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2,3-dihydro-7-methylindole
7-methyl-1H-indole
Conditions | Yield |
---|---|
With 6C44H32N6O4Ru(2+)*12Hf(2+)*8O(2-)*14HO(1-)*6C16H22ClCoN5O6(1-) In 2,2,2-trifluoroethanol; acetonitrile at 20℃; for 12h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Irradiation; | 99% |
With H8O20P8Pt2(4-)*4C34H72N(1+) In methanol Inert atmosphere; Irradiation; | 97% |
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; chloropyridinecobaloxime(III) In ethanol at 30℃; for 24h; Inert atmosphere; Schlenk technique; Irradiation; | 89% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; hexane at 40 - 45℃; for 40h; | 93% |
With n-butyllithium; diisopropylamine In tetrahydrofuran; hexanes at -78 - 45℃; for 40h; Inert atmosphere; | 93% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 7-methyl-1-tosylindoline In tetrahydrofuran at -78℃; for 2h; Stage #2: With oxygen In tetrahydrofuran at 20℃; | 84% |
6-methyl-2-vinylaniline
7-methyl-1H-indole
Conditions | Yield |
---|---|
With p-benzoquinone; lithium chloride; dichloro bis(acetonitrile) palladium(II) In tetrahydrofuran for 10h; Heating; | 82% |
Conditions | Yield |
---|---|
With triphenylphosphine; tin(ll) chloride; ruthenium trichloride In 1,4-dioxane; water at 180℃; for 20h; Cyclization; | 80% |
With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane; water at 180℃; for 20h; | 80% |
C9H8N2O4
7-methyl-1H-indole
Conditions | Yield |
---|---|
With indium; acetic acid In benzene at 80℃; for 5h; Inert atmosphere; | 76% |
7-methyl-1-(phenylsulfonyl)-1H-indole
7-methyl-1H-indole
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; 1,2-dimethoxyethane for 24h; Heating; | 75% |
7-methyl-2-trimethylsilanyl-indole-1-carboxylic acid diethylamide
7-methyl-1H-indole
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 12h; Heating; | 75% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -45 - -40℃; Cyclization; Bartoli reaction; | 71% |
In tetrahydrofuran at -40℃; for 0.333333h; | 67% |
In tetrahydrofuran at -40℃; for 1h; Inert atmosphere; | 34% |
1-(2-amino-3-methylphenyl)-2-chloroethan-1-one
7-methyl-1H-indole
Conditions | Yield |
---|---|
With sodium tetrahydroborate In 1,4-dioxane; water for 2h; Heating; | 71% |
7-Methylindole is used in the production of agricultural chemicals and pharmaceuticals.
7-Methylindole is used for organic synthetic reagent.