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Basic Information
| CAS No.: | 766-51-8 |
|---|---|
| Name: | 2-Chloroanisole |
| Molecular Structure: | |
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|
|
| Formula: | C7H7ClO |
| Molecular Weight: | 142.585 |
| Synonyms: | Anisole,o-chloro- (6CI,7CI,8CI);1-Chloro-2-methoxybenzene;2-Chloromethoxybenzene;2-Chlorophenol methyl ether;2-Methoxy-1-chlorobenzene;2-Methoxyphenyl chloride;NSC 155175;o-Chloroanisole;o-Chloromethoxybenzene;o-Chlorophenyl methyl ether;o-Methoxychlorobenzene; |
| EINECS: | 212-167-9 |
| Density: | 1.137 g/cm3 |
| Melting Point: | -27oC |
| Boiling Point: | 198.5 °C at 760 mmHg |
| Flash Point: | 70.8 °C |
| Solubility: | 0.49g/L(25 oC) |
| Appearance: | clear light yellow liquid |
| Safety: | 24/25 |
| PSA: | 9.23000 |
| LogP: | 2.34860 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With N-chloro-succinimide; copper(l) chloride In acetonitrile at 80℃; for 18h; | 97% |
| With N-chloro-succinimide In acetonitrile at 80℃; for 24h; | 90% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2-monochlorophenol With potassium carbonate In acetone for 0.25h; Stage #2: dimethyl sulfate In acetone for 10h; Reflux; | 96% |
| With sodium hydroxide In water at 90℃; for 0.5h; | 84.6% |
| With potassium hydroxide at 100℃; | |
| With sodium hydroxide at 100℃; | |
| With lithium hydroxide In tetrahydrofuran for 1h; Ambient temperature; Yield given; |
Conditions
| Conditions | Yield |
|---|---|
| With lithium chloride In N,N-dimethyl acetamide at 30℃; Pt anode, graphite cathode, sintered glass diaphragm, 1.3 V vs. SCE, 965 C; | A 95.8% B 2.8% |
| With aluminum oxide; sodium chlorite; water; manganese(III) acetylacetonate In dichloromethane at 25℃; for 0.583333h; Product distribution; other solvents, inorganic support materials, times and temperatures, also without H2O; | A 85% B 8% |
| With chlorine; natural kaolinitic clay In tetrachloromethane for 2h; Heating; | A 85% B 9% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium carbonate In dichloromethane at 20℃; | 95% |
| With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 51% |
| With sodium hydroxide In N,N-dimethyl acetamide at 25℃; Rate constant; | |
| With potassium carbonate at 130℃; |
Conditions
| Conditions | Yield |
|---|---|
| With nickel dichloride In N,N-dimethyl-formamide at 170℃; for 0.0833333h; microwave irradiation; | 94% |
| With CuCl-alumina In various solvent(s) at 150℃; for 24h; | 54 % Chromat. |
| With hydrogenchloride; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; oxygen In water; acetonitrile at 25℃; for 1.5h; Irradiation; | 53 %Chromat. |
- 14503-45-8
3-chloro-4-methoxybenzyl alcohol
- 766-51-8
2-Chloroanisole
Conditions
| Conditions | Yield |
|---|---|
| With chlorobis(cyclooctene)-iridium(I) dimer; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; lithium chloride In water; 1,3,5-trimethyl-benzene at 170℃; for 18h; Schlenk technique; Inert atmosphere; | 91% |
Conditions
| Conditions | Yield |
|---|---|
| With layered double hydroxide - supported L-methionine at 180℃; for 6h; Autoclave; chemoselective reaction; | 90% |
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide for 0.0583333h; microwave irradiation; | 85% |
| With dimanganese decacarbonyl at 180℃; for 1h; | 2% |
| With leucine intercalated Mg-Al layered double hydorxide at 180℃; for 6h; Autoclave; Green chemistry; chemoselective reaction; | 86 %Chromat. |
- 14596-60-2
N-chloro-N-(4-methylphenyl)acetamide
- 100-66-3
methoxybenzene
A
- 623-12-1
4-chloromethoxybenzene
B
- 766-51-8
2-Chloroanisole
C
- 18931-78-7
N-(2-chloro-4-methylphenyl)acetamide
D
- 103-89-9
4-Methylacetanilide
Conditions
| Conditions | Yield |
|---|---|
| at 110℃; for 12h; Mechanism; Orton Haloaniline Rearrangement; Inert atmosphere; Darkness; | A 82% B n/a C n/a D 87% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With 18-crown-6 ether; potassium carbonate at 150℃; for 2h; | 85% |
- 766-51-8
2-Chloroanisole
Conditions
| Conditions | Yield |
|---|---|
| In dimethyl sulfoxide Ambient temperature; | 84% |
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2-Chloroanisole
Chemistry
The Molecular formula of 2-Chloroanisole(766-51-8): C7H7ClO
The Molecular Weight of 2-Chloroanisole(766-51-8): 142.58
The Molecular Structure of 2-Chloroanisole(766-51-8):
EINECS: 212-167-9
Boiling Point: 198.5 °C at 760 mmHg
Flash Point: 70.8 °C
Index of Refraction: 1.515
Molar Refractivity: 37.82 cm3
Molar Volume: 125.3 cm3
Polarizability: 14.99 10-24 cm3
Surface Tension: 32.6 dyne/cm
Density: 1.137 g/cm3
Enthalpy of Vaporization: 41.69 kJ/mol
Vapour Pressure: 0.506 mmHg at 25°C
BRN: 2042179
IUPAC Name: 1-chloro-2-methoxybenzene
Synonyms: 1-chloro-2-methoxy-benzen;anisole,o-chloro-;benzene,1-chloro-2-methoxy-;2-chloromethoxybenzene;2-Chlorophenol methyl ether;o-Chloromethoxybenzene;o-Chlorophenyl methyl ether; Anisole, o-chloro-;
The Molecular Weight of 2-Chloroanisole(766-51-8): 142.58
The Molecular Structure of 2-Chloroanisole(766-51-8):
EINECS: 212-167-9
Boiling Point: 198.5 °C at 760 mmHg
Flash Point: 70.8 °C
Index of Refraction: 1.515
Molar Refractivity: 37.82 cm3
Molar Volume: 125.3 cm3
Polarizability: 14.99 10-24 cm3
Surface Tension: 32.6 dyne/cm
Density: 1.137 g/cm3
Enthalpy of Vaporization: 41.69 kJ/mol
Vapour Pressure: 0.506 mmHg at 25°C
BRN: 2042179
IUPAC Name: 1-chloro-2-methoxybenzene
Synonyms: 1-chloro-2-methoxy-benzen;anisole,o-chloro-;benzene,1-chloro-2-methoxy-;2-chloromethoxybenzene;2-Chlorophenol methyl ether;o-Chloromethoxybenzene;o-Chlorophenyl methyl ether; Anisole, o-chloro-;
Safety Profile
The Safety Statements information of 2-Chloroanisole(766-51-8):
24/25: Avoid contact with skin and eyes
WGK Germany: 3
24/25: Avoid contact with skin and eyes
WGK Germany: 3