Synthesis p. 195 - 197 (1996)
Update date:2022-08-03
Topics:
Ghosh, Debasis
Nichols, David E.
Nitration of cyclic conjugated olefins was achieved in a one-pot procedure using nitryl iodide generated in situ from iodine and potassium nitrite complexed with 18-crown-6 in tetrahydrofuran under sonication/stirring, followed by treatment of the unstable iodo nitro compound with base. The yield of the nitro compound varied from 52 to 90%.
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