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100-66-3

Basic Information
CAS No.: 100-66-3
Name: Anisole
Molecular Structure:
Molecular Structure of 100-66-3 (Anisole)
Formula: C7H8O
Molecular Weight: 108.14
Synonyms: Phenylmthyl ether;Ether, methyl phenyl-;Benzene, methoxy-;Anizol;Methyl phenyl ether;Anisole , Natural;Methoxy benzene;Anisol;Phenoxymethane;Methoxybenzene;Phenyl methyl ether;Anisole [UN2222] [Flammable liquid];Phenol methyl ether;Benzene,methoxy-;
EINECS: 202-876-1
Density: 0.953 g/cm3
Melting Point: -37 °C
Boiling Point: 153.599 °C at 760 mmHg
Flash Point: 44.454 °C
Solubility: Water: 1.6 g/L (20 °C)
Appearance: Clear straw colored liquid
Hazard Symbols: HarmfulXn
Risk Codes: 10-38-20
Safety: 37/39-26-16-24/25
Transport Information: UN 2222 3/PG 3
PSA: 9.23000
LogP: 1.69520
Synthetic route
74-88-4

methyl iodide

108-95-2

phenol

100-66-3

methoxybenzene

Conditions
ConditionsYield
With potassium hydroxide; acyclic polyethylene oxides In dichloromethane; water for 0.5h;100%
With aluminum oxide; potassium fluoride In N,N-dimethyl-formamide for 1h; Product distribution; Ambient temperature; other phenols and alcohols, other alkylating agents, other reagents and solvents, var. time;100%
With potassium hydroxide; Aliquat 336 at 20℃; for 5h;99%
17743-22-5

5-(2-methoxy-phenoxy)-1-phenyl-1H-tetrazole

A

5097-82-5

1-phenyl-5-hydroxytetrazole

B

100-66-3

methoxybenzene

Conditions
ConditionsYield
With hydrazine hydrate; palladium on activated charcoal In ethanol; water; benzene for 1.83333h; Ambient temperature;A n/a
B 100%
palladium on activated charcoal In ethanol; benzene Mechanism; Product distribution; various reagents, temperatures and reaction times;
With sodium hypophosphite; palladium on activated charcoal In ethanol; benzene at 80℃; Relative steady-state rates, relative extrapolated intercepts;
104-92-7

1-bromo-4-methoxy-benzene

100-66-3

methoxybenzene

Conditions
ConditionsYield
With hydrogen In methanol at 70℃; under 750.075 Torr; for 0.333333h;100%
With LiCrH4*2LiCl*2THF In tetrahydrofuran at 25℃; for 12h;98%
Stage #1: 1-bromo-4-methoxy-benzene With n-butyllithium In tetrahydrofuran; hexane at -58℃; for 0.000861111h;
Stage #2: With methanol In tetrahydrofuran; hexane at -58℃; for 0.000436111h;
92%
2398-37-0

3-methoxyphenyl bromide

100-66-3

methoxybenzene

Conditions
ConditionsYield
With tetraphenyldisilane; cesium fluoride In acetonitrile at 100℃; for 0.0833333h;100%
With tetrakis(triphenylphosphine) palladium(0); formaldehyd; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h;85%
With N,N,N,N,-tetramethylethylenediamine; C39H46IrN4 In acetonitrile at 45℃; for 48h; Sealed tube; Glovebox; Inert atmosphere;80%
696-62-8

para-iodoanisole

100-66-3

methoxybenzene

Conditions
ConditionsYield
With lithium aluminium tetrahydride; di-tert-butyl peroxide In tetrahydrofuran for 1.5h; Irradiation;100%
With potassium phosphate In N,N-dimethyl-formamide; cyclohexanol at 110℃; for 12h;96%
With formaldehyd; palladium diacetate; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h;95%
2886-59-1

1-methoxycyclohexa-1,4-diene

100-66-3

methoxybenzene

Conditions
ConditionsYield
With pyridinium chlorochromate In dichloromethane at 25℃; for 1h;100%
In acetone at 0℃; for 1h;90%
With manganese(IV) oxide In methyl cyclohexane at 70℃; for 16h;43%
With tris(1,10-phenantholine)iron(III) perchlorate In acetonitrile at -30℃; Rate constant; other reagent;
616-38-6

carbonic acid dimethyl ester

108-95-2

phenol

100-66-3

methoxybenzene

Conditions
ConditionsYield
N,N,N',N'-tetrabutyl-N''-methylguanidine at 160℃; for 4.5h;100%
N,N,N',N'-tetrabutyl-N''-methylguanidine at 160℃; for 4.5h; Product distribution; other catalysts, other reaction conditions, other phenols;100%
With tetrabutylammomium bromide; potassium carbonate at 93℃; for 5h;99%
100-67-4

potassium phenolate

74-88-4

methyl iodide

A

100-66-3

methoxybenzene

B

KI

KI

Conditions
ConditionsYield
acyclic polyethylene oxides In benzene at 25℃;A 100%
B n/a
99506-45-3

4-methoxyphenyl(m-carboran-9-yl)iodonium tetrafluoroborate

7647-14-5

sodium chloride

A

17157-02-7

9-iodo-m-carborane

B

17819-85-1

9-chloro-m-carborane

C

696-62-8

para-iodoanisole

D

100-66-3

methoxybenzene

Conditions
ConditionsYield
In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaCl, water and chloroform was vigorously stirred under reflux at 56°C, 2-2.5 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC;A 0%
B 100%
C 100%
D 0%
578-57-4

2-bromoanisole

100-66-3

methoxybenzene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); formaldehyd; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h;99%
With butyl magnesium bromide; zirconocene dichloride for 12h; Ambient temperature;98%
With lithium aluminium tetrahydride In 1,2-dimethoxyethane at 35℃; for 4h; ultrasonic acceleration of reduction;98%
529-28-2

4-iodoanisol

100-66-3

methoxybenzene

Conditions
ConditionsYield
With triethylamine In water at 25℃; for 1h; UV-irradiation;99%
With formaldehyd; palladium diacetate; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h;98%
With potassium phosphate In N,N-dimethyl-formamide; cyclohexanol at 110℃; for 12h;95%
874-90-8

4-methoxybenzonitrile

100-66-3

methoxybenzene

Conditions
ConditionsYield
With lithium borohydride; C22H19F3N4NiO2S In tetrahydrofuran at 70℃; for 24h; Reagent/catalyst;99%
With lithium borohydride; C30H21F6N2NiO2P In tetrahydrofuran at 70℃; for 3h; Reagent/catalyst; Concentration; Temperature; Time; Schlenk technique; Inert atmosphere;89%
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tri-n-butyl phosphite; chlorotriisopropylsilane In ethyl-cyclohexane at 130℃; for 15h; Inert atmosphere;74%
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tri-n-butyl phosphite; chlorotriisopropylsilane In ethylcyclohexane at 130℃; for 15h; Inert atmosphere;74 %Chromat.
With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; ethanol; potassium hexamethylsilazane In toluene at 140℃; for 8h; Inert atmosphere;30 %Chromat.
623-12-1

4-chloromethoxybenzene

100-66-3

methoxybenzene

Conditions
ConditionsYield
With ammonium formate In water at 20℃; for 3h;98%
With isopropyl alcohol; sodium hydroxide at 24.84℃; under 760.051 Torr; for 1h; Inert atmosphere; UV-irradiation;97%
With palladium on ceria; sodium hydroxide In isopropyl alcohol at 40℃; for 18h; Irradiation; Inert atmosphere; Sealed tube;94%
132636-68-1

3-(4-methoxyphenoxy)-1,2-benzisothiazole 1,1-dioxide

A

100-66-3

methoxybenzene

B

81-07-2

saccharin

Conditions
ConditionsYield
With sodium hypophosphite; palladium on activated charcoal In water; benzene for 3h; Heating;A 98%
B n/a
766-85-8

3-methoxy-1-iodobenzene

A

6161-50-8

3,3'-dimethoxybiphenyl

B

100-66-3

methoxybenzene

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 36h; Inert atmosphere;A 1%
B 98%
With 18-crown-6 ether; zinc; 10 percent Pd/C In water; acetone at 20℃; Product distribution; Further Variations:; Catalysts; Reagents; Solvents; Ullmann coupling;
623-12-1

4-chloromethoxybenzene

67-63-0

isopropyl alcohol

100-66-3

methoxybenzene

Conditions
ConditionsYield
With sodium hydroxide at 24.84℃; under 760.051 Torr; for 5h; Inert atmosphere; UV-irradiation; Sealed tube;98%
689-16-7

dimethyl 2-oxo-1,3-propanedisulfonate

108-95-2

phenol

100-66-3

methoxybenzene

Conditions
ConditionsYield
With sodium hydroxide at 40℃; for 6h; also diethyl 2-oxo-1,3-propanedisulfonate; var. reaction time; other alkylating agents;97.2%
77-78-1

dimethyl sulfate

108-95-2

phenol

100-66-3

methoxybenzene

Conditions
ConditionsYield
With potassium hydroxide In 1,4-dioxane for 1.5h;97%
With potassium carbonate In acetone for 0.0833333h; Etherification; methylation; microwave irradiation;92%
With sodium hydroxide; N-butyl-N,N-dimethyl-(α-phenyl)ethylammonium bromide In 1,2-dichloro-ethane for 6h; Heating;85%
623-12-1

4-chloromethoxybenzene

A

2132-80-1

4,4'-Dimethoxybiphenyl

B

100-66-3

methoxybenzene

Conditions
ConditionsYield
With water; triphenylphosphine; sodium iodide; nickel dichloride; zinc In N,N-dimethyl-formamide at 70℃; for 2h; Rate constant; Product distribution; Mechanism; var. organic halides; other solvent; var. temp., and reaction times;A 2.5%
B 96.8%
With potassium hydroxide In water; N,N-dimethyl-formamide at 35℃; for 12h; Ullmann Condensation; Inert atmosphere;A 92%
B 6%
With NaH-t-AmONa-Ni(OAc)2-bpy In tetrahydrofuran at 63℃; for 8h;A 73%
B 16 % Chromat.
36719-69-4

1-(4-Methoxyphenyl)-3,3-diethyl-1-triazene

A

696-62-8

para-iodoanisole

B

100-66-3

methoxybenzene

Conditions
ConditionsYield
With cation exchange resin BioRad AG 50W-X12 (H+); sodium iodide In acetonitrile at 75℃; Product distribution; further solvent: THF, DMSO;A 96%
B 4%
598-99-2

Methyl trichloroacetate

108-95-2

phenol

100-66-3

methoxybenzene

Conditions
ConditionsYield
With 18-crown-6 ether; potassium carbonate at 150℃; for 2h;96%
766-85-8

3-methoxy-1-iodobenzene

100-66-3

methoxybenzene

Conditions
ConditionsYield
With potassium phosphate In N,N-dimethyl-formamide; cyclohexanol at 110℃; for 12h;96%
With formaldehyd; palladium diacetate; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h;85%
With isopropyl alcohol at 20℃; for 18h; UV-irradiation; chemoselective reaction;78%
91-23-6

2-Nitroanisole

100-66-3

methoxybenzene

Conditions
ConditionsYield
With potassium phosphate; dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; palladium(II) acetylacetonate; isopropyl alcohol In 1,4-dioxane at 130℃; for 4h; Time; Reagent/catalyst; Solvent; Inert atmosphere;96%
With potassium phosphate; bis(acetylacetonato)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; isopropyl alcohol In 1,4-dioxane at 130℃; for 4h;96 %Chromat.

triethyl(4-methoxyphenyl)germane

100-66-3

methoxybenzene

Conditions
ConditionsYield
With trifluoromethanesulfonyloxy(triphenylphosphine)gold(I) In 1,4-dioxane at 20℃;96%
7417-18-7

2-methoxyphenethyl alcohol

100-66-3

methoxybenzene

Conditions
ConditionsYield
With 1,10-Phenanthroline; oxygen; copper diacetate; silver nitrate; sodium hydroxide In dimethyl sulfoxide at 140℃; under 3750.38 Torr; for 12h; Autoclave; Green chemistry;96%
67-56-1

methanol

7719-12-2, 52843-90-0

phosphorus trichloride

A

18351-42-3

dimethyl phenylphosphonite

B

7526-26-3

diphenyl methylphosphonate

C

100-66-3

methoxybenzene

Conditions
ConditionsYield
Stage #1: phosphorus trichloride; phenol at 65 - 250℃; for 4h;
Stage #2: methanol at 204 - 260℃; for 2h; Product distribution / selectivity;
A n/a
B 95.6%
C n/a
Stage #1: phosphorus trichloride; phenol at 65 - 250℃; for 4h;
Stage #2: methanol; methyl iodide at 210 - 250℃; Product distribution / selectivity;
A 7.14%
B 92.86%
C n/a
108-86-1

bromobenzene

124-41-4

sodium methylate

100-66-3

methoxybenzene

Conditions
ConditionsYield
copper(I) bromide In methanol; N,N-dimethyl-formamide at 110℃; for 0.75h;95%
copper(I) bromide In methanol for 6h; Product distribution; Mechanism; Rate constant; Heating; by investigating the influence of several reaction parameters (the nature and concentration of the copper catalyst, the cosolvents, the concentration and number of equivalents of the nucleophile, the bromide concentration, the aryl bromide subst. effect;95%
With methanol; Methyl formate; copper(l) chloride at 115℃; for 2h; Reagent/catalyst; Autoclave; Green chemistry;80%
With hemicucurbituril supported [Bmim]Cl In toluene for 9h; Reflux;78%
With ethyl acetate; copper(I) bromide In methanol for 2h; Heating; Yield given;
107-31-3

Methyl formate

696-62-8

para-iodoanisole

124-41-4

sodium methylate

A

121-98-2

methyl 4-methoxybenzoate

B

100-66-3

methoxybenzene

Conditions
ConditionsYield
bis-triphenylphosphine-palladium(II) chloride In dichloromethane at 40℃; under 11250.9 Torr; for 7h;A 95%
B 5%
13509-27-8

methyl phenyl carbonate

100-66-3

methoxybenzene

Conditions
ConditionsYield
dmap at 130℃; for 2h; other catalysts;95%
N,N,N',N'-tetrabutyl-N''-methylguanidine at 110℃; for 1h; Product distribution; other catalysts, other reaction conditions, other aryl methyl carbonates;93 % Chromat.
18412-81-2

dodecyl-dimethylsulphonium iodide

108-95-2

phenol

A

1187-84-4

S-methyl-L-cysteine

B

100-66-3

methoxybenzene

Conditions
ConditionsYield
With potassium hydroxide In water at 70℃; for 5h; pH = 9;A n/a
B 95%
79-03-8

propionyl chloride

100-66-3

methoxybenzene

121-97-1

4-Methoxypropiophenone

Conditions
ConditionsYield
With Noccaea caerulescens extract supported in montmorillonite K10 at 60℃; for 6h; Friedel Crafts acylation; Inert atmosphere; regioselective reaction;100%
With aluminum (III) chloride In dichloromethane at 5 - 20℃; for 2.5h;98%
With benzyltributylammonium tetrachloroferrate at 50℃; for 0.1h; Friedel-Crafts reaction;93%
108-24-7

acetic anhydride

100-66-3

methoxybenzene

100-06-1

1-(4-methoxyphenyl)ethanone

Conditions
ConditionsYield
With polystyrene-bound tetrafluorophenylbis(triflyl)methane In nitromethane at 50℃; for 2h; Friedel-Crafts acylation;100%
With lithium perchlorate at 60℃; for 1h;100%
With Sulfate; zirconium(IV) oxide at 110℃;100%
97-72-3

2-Methylpropionic anhydride

100-66-3

methoxybenzene

2040-20-2

4-methoxyisobutyrophenone

Conditions
ConditionsYield
With hafnium(IV) trifluoromethanesulfonate; lithium perchlorate In nitromethane for 6h; Ambient temperature;100%
With lithium perchlorate at 60℃; for 1.5h;99%
With trifluorormethanesulfonic acid; titanium(IV) chloride tris(trifluoromethanesulfonate) In acetonitrile for 12h; Ambient temperature;90%
64-19-7

acetic acid

100-66-3

methoxybenzene

100-06-1

1-(4-methoxyphenyl)ethanone

Conditions
ConditionsYield
Stage #1: acetic acid; methoxybenzene With trifluoroacetic anhydride In dichloromethane at 20℃; for 0.25h;
Stage #2: With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 1h;
100%
With methanesulfonic acid; pyrographite at 80℃; for 0.333333h; Friedel-Crafts acylation;98%
With aluminum oxide; trifluoroacetic anhydride for 0.166667h; Ambient temperature;96%
638-29-9

n-valeryl chloride

100-66-3

methoxybenzene

1671-76-7

p-Methoxyvalerophenon

Conditions
ConditionsYield
With aluminium trichloride In dichloromethane for 15h; Ambient temperature;100%
(p-MeOC6H4)2BSbCl6 In dichloromethane for 24h; Ambient temperature;88%
With aluminium trichloride In tetrachloromethane at 0℃; for 2h;87%
36854-57-6

2-Phenylbutyryl chloride

100-66-3

methoxybenzene

78423-10-6

1-(4-methoxyphenyl)-2-phenylbutan-1-one

Conditions
ConditionsYield
aluminum (III) chloride at 0 - 20℃; for 2h; Friedel Crafts Acylation;100%
Stage #1: 2-Phenylbutyryl chloride; methoxybenzene With aluminum (III) chloride In carbon disulfide at 10 - 20℃; for 20h; Inert atmosphere; Cooling with ice;
Stage #2: With water In carbon disulfide
94%
With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 2.5h; Friedel-Crafts Acylation;76%
100-66-3

methoxybenzene

93-97-0

benzoic acid anhydride

611-94-9

4-Methoxybenzophenone

Conditions
ConditionsYield
With gallium(III) trichloride; silver hexafluoroantimonate In 1,2-dichloro-ethane for 7h; Heating;100%
With trifluoroacetic acid at 20℃; for 1.5h; Friedel-Crafts Acylation;98%
With lithium perchlorate In nitromethane at 100℃; for 4h;97%
100-66-3

methoxybenzene

586-75-4

4-chlorobenzoyl chloride

54118-75-1

4-bromo-4'-methoxybenzophenone

Conditions
ConditionsYield
aluminum (III) chloride In dichloromethane at 5 - 20℃; for 3h; Friedel Crafts Acylation;100%
With aluminum (III) chloride In dichloromethane at 0℃; for 3h;99%
With aluminum (III) chloride In dichloromethane for 3h;99%
100-66-3

methoxybenzene

104-92-7

1-bromo-4-methoxy-benzene

Conditions
ConditionsYield
With benzyltriphenylphosphonium peroxodisulfate; potassium bromide In acetonitrile for 3.5h; Heating;100%
With Selectfluor; sodium bromide In acetonitrile at 20℃; for 21h;100%
With bis[1-methyl-3-(3-sulfopropyl)imidazolium] hexafluorotitanate; dihydrogen peroxide; sodium bromide In water at 25℃; for 3h; Reagent/catalyst; Concentration; Solvent; Temperature; Green chemistry;100%
100-66-3

methoxybenzene

931-56-6

2-methoxycyclohexane

Conditions
ConditionsYield
With hydrogen; [(norbornadiene)rhodium(I)chloride]2; phosphinated polydiacetylene In n-heptane at 30℃; under 60800 Torr; for 0.7h;100%
With hydrogen; Rh on carbon In methanol at 20℃; under 760.051 Torr; for 1h;100%
With hydrogen In hexane at 24.84℃; under 750.075 Torr; for 3h;100%
100-66-3

methoxybenzene

696-62-8

para-iodoanisole

Conditions
ConditionsYield
With IPy2BF4*2HBF4 In dichloromethane for 0.25h; Ambient temperature;100%
With iodine; n-butyltriphenylphosphonium peroxodisulfate In acetonitrile for 0.5h; Heating;100%
With ammonium iodide; 3-chloro-benzenecarboperoxoic acid for 2h;100%
768-90-1

1-Adamantyl bromide

100-66-3

methoxybenzene

726-94-3

1-(4-methoxyphenyl)adamantane

Conditions
ConditionsYield
With molybdenum hexacarbonyl Sealed tube; regioselective reaction;100%
With potassium carbonate; palladium on activated charcoal at 120℃; for 12h;91%
With palladium 10% on activated carbon; potassium carbonate for 20h; Heating;82.65%
69435-89-8

trimethylsilyl cyclohexanecarboxylate

100-66-3

methoxybenzene

7469-80-9

cyclohexyl 4-methoxyphenyl ketone

Conditions
ConditionsYield
With tetrachlorosilane; 4-(trifluoromethyl)benzoic anhydride; silver perchlorate In dichloromethane for 25h; Ambient temperature;100%
21273-15-4

trimethylsilyl ester of hydrocinnamic acid

100-66-3

methoxybenzene

5739-38-8

1-(4-methoxyphenyl)-3-phenylpropan-1-one

Conditions
ConditionsYield
With SiClO4; 4-(trifluoromethyl)benzoic anhydride; silver perchlorate In dichloromethane for 63h; Ambient temperature;100%
100-66-3

methoxybenzene

84858-88-8

1-(2,3,4,5,6-pentamethylphenyl)butan-1-one

A

13404-83-6

1-(2-methoxyphenyl)butan-1-one

B

700-12-9

pentamethylbenzene,

C

4160-51-4

1-(4-methoxyphenyl)-1-butanone

Conditions
ConditionsYield
trifluoroacetic acid for 5h; Heating;A n/a
B 100%
C n/a
100-66-3

methoxybenzene

882-33-7

diphenyldisulfane

5633-57-8

1-methoxy-4-(phenylsulfanyl)benzene

Conditions
ConditionsYield
With silver hexafluoroantimonate; antimonypentachloride In 1,2-dichloro-ethane for 3h; Heating;100%
With dipotassium peroxodisulfate In trifluoroacetic acid at 20℃; for 16h;89%
Stage #1: diphenyldisulfane With thionyl chloride In 1,2-dichloro-ethane at 5 - 30℃; for 4h;
Stage #2: With aluminum (III) chloride In 1,2-dichloro-ethane at 5 - 10℃; for 1h;
Stage #3: methoxybenzene In 1,2-dichloro-ethane for 4h;
88.5%
With silver hexafluoroantimonate; antimonypentachloride In 1,2-dichloro-ethane for 3h; Product distribution; Heating; effect of Lewis acid and silver salt;
100-66-3

methoxybenzene

79562-11-1

N,N-diacetyl-p-nitrophenylsulphenamide

A

22865-50-5

4-(4-methoxyphenylsulfanyl)nitrobenzene

B

100-06-1

1-(4-methoxyphenyl)ethanone

Conditions
ConditionsYield
With trifluoroacetic acid at 190 - 200℃;A 100%
B 21%
100-66-3

methoxybenzene

108-95-2

phenol

Conditions
ConditionsYield
With aluminium(III) iodide; tetra-(n-butyl)ammonium iodide In cyclohexane for 0.3h; Heating;100%
With water; hydrogen bromide; Aliquat 336 at 105℃; for 5h; Catalytic behavior;96%
With monochloroborane dimethyl sulfide complex In benzene Heating;95%
6223-78-5

2,5-dichloro-2,5-dimethyl hexane

100-66-3

methoxybenzene

51510-70-4

1,2,3,4-tetrahydro-1,1,4,4-tetramethyl-6-methoxynaphthalene

Conditions
ConditionsYield
aluminum (III) chloride at 0℃; for 2h;100%
With aluminium trichloride 1.) RT, 30 min, 2.) reflux, 15 min;86%
With aluminium trichloride Heating;
100-66-3

methoxybenzene

1516-21-8

4-methoxynitrosobenzene

Conditions
ConditionsYield
With nitric oxide; trifluoroacetic anhydride for 0.133333h; Product distribution; Ambient temperature;100%
With hydrogenchloride; 1-(4-(nitrosooxy)butyl)-3-methylimidazolium chloride In water at 0 - 5℃; for 1.08333h; regioselective reaction;88%
With nitrosonium tetrafluoroborate In acetonitrile at 25℃; for 0.5h;87%
4509-90-4

5-bromovaleroyl chloride

100-66-3

methoxybenzene

69287-12-3

5-bromo-1-(4-methoxyphenyl)pentan-1-one

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 2h;100%
With aluminium trichloride Friedel-Crafts acylation;85%
With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 2h; Friedel-Crafts Acylation;
With metallic chloride at 50℃; Friedel-Crafts Acylation;
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Inert atmosphere;
27607-77-8

trimethylsilyl trifluoromethanesulfonate

100-66-3

methoxybenzene

350693-36-6

1,1-diphenyl-3-(trimethylsilyl)-1-(trimethylsilyloxy)prop-2-yne

(1-(4-methoxyphenyl)-3,3-diphenylpropa-1,2-dien-1-yl)trimethylsilane

Conditions
ConditionsYield
In dichloromethane at -78℃; for 3h; Friedel-Crafts reaction;100%
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  • High purity  Anisole supplier CAS: 100-66-3

  • Casno:

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  •  Simagchem Corporation

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    Business Type:Manufacturers

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  • Casno:

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    Anisole CAS No.: 100-66-3 Molecular Formula: C7H8O Molecular Weight: 108.13 Structural formula: A. Physical & Chemical Properties 1.Density:0.995 2.Melting point:-37℃ 3.Boiling point: 154℃ 4.Refractive lndex: 1.516-1.519 5.Solubilit

    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

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     China (Mainland)  |  Contact Details

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    Anisole CAS:100-66-3

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    Product Name Anisole Synonyms Methoxybenzine;Anisole, SuperDry, J&KSeal;Anisole, 99%, SpcDry, Water≤50 ppM (by K.F.), SpcSeal;Anisole ReagentPlus(R), 99%;ANISOL;ANISOLE;METHOXYBENZENE;METHYL PHENY

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     China (Mainland)  |  Contact Details

    Business Type:Other

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Block A of Central Mansion, No.113 of Weiyang Rd, ETDZ, Xi'an, Shaanxi 710016, China

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     China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

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  • Anisole  CAS No.: 100-66-3

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     China (Mainland)  |  Contact Details

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    Address:Room 302, 47 Changping Street, Chaoyang District, Changchun, Jilin Province,China

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     China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

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    1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume

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     China (Mainland)  |  Contact Details

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    Business Type:Other

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15988566987

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0570-4045877

    Address:46# zhongshan road, quzhou zhejiang

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 21 34943721

    Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,

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    Address:hebei

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15821988213

    Address:Dalian Rd 950th

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    Min.Order: 1 Kilogram

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    Clear straw colored liquid Appearance:Clear straw colored liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used for analysis of reagents, s

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  • Anisole

  • Casno:

    100-66-3

    Anisole

    Min.Order: 1 Gram

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  • AnisoleCAS NO.: 100-66-3

  • Casno:

    100-66-3

    AnisoleCAS NO.: 100-66-3

    Min.Order: 1 Gram

    FOB Price:  USD $ 2.0-2.0/Gram

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  • Best Quality Anisole

  • Casno:

    100-66-3

    Best Quality Anisole

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0/Kilogram

    Product name: Anisole CAS No.:100-66-3 Molecule Formula:C7H8O Molecule Weight:108.14 Purity: 99.5% Package: 200kg/drum Description:Clear colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEMS

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  • Casno:

    100-66-3

    Factory Supply Anisole

    Min.Order: 0

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  • Anisole

  • Casno:

    100-66-3

    Anisole

    Min.Order: 200 Kilogram

    FOB Price:  USD $ 0.0-0.0/Kilogram

    Synonyms:?ANISOL;ANISOLE;METHOXYBENZENE;METHYL?PHENYL?ETHER;AQUALINE?STANDARD?1.0;FEMA?2097;MOB;PHENOL?METHYL?ETHER MF:?C7H8O MW:?1…Appearance:colorless transperent liquid Storage:Store at RT. Package:200kg drums Application:interm

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Specification

The Anisole with CAS registry number of 100-66-3 is also known as Methoxybenzene. The IUPAC name and product name are the same. It belongs to product categories of Benzene derivatives; Anisole; Other Reagents. Its EINECS registry number is 202-876-1. In addition, the formula is C7H8O and the molecular weight is 108.14. This chemical is a clear straw colored liquid and should be stored in a ventilated and dry place.

Physical properties about Anisole are: (1)ACD/LogP: 2.17; (2)ACD/LogD (pH 5.5): 2.17; (3)ACD/LogD (pH 7.4): 2.17; (4)ACD/BCF (pH 5.5): 26.263; (5)ACD/BCF (pH 7.4): 26.263; (6)ACD/KOC (pH 5.5): 361.066; (7)ACD/KOC (pH 7.4): 361.066; (8)#H bond acceptors: 1; (9)#Freely Rotating Bonds: 1; (10)Index of Refraction: 1.492; (11)Molar Refractivity: 32.931 cm3; (12)Molar Volume: 113.436 cm3; (13)Surface Tension: 29.313 dyne/cm; (14)Density: 0.953 g/cm3; (15)Flash Point: 44.454 °C; (16)Enthalpy of Vaporization: 38.97 kJ/mol; (17)Boiling Point: 153.599 °C at 760 mmHg; (18)Vapour Pressure: 4.242 mmHg at 25 °C.

Preparation of Anisole: it is prepared by reaction of sodium phenoxide, a methyl bromide and related methylating reagents. What's more, the reaction belongs to the Williamson ether synthesis.

C6H5O-Na++CH3Br→CH3OC6H5+NaBr

Uses of Anisole: it is used to produce 2-methoxy-aniline. The reaction occurs with reagent n-BuLi the yield is about 35%. Besides, it is a precursor to perfumes, insect pheromones, and pharmaceuticals.

Anisole is used to produce 2-methoxy-aniline.

When you are using this chemical, please be cautious about it. As a chemical, it is irritating to skin, harmful by inhalation and flammable. During using it, wear suitable gloves and eye/face protection. Avoid contact with skin and eyes. Besides, keep away from sources of ignition. If contact with eyes accidently, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
1. Canonical SMILES: COC1=CC=CC=C1
2. InChI: InChI=1S/C7H8O/c1-8-7-5-3-2-4-6-7/h2-6H,1H3
3. InChIKey: RDOXTESZEPMUJZ-UHFFFAOYSA-N