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Cas Database

Name	4-methoxybenzamide	EINECS	222-319-6
CAS No.	3424-93-9	Density	1.144 g/cm³
PSA	52.32000	LogP	1.49440
Solubility	N/A	Melting Point	164-167 °C(lit.)
Formula	C₈H₉NO₂	Boiling Point	295.803 °C at 760 mmHg
Molecular Weight	151.165	Flash Point	161.563 °C
Transport Information	N/A	Appearance	White crystalline powder
Safety	22-24/25	Risk Codes	36/37/38
Molecular Structure		Hazard Symbols	Xn
Synonyms	p-Anisamide(6CI,7CI,8CI);Anisamide;NSC 11139;p-Methoxybenzamide;	Article Data	403

4-methoxybenzamide Synthetic route

: 874-90-8
4-methoxybenzonitrile

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
With C18H57O3P6Ru2(1+)C6H5O(1-)C6H6O; water In 1,4-dioxane for 6h; Time; Sealed tube; Inert atmosphere; Schlenk technique;	100%
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); water; 2-(diphenylphosphino)-N,N-dimethylpyridine-4-amine In 1,2-dimethoxyethane at 80℃; for 5h;	99%
With C12H24O16Ru3*2H2O In water at 110℃; for 13h; Catalytic behavior; Schlenk technique; Inert atmosphere;	99%

: 123-11-5
4-methoxy-benzaldehyde

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
With hydroxylamine; C33H28F3N5O3Ru(1+)*Cl(1-) In water at 60℃; for 0.5h; Catalytic behavior; Sonication;	99%
Stage #1: 4-methoxy-benzaldehyde With hydroxylamine hydrochloride; caesium carbonate In water; dimethyl sulfoxide at 100℃; Stage #2: With palladium diacetate In water; dimethyl sulfoxide at 125℃; chemoselective reaction;	97%
With copper(ll) sulfate pentahydrate; hydroxylamine hydrochloride; sodium acetate at 110℃; for 2h; Neat (no solvent);	97%

: 100-09-4
4-methoxybenzoic acid

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
Stage #1: 4-methoxybenzoic acid With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In tetrahydrofuran for 0.0166667h; Milling; Stage #2: With ammonium thiocyanate In tetrahydrofuran for 0.0833333h; Milling;	99%
With pyridine; urea for 0.00833333h; microwave irradiation;	90%
Stage #1: 4-methoxybenzoic acid With thionyl chloride In tetrahydrofuran at 50℃; for 1h; Stage #2: With ammonium hydroxide In tetrahydrofuran at 0℃; for 0.0833333h;	84%

: 19486-73-8
N-tert-butyl-4-methoxybenzamide

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
scandium tris(trifluoromethanesulfonate) In nitromethane at 170℃; for 1h; Irradiation;	99%
With t-butyldimethylsiyl triflate In toluene at 100℃; for 8h;	74%

: 619-57-8
p-hydroxybenzamide

: 616-38-6
carbonic acid dimethyl ester

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
With dmap at 135℃; under 3000.3 Torr; for 7h; Pressure; Temperature; Reagent/catalyst;	99%

: 100-07-2
4-methoxy-benzoyl chloride

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
With ammonia Inert atmosphere;	98%
With ammonia at -10 - 20℃; for 1h; Temperature;	96.3%
With ammonia In water at 20℃; for 1h;	79%

: 105-13-5
4-Methoxybenzyl alcohol

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
With tert.-butylhydroperoxide; ammonia; oxygen In water; N,N-dimethyl-formamide at 80℃; under 1520.1 Torr; for 5h; Green chemistry;	98%
Stage #1: 4-Methoxybenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ammonia; oxygen; copper(II) nitrate In water; dimethyl sulfoxide at 80℃; under 760.051 Torr; for 5h; Stage #2: With Acetaldehyde oxime In water; dimethyl sulfoxide at 110℃; for 24h; Inert atmosphere;	97%
With ammonia; oxygen In water at 150℃; under 22502.3 Torr; for 3h;	96.5%

: 2393-23-9
4-methoxy-benzylamine

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
With manganese(IV) oxide at 130℃; under 4560.31 Torr; for 3h;	98%
With dihydrogen peroxide at 80℃; for 10h; Inert atmosphere;	96%
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); potassium tert-butylate In tert-butyl alcohol at 70℃; for 12h;	95%

: 3532-17-0
4-methoxybenzoyl azide

: 3424-93-9
4-methoxyphenylacetamide

Conditions

Conditions	Yield
With (1,4-diazabicyclo{2.2.2}-octane)zinc(II) tetrahydoborate In tetrahydrofuran for 48h; Ambient temperature;	97%
With 1,3-diadamantane-4,5-dihydroimidazole chloride; potassium tert-butylate; bis(pinacol)diborane; copper(l) chloride In toluene at 25℃; for 4h; Schlenk technique; Inert atmosphere;	94%
With sodium tetrahydroborate; copper(II) sulfate In methanol at 0 - 5℃; for 1h;	92%

: 874-90-8
4-methoxybenzonitrile

A: 3424-93-9
4-methoxyphenylacetamide

B: 5373-87-5
4-methoxybenzamidoxime

Conditions

Conditions	Yield
With hydroxylamine In ethanol for 3h; Reagent/catalyst; Reflux;	A 97% B n/a
With hydroxylamine hydrochloride; sodium hydroxide In ethanol; water Reflux;

4-methoxybenzamide Chemical Properties

Product Name: 4-Methoxybenzamide
The MF of 4-Methoxybenzamide (3424-93-9) is C₈H₉NO₂.

The MW of 4-Methoxybenzamide (3424-93-9) is 151.16.
Synonyms of 4-Methoxybenzamide (3424-93-9): p-Anisamide ; p-Methoxybenzamide
Product Categories: Aromatic Carboxylic Acids,Anilides, Anhydrides & Salts
Form: white crystalline powder
Index of Refraction: 1.546
EINECS: 222-319-6
Density: 1.143 g/ml
Flash Point: 161.5 °C
Boiling Point: 295.8 °C
Melting Point: 164-167 °C
BRN: 1862847

4-methoxybenzamide Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
mammal (species unspecified)	LD50	unreported	1gm/kg (1000mg/kg)		Pharmaceutical Chemistry Journal Vol. 28, Pg. 335, 1994.

4-methoxybenzamide Safety Profile

Safety information of 4-Methoxybenzamide (3424-93-9):
Risk Statements
36/37/38 Irritating to eyes, respiratory system and skin
Safety Statements
22 Do not breathe dust
24/25 Avoid contact with skin and eyes
WGK Germany 3
RTECS CV5466666

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