Conditions |
Yield |
With
2C12H30N2(2+)*Ga(3+)*7Zn(2+)*10HO3P(2-)*8H2O*F(1-);
In
ethanol;
at 85 ℃;
|
99%
|
With
(H3O)2[Cd3(9H-carbazole-2,7-dicarboxylic acid(-2H))4]·3DMF·4H2O;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
Reagent/catalyst;
Temperature;
Inert atmosphere;
|
97%
|
With
G/MFSiO2Cu(proline)2;
at 20 ℃;
for 5h;
Green chemistry;
|
97%
|
With
piperidine;
In
acetic acid; benzene;
for 2h;
Heating;
|
93%
|
With
iridium hydroxyapatite;
at 120 ℃;
for 1h;
|
92%
|
With
aluminum (III) chloride;
In
dichloromethane;
at 20 ℃;
for 2h;
|
88%
|
benzaldehyde;
With
L-proline;
In
dimethyl sulfoxide;
at 20 ℃;
ethyl acetoacetate;
In
dimethyl sulfoxide;
at 80 ℃;
|
88%
|
With
1-butyl-3-methylimidazolium hydroxide;
at 25 - 30 ℃;
for 0.333333h;
|
87%
|
With
cobalt hydroxyapatite;
at 80 ℃;
for 0.166667h;
|
87%
|
With
piperidine; acetic acid;
In
toluene;
at 20 ℃;
for 19h;
Molecular sieve;
|
84%
|
With
L-Tryptophan;
In
dimethyl sulfoxide;
at 20 ℃;
|
81%
|
|
80%
|
With
potassium carbonate;
PEG400;
at 90 ℃;
for 2h;
|
76%
|
With
samarium (III) iodide;
In
tetrahydrofuran;
for 3h;
Ambient temperature;
|
75%
|
With
1-(butyl-4-sulfo)-3-methylimidazolium hydrogen sulfate;
In
neat (no solvent);
at 100 ℃;
Green chemistry;
|
70%
|
With
mesoporous hybrid catalyst HYB-75P-25B;
In
ethanol;
at 79.84 ℃;
for 24h;
Inert atmosphere;
|
66%
|
With
mesoporous MCM-41 silica-supported silylated base hybrid catalyst;
In
acetonitrile;
at 80 ℃;
for 24h;
Reagent/catalyst;
Catalytic behavior;
|
65%
|
With
3-aminopropyl-functionalized silica gel;
In
toluene;
at 25 ℃;
Product distribution;
also 3-(N,N-dimethylamino)propyl-functionalized silica gel, unfunctionalized silica gel; other active methylene compounds, other carbonyl compounds, other temperature;
|
59%
|
With
3-aminopropyl-functionalized silica gel;
In
toluene;
at 25 ℃;
continuous-flow conditions;
|
59%
|
With
urea-functionalized mesoporous polymeric catalyst;
In
water;
at 50 ℃;
for 24h;
|
57%
|
With
mesoporous titanosilicate Ti-TUD-1 catalyst;
In
ethanol;
at 20 ℃;
for 6h;
|
54%
|
With
piperidine; benzoic acid;
In
ethanol;
at 20 ℃;
for 18h;
|
54%
|
With
chloro-trimethyl-silane; sodium iodide;
In
diethyl ether; acetonitrile;
for 7h;
0 deg C to room temperature;
|
45%
|
With
layered hybrid materials from triethoxymethylsilane modified with protonic acid;
In
acetonitrile;
at 80 ℃;
for 7h;
Inert atmosphere;
|
23%
|
modified Amberlite IRC-50 resin;
In
benzene;
for 6h;
Ambient temperature;
|
22%
|
With
KNO3 converted to K2O at 300°C on nanoporous Cr-organic framework (MIL-53(Cr));
In
ethanol;
at 70 ℃;
for 1h;
|
20.1%
|
With
bifunctional Fe nanoparticles implanted on p-phenylenediamine-modified reduced graphene oxide;
In
toluene;
at 40 ℃;
for 3.5h;
Catalytic behavior;
|
20.6%
|
With
Thiamine hydrochloride;
for 1h;
|
10%
|
With
piperidine; ethanol;
|
|
With
hydrogenchloride;
at 0 ℃;
|
|
3-(trimethoxysilyl)propan-1-amine; silica gel;
In
toluene;
at 25 ℃;
|
|
|
|
With
piperidine;
In
1,4-dioxane;
at 20 ℃;
further method: piperidine, HOAc, benzene, reflux;
|
|
With
chloro-trimethyl-silane;
at 20 ℃;
|
|
With
piperidine; acetic acid;
In
benzene;
for 1h;
Heating;
|
|
With
piperidine; acetic acid;
|
|
With
polymer-bound piperazinediium diacetate;
In
chlorobenzene;
at 115 ℃;
for 5h;
|
|
1,1'-methylenebis(3-methylpiperidine);
at 20 ℃;
|
|
With
pyridine;
for 1h;
Heating;
|
|
With
gem-diamine piperidinomethane piperidium tetrafluoroborate;
at 80 ℃;
for 0.166667h;
Inert atmosphere;
neat (no solvent);
|
100 %Chromat.
|
With
piperidine;
|
|
With
(2-hydroxyethyl)trimethylammonium DL-threoninate;
at 20 ℃;
for 24h;
Inert atmosphere;
Neat (no solvent);
|
|
With
piperidine; acetic acid;
In
toluene;
at 20 ℃;
for 19h;
Molecular sieve;
|
|
|
|
Acidic conditions;
|
|
With
activated Cs-Norit carbon catalyst;
at 119.84 ℃;
for 4h;
|
|
With
sodium hydroxide;
In
water;
at 40 ℃;
|
|
With
piperidine; acetic acid;
In
toluene;
Reflux;
Inert atmosphere;
|
|
With
3C14H15N2O(1+)*O40PW12(3-);
In
neat (no solvent);
at 70 ℃;
for 20h;
|
|
With
3-aminopropyl immobilised on mesoporous silica MCM-41;
In
toluene;
at 60 ℃;
for 1h;
|
|
With
zeolite TS-1;
In
para-xylene;
at 130 ℃;
for 24h;
under 760.051 Torr;
Reagent/catalyst;
Time;
|
|
ethyl acetoacetate;
With
isoreticular MOF-3 catalyst;
In
dimethyl sulfoxide;
at 79.84 ℃;
Inert atmosphere;
benzaldehyde;
In
dimethyl sulfoxide;
at 79.84 ℃;
for 2.16667h;
Solvent;
Temperature;
Reagent/catalyst;
Kinetics;
Inert atmosphere;
|
|
With
10 wt.percent magnetic iron oxide nanoparticles incorporating and alklylamine grafting in MCM-41;
In
neat (no solvent);
at 119.84 ℃;
Reagent/catalyst;
Inert atmosphere;
|
|
With
Cs-X zeolite;
at 140 ℃;
Reagent/catalyst;
|
|
With
{[Ni4(μ6-methanetetrabenzoate)2(μ2-H2O)4(H2O)4]·10DMF·11H2O}n;
In
dodecane; para-xylene;
at 130 ℃;
under 760.051 Torr;
|
|
With
strongly basic gel-type cross-linked guanidine-methylated poly(styrene-co-divinylbenzene) resin (PGX resin);
In
ethanol;
at 70 ℃;
for 4h;
|
83.1 %Chromat.
|
|
|
With
halloysite;
In
neat (no solvent);
at 70 ℃;
|
|
With
Ba2(1,3,5-benzenetricarboxylate)(NO3)(N,N-dimethylformamide);
In
toluene;
at 110 ℃;
|
|
|
|
With
morpholine;
In
ethanol;
at 20 ℃;
for 24h;
|
1.85 g
|
With
triethylamine;
In
ethanol;
for 2h;
Reflux;
|
|
With
piperidine;
In
ethyl acetate;
at 85 ℃;
Temperature;
Flow reactor;
|
|
With
L-Tryptophan;
In
dimethyl sulfoxide;
at 20 ℃;
|
|
With
piperidine; acetic acid;
In
neat (no solvent);
at 20 ℃;
for 24h;
|
|
With
aluminum (III) chloride;
In
neat (no solvent);
at 20 ℃;
for 0.5h;
Sealed tube;
Milling;
|
|
With
piperidine;
In
dichloromethane;
at 20 ℃;
|
|
With
[Pb4(μ8-methanetetrabenzoate)2];
In
para-xylene;
at 129.84 ℃;
for 8h;
|
|
With
4Pb(2+)*2C29H16O8(4-)*4H2O*5C3H7NO;
In
para-xylene;
at 130 ℃;
for 6h;
under 760.051 Torr;
|
|
With
piperidine; trifluoroacetic acid;
In
dichloromethane;
Reflux;
|
|
With
Na0.13Cs0.81AlSi5O12;
In
dimethyl sulfoxide;
at 100 ℃;
Reagent/catalyst;
Catalytic behavior;
Inert atmosphere;
|
|
With
[Zn(oba)(4-bpdh)0.5]n*(DMF)1.5;
In
water;
at 20 ℃;
for 0.416667h;
under 760.051 Torr;
Reagent/catalyst;
Catalytic behavior;
Sealed tube;
Green chemistry;
|
|
With
piperidine; acetic acid;
In
benzene;
Reflux;
Dean-Stark;
|
|