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Ciprofloxacin hydrochloride hydrate
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Name

Ciprofloxacin hydrochloride hydrate

 EINECS 617-845-1
CAS No. 86393-32-0 Density N/A
PSA 83.80000 LogP 2.71480
Solubility Soluble in water (35mg/ml). Melting Point 318-320 °C
Formula C17H18FN3O3.ClH.H2O Boiling Point 581.8 °C at 760 mmHg
Molecular Weight 385.823 Flash Point 305.6 °C
Transport Information N/A Appearance White or yellowish crystalline powder
Safety Risk Codes R36/37/38
Molecular Structure Molecular Structure of 86393-32-0 (Ciprofloxacin hydrochloride hydrate) Hazard Symbols Xi
Synonyms

3-Quinolinecarboxylicacid, 1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-,monohydrochloride, monohydrate (9CI);Ciprofloxacin hydrochloride monohydrate;Ciprofloxacin Monohydrochloridecas;Ciprofloxacin Monohydrochloride;Ciprofloxacin hydrochloride;Ciprofloxaicin HCl;3-Quinolinecarboxylicacid, 1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-,hydrochloride, hydrate (1:1:1);

 

Ciprofloxacin hydrochloride hydrate Synthetic route

86393-32-0

1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-quinoline-3-carboxylic acid HCl monohydrate

93107-08-5

ciprofloxacin hydrochloride

Conditions
ConditionsYield
In ethanol for 24 - 72h; Product distribution / selectivity;88%
In iso-butanol for 2h; Product distribution / selectivity;88%
86393-32-0

1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-quinoline-3-carboxylic acid HCl monohydrate

europium(III) chloride hexahydrate

7732-18-5

water

[Eu(ciprofloxacin)(ciprofloxacin(-1H))(H2O)4]Cl2*8H2O

Conditions
ConditionsYield
With 1,3-bis(dimethylamino)-2-propanol In ethanol; water High Pressure; Eu salt, ligand and 1,3-bis(dimethylamino)-2-propanol added to a mixt. of H2O and EtOH, stirred, placed in an autoclave, heated at 150°C for 48 h; crystd. for 1 wk; elem. anal.;47.2%
86393-32-0

1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-quinoline-3-carboxylic acid HCl monohydrate

7732-18-5

water

mercury dichloride

(H-1-cyclopropyl-6-fluoro-4-oxo-7-(1-piperazinyl)-1,4-dihydroquinoline-3-carboxylic acid)2HgCl4*2H2O

Conditions
ConditionsYield
In water satd. aq. solns. ligand and HgCl2 were mixed in 2:1 ratio; ppt. was filtered off, dried in air; elem. anal.;
86393-32-0

1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-quinoline-3-carboxylic acid HCl monohydrate

aqueous cadmium chloride

(H-1-cyclopropyl-6-fluoro-4-oxo-7-(1-piperazinyl)-1,4-dihydroquinoline-3-carbohylic acid)2(CdCl4)*2H2O

Conditions
ConditionsYield
In water satd. aq. solns. ligand and CdCl2*2.5H2O were mixed in 2:1 ratio; ppt. was filtered off, dried in air; elem. anal.;
86393-32-0

1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-quinoline-3-carboxylic acid HCl monohydrate

aqueous cadmium chloride

(H2-1-cyclopropyl-6-fluoro-4-oxo-7-(1-piperazinyl)-1,4-dihydroquinoline-3-carboxylic acid)CdCl4*H2O

Conditions
ConditionsYield
With HCl In hydrogenchloride solns. ligand and CdCl2*2.5H2O in concd. HCl were mixed in 1:1 ratio, mixt. was stand for several days; ppt. was filtered off, washed with acetone, dried in air; elem. anal.;
86393-32-0

1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-quinoline-3-carboxylic acid HCl monohydrate

mercury dichloride

(H2-1-cyclopropyl-6-fluoro-4-oxo-7-(1-piperazinyl)-1,4-dihydroquinoline-3-carboxylic acid)HgCl4

Conditions
ConditionsYield
With HCl In hydrogenchloride solns. ligand and HgCl2 in concd. HCl were mixed in 1:1 ratio, mixt. wasstand for several days; ppt. was filtered off, washed with acetone, dried in air; elem. anal.;

Ciprofloxacin hydrochloride hydrate Chemical Properties


IUPAC Name: 1-Cyclopropyl-6-fluoro-4-oxo-7-piperazin-1-ylquinoline-3-carboxylic acid hydrate hydrochloride
Molecular Formula: C17H18FN3O3.HCl.H2O
Molecular Weight: 385.82 g/mol
InChI: InChI=1/C17H18FN3O3.ClH.H2O/c18-13-7-11-14(8-15(13)20-5-3-19-4-6-20)21(10-1-2-10)9-12(16(11)22)17(23)24;;/h7-10,19H,1-6H2,(H,23,24);1H;1H2
SMILES: N1CCN(CC1)c1c(F)cc2c(n(cc(c2=O)C(O)=O)C2CC2)c1.Cl.O
Classification Code: Antibacterial
Product Categories: Active Pharmaceutical Ingredients; Quinolones (Antibiotics for Research and Experimental Use); Antibiotics for Research and Experimental Use; Biochemistry; Antibiotic Explorer; Peptide Synthesis / Antibiotics
Flash Point: 305.6 °C
Enthalpy of Vaporization: 91.5 kJ/mol
Boiling Point: 581.8 °C at 760 mmHg
Melting Point: 318-320 °C
storage temperature: 0-6 °C
Vapour Pressure of Ciprofloxacin hydrochloride hydrate (CAS NO.86393-32-0): 2.24E-14 mmHg at 25 °C

Ciprofloxacin hydrochloride hydrate Specification

 Ciprofloxacin hydrochloride hydrate (CAS NO.86393-32-0), its Synonyms are 1-Cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(1-piperazinyl)-3-quinolinecarboxylic acid, monohydrochloride, monohydrate ; Alcipro ; Belmacina ; Catex ; Cenin ; Ceprimax ; Ciprofloxacin HCl ; Ciprofloxacin hydrochloride ; Ciprofloxacin hydrochloride monohydrate .

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