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Cas Database |
| Name |
3-Nitrobenzyl alcohol |
EINECS | 210-588-2 |
| CAS No. | 619-25-0 | Density | 1.33 g/cm3 |
| PSA | 66.05000 | LogP | 1.61030 |
| Solubility | It is soluble in water. | Melting Point |
29-33 °C |
| Formula | C7H7NO3 | Boiling Point | 349.8 °C at 760 mmHg |
| Molecular Weight | 153.137 | Flash Point | 146.2 °C |
| Transport Information | N/A | Appearance | yellow to brown crystalline low melting solid |
| Safety | 24/25 | Risk Codes | 11-34 |
| Molecular Structure |
|
Hazard Symbols | Xi,C,F |
| Synonyms |
Benzyl alcohol,m-nitro- (6CI,7CI,8CI);(3-Nitrophenyl)methanol;3-Nitrobenzenemethanol;3-Nitrobenzyl alcohol;NSC 5388;m-Nitrobenzyl alcohol; |
Article Data | 180 |
3-Nitrobenzyl alcohol Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With magnesium(II) perchlorate; polymer-bound NADH (2a) In acetonitrile; benzene at 80℃; for 120h; Further byproducts given; | 100% |
| With sodium tetrahydroborate In ethanol at 20℃; for 0.5h; Inert atmosphere; | 100% |
| With sodium tetrahydroborate In ethanol at 0 - 20℃; | 99% |
- 18483-95-9
2-<3-Nitro-benzyloxy>-tetrahydro-pyran
- 619-25-0
3-Nitrobenzyl alcohol
Conditions
| Conditions | Yield |
|---|---|
| With aluminium trichloride; 2-(3-nitrophenyl)-1,3-dioxolane; 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane dichromate for 0.05h; | 100% |
| With silica triflate In methanol for 0.133333h; Heating; | 95% |
| With 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane dichromate In dichloromethane for 0.0569444h; Irradiation; | 93% |
- 62673-14-7
trimethyl(3-nitrobenzyloxy)silane
- 619-25-0
3-Nitrobenzyl alcohol
Conditions
| Conditions | Yield |
|---|---|
| With aluminium trichloride; 2-(3-nitrophenyl)-1,3-dioxolane; 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane dichromate for 0.05h; | 100% |
| With bismuth(lll) trifluoromethanesulfonate In methanol at 20℃; for 0.0666667h; | 97% |
| With Oxone In methanol for 0.4h; Heating; | 96% |
- 619-25-0
3-Nitrobenzyl alcohol
Conditions
| Conditions | Yield |
|---|---|
| With water | 100% |
Conditions
| Conditions | Yield |
|---|---|
| With N-methylpyrrolidine zinc borohydride In tetrahydrofuran at 20℃; for 0.666667h; | 98% |
| With (1,4-diazabicyclo{2.2.2}-octane)zinc(II) tetrahydoborate In tetrahydrofuran for 0.08h; Ambient temperature; | 90% |
- 1058649-37-8
3-nitro-1-[(ethoxymethoxy)methyl]benzene
- 619-25-0
3-Nitrobenzyl alcohol
Conditions
| Conditions | Yield |
|---|---|
| phosphotungstic acid In ethanol for 2h; Heating; | 97% |
- 256334-95-9
tert-butyl-dimethyl-(3-nitro-benzyloxy)-silane
- 619-25-0
3-Nitrobenzyl alcohol
Conditions
| Conditions | Yield |
|---|---|
| With Decaborane In methanol at 20℃; for 5h; | 93% |
Conditions
| Conditions | Yield |
|---|---|
| With C62H74Cl2N4Pd2S2; caesium carbonate In tetrahydrofuran; water at 50℃; for 2h; Inert atmosphere; Sealed tube; | 93% |
| With di-μ-chloro-bis{2-[3-(2,6-diisopropylphenyl)imidazolin-2-ylidene]-(3-phenylthio)phenyl-κ2C,C’}dipalladium(II) In tetrahydrofuran; water at 70℃; for 2h; Inert atmosphere; Sealed tube; Alkaline conditions; | 91% |
| With bis(η3-allyl-μ-chloropalladium(II)); 1-(2-bromophenyl)-3-(2,6-diisopropylphenyl)-4,5-dihydroimidazolinium chloride In tetrahydrofuran; water at 100℃; for 2h; Inert atmosphere; Sealed tube; | 73% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 3-nitro-benzaldehyde With potassium hydroxide In water at 20℃; Cannizzaro reaction; Stage #2: With hydrogenchloride In water | A 92% B 80% |
| With potassium hydroxide at 20℃; for 0.166667h; solvent-free Cannizzaro reaction; | A 33% B 53% |
| With N,N,N',N'-tetramethylguanidine In water at 100℃; for 10h; Cannizzaro reaction; | A 42% B 43% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; ethanol; cerium(III) chloride heptahydrate at 20℃; for 24h; chemospecific reaction; | 91% |
| With sodium tetrahydroborate; zinc phthalocyanine In PEG-400 at 100℃; for 10h; | 90% |
| With sodium tetrahydroborate In 1,4-dioxane; water for 2h; Ambient temperature; | 80% |
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3-Nitrobenzyl alcohol
