Journal of Organic Chemistry p. 2500 - 2504 (1986)
Update date:2022-08-04
Topics:
Stipanovic, Robert D.
McCormick, John P.
Schlemper, Elmer O.
Hamper, Bruce C.
Shinmyozu, Teruo
Pirkle, William H.
Methods for determination of absolute configuration were independently applied to the phytoalexin lacinilene C methyl ether.The results from circular dichroism, NMR spectroscopy utilizing chiral solvating agents, and chiral stationary phase chromatography allow assignment of the R configuration to (+)-lacinilene C methyl ether.This assignment was verified by X-ray diffraction.Chemical conversion permitted assignment of the R configuration to (+)-lacinilene C.
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