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Cas Database |
| Name |
2,4-Dichlorophenylacetonitrile |
EINECS | 228-621-4 |
| CAS No. | 6306-60-1 | Density | 1.333 g/cm3 |
| PSA | 23.79000 | LogP | 3.05948 |
| Solubility | N/A | Melting Point |
58-61 °C(lit.) |
| Formula | C8H5Cl2N | Boiling Point | 286.9 °C at 760 mmHg |
| Molecular Weight | 186.04 | Flash Point | 124 °C |
| Transport Information | N/A | Appearance | white to light yellow crystal powder |
| Safety | 26-36/37/39 | Risk Codes | 36/37/38-20/21/22 |
| Molecular Structure |
|
Hazard Symbols |
 Xi, Xn
|
| Synonyms |
Acetonitrile,(2,4-dichlorophenyl)- (6CI,7CI,8CI);2,4-Dichlorobenzyl cyanide;2-(2,4-Dichlorophenyl)acetonitrile;NSC 22988; |
Article Data | 23 |
2,4-Dichlorophenylacetonitrile Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With tetrabutylammomium bromide In water; 1,2-dichloro-ethane at 70℃; for 5h; | 88.1% |
| With sodium iodide In methanol for 6h; Finkelstein reaction; Reflux; | 87% |
| With polyethylene glycol functionalized magnetic dicationic ionic liquid In water for 1.25h; Reflux; Green chemistry; | 84% |
- 877468-98-9
2,4-dichloro-1-(methoxymethoxy)methyl benzene
- 10442-39-4
tetra-n-butylammonium cyanide
- 6306-60-1
2,4-Dichlorophenylacetonitrile
Conditions
| Conditions | Yield |
|---|---|
| With phosphotungstic acid at 130 - 142℃; for 0.05h; Microwave irradiation; Ionic liquid; chemoselective reaction; | 89% |
| With 1-(n-butyl)-3-methylimidazolium tetrachloroindate at 135 - 140℃; for 0.0916667h; Microwave irradiation; Neat (no solvent); chemoselective reaction; | 82% |
| With 1-methyl-3H-imidazolium nitrate at 135 - 140℃; for 0.075h; Microwave irradiation; | 82% |
- 19719-28-9
2,4-dichlorophenylacetic acid
- 6306-60-1
2,4-Dichlorophenylacetonitrile
Conditions
| Conditions | Yield |
|---|---|
| With sodium azide; TEA; triethylphosphine; (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane; dimethyl sulfoxide at 0℃; for 30h; | 92% |
- 773837-37-9
sodium cyanide
- 20443-99-6
2,4-dichlorobenzyl bromide
- 6306-60-1
2,4-Dichlorophenylacetonitrile
Conditions
| Conditions | Yield |
|---|---|
| In ethanol; water | 93% |
| With silica-coated Fe3O4 nanoparticles-functionalized polycalix[4]resorcinarene In water at 90℃; for 0.333333h; Green chemistry; | 80% |
- 1058649-24-3
2,4-dichloro-1-[(ethoxymethoxy)methyl]benzene
- 10442-39-4
tetra-n-butylammonium cyanide
- 6306-60-1
2,4-Dichlorophenylacetonitrile
Conditions
| Conditions | Yield |
|---|---|
| With 1-(n-butyl)-3-methylimidazolium tetrachloroindate at 135 - 140℃; for 0.0916667h; Microwave irradiation; Neat (no solvent); chemoselective reaction; | 80% |
Conditions
| Conditions | Yield |
|---|---|
| With ethanol |
Conditions
| Conditions | Yield |
|---|---|
| In dimethyl sulfoxide at 40 - 50℃; for 5h; Yield given; |
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: PBr3 / CH2Cl2 View Scheme | |
| Multi-step reaction with 2 steps 1: phosphorus tribromide / dichloromethane; N,N-dimethyl-formamide / 80 °C 2: ethanol; water View Scheme | |
| Multi-step reaction with 3 steps 1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 - 20 °C 2: tris(pentafluorophenyl)borate / 1,2-dichloro-ethane / 0.08 h / 20 °C / Glovebox; Schlenk technique 3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 20 °C View Scheme |
Conditions
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 18h; |
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: SOCl2, (PhCO)2O2 View Scheme | |
| Multi-step reaction with 2 steps 1: 2,2'-azobis(isobutyronitrile); chlorine / 3 h / 110 °C 2: tetrabutylammomium bromide / 1,2-dichloro-ethane; water / 5 h / 70 °C View Scheme |
2,4-Dichlorophenylacetonitrile Chemical Properties
2,4-Dichlorophenylacetonitrile is also named as 2-(2,4-Dichlorophenyl)acetonitrile;2,4-Dichlorobenzeneacetonitrile;Acetonitrile, (2,4-dichlorophenyl)-;2,4-dichloro cyanobenzene;2,4-Dichlorophenylacetonitrile,98%,and so on.2,4-Dichlorophenylacetonitrile is usually white powder.
CAS: 6306-60-1
Molecular Formula: C8H5Cl2N
Molecular Weight: 186.04
EINECS: 228-621-4
Molecular structure:
Melting point: 58-61 °C(lit.)
Flash point: 176 °C
BRN: 2047688
2,4-Dichlorophenylacetonitrile Uses
2,4-Dichlorophenylacetonitrile is usually used as organic intermediates forthe synthetic of pesticides and medicine.
2,4-Dichlorophenylacetonitrile Safety Profile
Hazard Codes: Xi,Xn
Risk Statements: 36/37/38-20/21/22
Safety Statements: 26-36/37/39
RIDADR: 3276
WGK Germany: 1
HazardClass: 6.1
PackingGroup: III
Risk Statements: 36/37/38-20/21/22
Safety Statements: 26-36/37/39
RIDADR: 3276
WGK Germany: 1
HazardClass: 6.1
PackingGroup: III
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2,4-Dichlorophenylacetonitrile
