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3663-20-5

3663-20-5

Identification

Synonyms:Acetanilide,4'-butyl- (7CI,8CI);4-(n-Butyl)acetanilide;4'-Butylacetanilide;N-(4-Butylphenyl)acetamide;p-Butylacetanilide;

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Safety information and MSDS view more

  • Pictogram(s):R22:Harmful if swallowed.;

  • Hazard Codes: Xn:Harmful;

  • Signal Word:no data available

  • Hazard Statement:no data available

  • First-aid measures: General adviceConsult a physician. Show this safety data sheet to the doctor in attendance.If inhaled If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician. In case of skin contact Wash off with soap and plenty of water. Consult a physician. In case of eye contact Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician. If swallowed Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.

  • Fire-fighting measures: Suitable extinguishing media Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide. Wear self-contained breathing apparatus for firefighting if necessary.

  • Accidental release measures: Use personal protective equipment. Avoid dust formation. Avoid breathing vapours, mist or gas. Ensure adequate ventilation. Evacuate personnel to safe areas. Avoid breathing dust. For personal protection see section 8. Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the environment must be avoided. Pick up and arrange disposal. Sweep up and shovel. Keep in suitable, closed containers for disposal.

  • Handling and storage: Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Avoid exposure - obtain special instructions before use.Provide appropriate exhaust ventilation at places where dust is formed. For precautions see section 2.2. Store in cool place. Keep container tightly closed in a dry and well-ventilated place.

  • Exposure controls/personal protection:Occupational Exposure limit valuesBiological limit values Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of workday. Eye/face protection Safety glasses with side-shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN 166(EU). Skin protection Wear impervious clothing. The type of protective equipment must be selected according to the concentration and amount of the dangerous substance at the specific workplace. Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique(without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and the standard EN 374 derived from it. Respiratory protection Wear dust mask when handling large quantities. Thermal hazards

Supplier and reference price view more

  • Manufacture/Brand
  • Product Description
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  • Manufacture/Brand:TRC
  • Product Description:N-(4-Butylphenyl)acetamide
  • Packaging:100mg
  • Price:$ 45
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:N-(4-BUTYLPHENYL)ACETAMIDE AldrichCPR
  • Packaging:50mg
  • Price:$ 144
  • Delivery:In stock
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  • Manufacture/Brand:Biosynth Carbosynth
  • Product Description:N-(4-Butylphenyl)acetamide
  • Packaging:1 g
  • Price:$ 150
  • Delivery:In stock
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  • Manufacture/Brand:Biosynth Carbosynth
  • Product Description:N-(4-Butylphenyl)acetamide
  • Packaging:500 mg
  • Price:$ 95
  • Delivery:In stock
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  • Manufacture/Brand:Biosynth Carbosynth
  • Product Description:N-(4-Butylphenyl)acetamide
  • Packaging:250 mg
  • Price:$ 50
  • Delivery:In stock
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  • Manufacture/Brand:Biosynth Carbosynth
  • Product Description:N-(4-Butylphenyl)acetamide
  • Packaging:5 g
  • Price:$ 550
  • Delivery:In stock
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  • Manufacture/Brand:Biosynth Carbosynth
  • Product Description:N-(4-Butylphenyl)acetamide
  • Packaging:2 g
  • Price:$ 260
  • Delivery:In stock
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  • Manufacture/Brand:American Custom Chemicals Corporation
  • Product Description:N1-(4-BUTYLPHENYL)ACETAMIDE 95.00%
  • Packaging:25G
  • Price:$ 1243.07
  • Delivery:In stock
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  • Manufacture/Brand:American Custom Chemicals Corporation
  • Product Description:N1-(4-BUTYLPHENYL)ACETAMIDE 95.00%
  • Packaging:10G
  • Price:$ 1177.59
  • Delivery:In stock
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  • Manufacture/Brand:AK Scientific
  • Product Description:N-(4-Butylphenyl)acetamide
  • Packaging:1g
  • Price:$ 252
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Relevant articles and documentsAll total 13 Articles be found

Efficient nitriding reagent and application thereof

-

Paragraph 0111-0112, (2021/03/31)

The invention discloses an efficient nitriding reagent and application thereof, wherein the nitriding reagent comprises nitrogen oxide, an active agent, a reducing agent and an organic solvent. By applying the nitriding reagent, nitrogen-containing compounds such as amide, nitrile and the like can be produced, and the method is simple in condition, low in waste discharge amount and simple in reaction equipment.

Visible-Light-Induced Nickel-Catalyzed Cross-Coupling with Alkylzirconocenes from Unactivated Alkenes

Bai, Songlin,Gao, Yadong,Jiang, Chao,Liu, Xiaolei,Qi, Xiangbing,Wang, Jing,Wu, Qingcui,Yang, Chao

supporting information, p. 675 - 688 (2020/03/11)

-

Efficient Heterogeneous Gold(I)-Catalyzed Direct C(sp2)–C(sp) Bond Functionalization of Arylalkynes through a Nitrogenation Process to Amides

Nie, Quan,Yi, Feiyan,Huang, Bin,Cai, Mingzhong

, p. 3968 - 3976 (2017/11/20)

The first heterogeneous gold(I)-catalyzed direct C(sp2)–C(sp) bond functionalization of arylalkynes through a nitrogenation process to amides has been achieved by using an ordered mesoporous silica (MCM-41)-immobilized phosphine gold(I) complex [MCM-41-PPh3-AuCl] as catalyst and silver carbonate (Ag2CO3) as cocatalyst with trimethylsilyl azide (TMSN3) as a nitrogen source, yielding a variety of amides in moderate to excellent yields under mild conditions. This heterogeneous phosphine gold(I) complex shows the same turnover numbers as the homogeneous chloro(triphenylphosphine)gold(I) (Ph3PAuCl) and can easily be recovered by simple filtration of the reaction solution and recycled at least eight times without significant loss of activity, providing a novel, efficient, practical and economic method for the synthesis of amides from alkynes. (Figure presented.).

Process route upstream and downstream products

Process route

4-Butylaniline
104-13-2

4-Butylaniline

acetic anhydride
108-24-7

acetic anhydride

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
With N,N,N-trimethyl-2-(sulfooxy)ethanaminium chloride; In neat (no solvent); at 20 ℃; for 0.233333h; Milling; Green chemistry;
92%
sulfuric acid; at 50 ℃; for 1h;
90%
With pyridine; at 0 - 90 ℃; for 4h; Inert atmosphere;
88%
With pyridine; acetic anhydride; at 80 ℃; for 3.5h;
84%
With dmap; triethylamine; In toluene; at 20 ℃; for 12.5h; Cooling with ice;
In water; at 20 ℃; for 2h;
5.21 g
With sulfuric acid; at 58 ℃; for 1.8h;
1-(4-butylphenyl)ethanone
37920-25-5

1-(4-butylphenyl)ethanone

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
With nitromethane; trifluoromethylsulfonic anhydride; In formic acid; at 80 - 120 ℃;
70%
With formic acid; nitromethane; trifluoromethylsulfonic anhydride; In acetic acid; at 100 ℃; for 12h;
70%
4-Butylaniline
104-13-2

4-Butylaniline

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
With acetic anhydride; In ethanol; water; toluene;
90.3%
(4-butylphenyl)acetylene
79887-09-5

(4-butylphenyl)acetylene

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
With trimethylsilylazide; silver carbonate; trifluoroacetic acid; In water; 1,2-dichloro-ethane; at 60 ℃; for 12h; Schlenk technique; Inert atmosphere;
96%
With formic acid; nitromethane; trifluoromethylsulfonic anhydride; In acetic acid; at 100 ℃; for 12h;
68%
4-Butylaniline
104-13-2

4-Butylaniline

acetic acid
64-19-7,77671-22-8

acetic acid

4-butyl-2-chlorophenylamine
1111300-72-1

4-butyl-2-chlorophenylamine

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
With oxygen; lithium chloride; copper dichloride; In dodecane; at 100 ℃; for 15h; under 760.051 Torr;
1-butyl-4-nitro-benzene
20651-75-6

1-butyl-4-nitro-benzene

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: tin; hydrochloric acid
With hydrogenchloride; tin;
4-Acetamido-1-iodobenzene
622-50-4

4-Acetamido-1-iodobenzene

N-(4-hexylphenyl)acetamide
20330-59-0

N-(4-hexylphenyl)acetamide

N-(4-heptylphenyl)acetamide
20330-65-8

N-(4-heptylphenyl)acetamide

N-(4-octylphenyl)acetamide
37593-11-6

N-(4-octylphenyl)acetamide

N-(4-nonylphenyl)acetamide
37593-12-7

N-(4-nonylphenyl)acetamide

N-(4-decylphenyl)acetamide
37593-13-8

N-(4-decylphenyl)acetamide

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

N-(4-pentylphenyl)acetamide
20330-52-3

N-(4-pentylphenyl)acetamide

N-(4-undecylphenyl)acetamide
102707-88-0

N-(4-undecylphenyl)acetamide

N-acetyl-4-n-dodecylaniline
3663-30-7

N-acetyl-4-n-dodecylaniline

N-(4-tridecylphenyl)acetamide
68777-64-0

N-(4-tridecylphenyl)acetamide

N-(4-tetradecylphenyl)acetamide
72755-62-5

N-(4-tetradecylphenyl)acetamide

Conditions
Conditions Yield
1-hexene; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; at 70 ℃; for 12h; Inert atmosphere; Sealed tube;
With Schwartz's reagent; In tetrahydrofuran; at 50 ℃; for 5h; Inert atmosphere; Sealed tube;
4-Acetamido-1-iodobenzene; With 4,4'-di-tert-butyl-2,2'-bipyridine nickel(II) bromide; tetrabutylammonium p-toluenesulfonate; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Irradiation; Sealed tube;
12%
11%
11%
10%
8%
7%
7%
5%
5%
2%
2%
4-Butylaniline
104-13-2

4-Butylaniline

acetic acid
64-19-7,77671-22-8

acetic acid

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
aniline
62-53-3

aniline

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: zinc chloride / 230 - 240 °C
With zinc(II) chloride;
Multi-step reaction with 3 steps
1: zinc chloride / 180 - 200 °C
2: cobalt chloride / >200
With cobalt chloride; zinc(II) chloride;
acetic acid-(4-but-2-enyl-anilide)

acetic acid-(4-but-2-enyl-anilide)

N-(4-butylphenyl)acetamide
3663-20-5

N-(4-butylphenyl)acetamide

Conditions
Conditions Yield
With palladium; acetic acid; Hydrogenation;

Global suppliers and manufacturers

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  • Finetech Industry Limited
  • Business Type:Trading Company
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  • Antimex Chemical Limied
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  • MENGNA
  • Business Type:Lab/Research institutions
  • Contact Tel:18698110882
  • Emails:mengna198504@163.com
  • Main Products:1
  • Country:China (Mainland)
  • Debye Scientific
  • Business Type:Lab/Research institutions
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  • Emails:sales@debyesci.com
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  • Country:China (Mainland)
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