-butylate

: 2013-91-4
N,N,N',N'-tetramethylformamidinium methyl sulfate

A: 5762-56-1
tris(dimethylamino)methane

B: 5815-08-7
tert-Butoxybis(dimethylamino)methane

C: 36805-97-7
N,N-dimethylformamide di-tert-butyl acetal

Conditions

Conditions	Yield
In tetrahydrofuran at 60℃; for 1h;

: 865-47-4
potassium tert-butylate

: 3218-35-7
N,N,N',N'-Tetramethylformamidinium-(p-toluolsulfonat)

A: 5762-56-1
tris(dimethylamino)methane

B: 5815-08-7
tert-Butoxybis(dimethylamino)methane

C: 36805-97-7
N,N-dimethylformamide di-tert-butyl acetal

Conditions

Conditions	Yield
In tetrahydrofuran at 50℃; for 1h;

: 5762-56-1
tris(dimethylamino)methane

: 36805-97-7
N,N-dimethylformamide di-tert-butyl acetal

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

Conditions

Conditions	Yield
at 20℃; Product distribution / selectivity;

: 865-47-4
potassium tert-butylate

: N,N,N',N'-tetramethylformamidinium hexafluorophosphate

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

Conditions

Conditions	Yield
In tetrahydrofuran at 20 - 60℃; for 4.5h; Inert atmosphere;

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

: 81614-72-4
5-(2,4-difluorophenoxy)-6-nitroindan

: 82505-46-2
[6-(2,4-Difluoro-phenoxy)-5-nitro-indan-(1E)-ylidenemethyl]-dimethyl-amine

Conditions

Conditions	Yield
at 155 - 160℃; for 2h;	100%

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

: 632365-56-1
benzyl 3-phenoxyphenyl ketone

: 632365-57-2
C23H21NO2

Conditions

Conditions	Yield
In toluene at 20 - 60℃; for 16h;	100%

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

: 325708-09-6
7-Methyl-4-nitrobenzo[b]furan

: 603305-64-2
N,N-[dimethyl] (2-(4-nitrobenzofur-7-yl)vinyl)amine

Conditions

Conditions	Yield
for 0.666667h; Heating / reflux;	100%
for 0.666667h; Heating / reflux;	100%

1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine Chemical Properties

Molecular Structure:

Molecular Formula: C₉H₂₂N₂O
Molecular Weight: 174.2838
IUPAC Name: N,N,N',N'-Tetramethyl-1-[(2-methylpropan-2-yl)oxy]methanediamine
Synonyms of 1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine (CAS NO.5815-08-7): EINECS 227-383-9 ; T-Butoxybis(dimethylamino)methane ; tert-Butoxybis(dimethylamino)methane ; brederecks reagent ; Bredereck's reagent ; Butoxybis(dimethylamino)methane ; tert-Butoxybis(dimethylamino)methane, 85+% ; Methanediamine, 1-(1,1-dimethylethoxy)-N,N,N,N-tetramethyl- ; tert-Butoxy bis(dimethylamino)methane (brederecks reagent)
CAS NO: 5815-08-7
Index of Refraction: 1.445
Molar Refractivity: 52.85 cm³
Molar Volume: 198.3 cm³
Surface Tension: 27.3 dyne/cm
Density: 0.878 g/cm³
Flash Point: 35.2 °C
Enthalpy of Vaporization: 41.32 kJ/mol
Boiling Point: 176.9 °C at 760 mmHg
Vapour Pressure of 1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine (CAS NO.5815-08-7): 1.07 mmHg at 25°C

1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine Safety Profile

Hazard Codes of 1-tert-Butoxy-N,N,N',N'-tetramethylmethanediamine (CAS NO.5815-08-7): Irritant Xi,F
Risk Statements: 10-36/37/38
R10: Flammable.
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
RIDADR: UN 1993 3/PG 3
WGK Germany: 3
F: 10
HazardClass: 3
PackingGroup: III

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